M-AMINOBENZYL CYANIDE
- Product Name
- M-AMINOBENZYL CYANIDE
- CAS No.
- 4623-24-9
- Chemical Name
- M-AMINOBENZYL CYANIDE
- Synonyms
- 2-(3-Aminophenyl)acetonitrile;2-(3-Aminophenyl);3-AMINOBENZYL CYANIDE;M-AMINOBENZYL CYANIDE;3-(Cyanomethyl)aniline;m-Aminophenylacetonitrile;3-AMino-benzeneacetonitrile;Benzeneacetonitrile, 3-amino-
- CBNumber
- CB2128207
- Molecular Formula
- C8H8N2
- Formula Weight
- 132.16
- MOL File
- 4623-24-9.mol
M-AMINOBENZYL CYANIDE Property
- Melting point:
- 137-138 °C
- Boiling point:
- 183-187 °C(Press: 13 Torr)
- Density
- 1.120±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 4.12±0.10(Predicted)
- Appearance
- Yellow to brown Liquid
Safety
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 299519
- Product name
- 2-(3-Aminophenyl)acetonitrile
- Packaging
- 250.00mg
- Price
- $38
- Updated
- 2026/05/19
- Product number
- 299519
- Product name
- 2-(3-Aminophenyl)acetonitrile
- Packaging
- 1.00g
- Price
- $86
- Updated
- 2026/05/19
- Product number
- 299519
- Product name
- 2-(3-Aminophenyl)acetonitrile
- Packaging
- 5.00g
- Price
- $269
- Updated
- 2026/05/19
- Product number
- A48787
- Product name
- 2-(3-Aminophenyl)acetonitrile
- Purity
- 96%
- Packaging
- 100mg
- Price
- $36
- Updated
- 2026/05/06
- Product number
- A48787
- Product name
- 2-(3-Aminophenyl)acetonitrile
- Purity
- 96%
- Packaging
- 250mg
- Price
- $42
- Updated
- 2026/05/06
M-AMINOBENZYL CYANIDE Chemical Properties,Usage,Production
Uses
2-(3-Aminophenyl)acetonitrile is a useful reagent in the synthesis of aminophenylalkylaminopyrrolopyrimidines with antiinfluenza activity.
Synthesis
621-50-1
4623-24-9
GENERAL METHOD: To a solution of m-nitrobenzeneacetonitrile (150.1 mg, 0.66 mmol) and ammonium chloride (NH4Cl, 183.6 mg, 3.43 mmol) in a solvent mixture of ethanol/water (EtOH/H2O, 5:1, 6 mL) was added powdered iron (Fe, 184.4 mg, 3.30 mmol) and vigorously stirred for 1 hour at 85 °C. . After completion of the reaction, the mixture was cooled to room temperature and filtered through a diatomaceous earth pad to remove solid impurities. The filtrate was concentrated and the residue was purified by column chromatography (eluent: ethyl acetate/hexane, 20:70) to afford 2-(3-aminophenyl)acetonitrile (10a, 99.2 mg, 76% yield) as a brown oil.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2018, vol. 28, # 4, p. 577 - 583
[2] Patent: US2015/175557, 2015, A1. Location in patent: Paragraph 0347
[3] Patent: CN107098786, 2017, A. Location in patent: Paragraph 0049-0050
[4] Patent: WO2011/47156, 2011, A1. Location in patent: Page/Page column 82
[5] Patent: WO2009/122180, 2009, A1. Location in patent: Page/Page column 95
M-AMINOBENZYL CYANIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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