3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE

Product Name: 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE
CAS No.: 39741-46-3
Chemical Name: 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE
Synonyms: 5-Bromo-3-(chloromethyl)pyridine hydrochloride;3-Bromo-5-(chloromethyl)pyridine hydrochloride 95%;3-Bromo-5-(chloromethyl)pyridine hydrochloride 95+%;3-bromo-5-(chloromethyl)-Pyridine hydrochloride (1:1);Pyridine, 3-bromo-5-(chloromethyl)-, hydrochloride (1:1)
CBNumber: CB21010330
Molecular Formula: C6H5BrClN.ClH
Formula Weight: 0
MOL File: 39741-46-3.mol

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3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Property

storage temp.: Inert atmosphere,Room Temperature
form: crystalline solid
color: White to off-white
CAS DataBase Reference: 39741-46-3

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Safety

Hazard Codes: C
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B415535
Product name: 3-Bromo-5-(chloromethyl)pyridineHydrochloride
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: V1765
Product name: 3-Bromo-5-(chloromethyl)pyridinehydrochloride
Packaging: 250mg
Price: $64
Updated: 2021/12/16

Apolloscientific

Product number: OR14923
Product name: 3-Bromo-5-(chloromethyl)pyridinehydrochloride
Purity: 95+%
Packaging: 250mg
Price: $174
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-D-60
Product name: 3-Bromo-5-(chloromethyl)pyridinehydrochloride
Purity: 95%
Packaging: 250mg
Price: $192
Updated: 2021/12/16

Apolloscientific

Product number: OR14923
Product name: 3-Bromo-5-(chloromethyl)pyridinehydrochloride
Purity: 95+%
Packaging: 1g
Price: $290
Updated: 2021/12/16

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3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

37669-64-0

39741-46-3

The general procedure for the synthesis of 3-bromo-5-(chloromethyl)pyridine hydrochloride from 3-bromopyridine-5-methanol was as follows: (5-bromopyridin-3-yl)methanol (XLV) (1.54 g, 8.2 mmol) was dissolved in a dioxane solution (10 mL) of 4 M HCl at 0 °C, followed by evaporation treatment. The resulting residue was dissolved in SOCl2 (4 mL) and reacted under reflux conditions for 2 hours. Upon completion of the reaction, SOCl2 was removed and the residue was ground with hexane to afford the HCl salt of 3-bromo-5-(chloromethyl)pyridine (XLVT) as a brown solid (1.30 g, 5.4 mmol, 66% yield). The product was used for subsequent experiments without further purification.ESIMS analysis showed that the product C6H5BrClN had a m/z of 206 (M + H).

References

[1] Patent: WO2013/40215, 2013, A1. Location in patent: Paragraph 00268
[2] Nucleosides and Nucleotides, 1994, vol. 13, # 10, p. 2345 - 2366
[3] Patent: WO2012/148808, 2012, A1. Location in patent: Page/Page column 78
[4] Patent: WO2018/75858, 2018, A1. Location in patent: Paragraph 0299; 0301

3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Suppliers

Belgium 1 China 56 India 1 United Kingdom 1 United States 10 Global 69

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View Lastest Price from 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-Bromo-5-(chloromethyl)pyridine hydrochloride 39741-46-3
Price: US $0.10/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000 tons
Release date: 2019-12-30

Career Henan Chemical Co

Product: 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE 39741-46-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-18

39741-46-3, 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDERelated Search:

Chloropyramine hydrochloride Pyridine hydrochloride

3-Bromo-5-(chloromethyl)pyridine hydrochloride 95%

3-Bromo-5-(chloromethyl)pyridine hydrochloride 95+%

5-Bromo-3-(chloromethyl)pyridine hydrochloride

Pyridine, 3-bromo-5-(chloromethyl)-, hydrochloride (1:1)

3-bromo-5-(chloromethyl)-Pyridine hydrochloride (1:1)

39741-46-3

C6H5BrClNClH

Heterocycle-Pyridine series