ChemicalBook > CAS DataBase List > M-AMINOBENZYL CYANIDE

M-AMINOBENZYL CYANIDE

Product Name
M-AMINOBENZYL CYANIDE
CAS No.
4623-24-9
Chemical Name
M-AMINOBENZYL CYANIDE
Synonyms
2-(3-Aminophenyl);M-AMINOBENZYL CYANIDE;3-AMINOBENZYL CYANIDE;3-(Cyanomethyl)aniline;m-Aminophenylacetonitrile;3-AMino-benzeneacetonitrile;Benzeneacetonitrile, 3-amino-;2-(3-Aminophenyl)acetonitrile
CBNumber
CB2128207
Molecular Formula
C8H8N2
Formula Weight
132.16
MOL File
4623-24-9.mol
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M-AMINOBENZYL CYANIDE Property

Melting point:
137-138 °C
Boiling point:
183-187 °C(Press: 13 Torr)
Density 
1.120±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
4.12±0.10(Predicted)
Appearance
Yellow to brown Liquid
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Safety

HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A638080
Product name
2-(3-Aminophenyl)acetonitrile
Packaging
500mg
Price
$110
Updated
2021/12/16
TRC
Product number
A638080
Product name
2-(3-Aminophenyl)acetonitrile
Packaging
100mg
Price
$60
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0093740
Product name
(3-AMINOPHENYL)-ACETONITRILE
Purity
95.00%
Packaging
1G
Price
$909.56
Updated
2021/12/16
AK Scientific
Product number
Z4772
Product name
2-(3-Aminophenyl)acetonitrile
Packaging
25g
Price
$1331
Updated
2021/12/16
J&W Pharmlab
Product number
20R0416
Product name
(3-Amino-phenyl)-acetonitrile
Purity
96%
Packaging
1g
Price
$80
Updated
2021/12/16
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M-AMINOBENZYL CYANIDE Chemical Properties,Usage,Production

Uses

2-(3-Aminophenyl)acetonitrile is a useful reagent in the synthesis of aminophenylalkylaminopyrrolopyrimidines with antiinfluenza activity.

Synthesis

621-50-1

4623-24-9

GENERAL METHOD: To a solution of m-nitrobenzeneacetonitrile (150.1 mg, 0.66 mmol) and ammonium chloride (NH4Cl, 183.6 mg, 3.43 mmol) in a solvent mixture of ethanol/water (EtOH/H2O, 5:1, 6 mL) was added powdered iron (Fe, 184.4 mg, 3.30 mmol) and vigorously stirred for 1 hour at 85 °C. . After completion of the reaction, the mixture was cooled to room temperature and filtered through a diatomaceous earth pad to remove solid impurities. The filtrate was concentrated and the residue was purified by column chromatography (eluent: ethyl acetate/hexane, 20:70) to afford 2-(3-aminophenyl)acetonitrile (10a, 99.2 mg, 76% yield) as a brown oil.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2018, vol. 28, # 4, p. 577 - 583
[2] Patent: US2015/175557, 2015, A1. Location in patent: Paragraph 0347
[3] Patent: CN107098786, 2017, A. Location in patent: Paragraph 0049-0050
[4] Patent: WO2011/47156, 2011, A1. Location in patent: Page/Page column 82
[5] Patent: WO2009/122180, 2009, A1. Location in patent: Page/Page column 95

M-AMINOBENZYL CYANIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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M-AMINOBENZYL CYANIDE Suppliers

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4623-24-9, M-AMINOBENZYL CYANIDERelated Search:

ALPHA-AMINOBENZYL CYANIDE HYDROCHLORIDE,à-aminobenzyl cyanide hydrochloride,α-aminobenzyl cyanide hydrochloride o-Aminobenzyl cyanide,2-AMINOBENZYL CYANIDE / 2-AMINOPHENYLACETONITRILE,2-AMINOBENZYL CYANIDE 4-AMINOBENZYL CYANIDE,P-AMINOBENZYL CYANIDE,4-AMINOBENZYL CYANIDE / 4-AMINOPHENYLACETONITRILE 2-METHYL-3-NITROBENZYL CYANIDE 3-NITROPHENYLACETONITRILE (S)-10-(Cyanomethyl)-9-fluoro-2,3-dihydro-3-methyl-7-oxo-7H-pyrido[1,2,3-de]-1,4-benzoxazine-6-carboxylic acid ALPHA-AMINOBENZYL CYANIDE HYDROCHLORIDE,alpha-Aminobenzyl cyanide hydrochloride~alpha-Aminophenylacetonitrile hydrochloride (4-FLUORO-3-NITROPHENYL)ACETONITRILE Benzeneacetonitrile, 5-amino-2-fluoro- (9CI) 2-Fluoro-5-nitrophenylacetonitrile M-AMINOBENZYL CYANIDE 4-CHLORO-3-NITROPHENYLACETONITRILE 2-(2-METHYL-5-NITROPHENYL)ACETONITRILE (3-CYANOMETHYL-PHENYL)-CARBAMIC ACID TERT-BUTYL ESTER AKOS 91783 2-(4-METHYL-3-NITROPHENYL)ACETONITRILE 2-(3-(dimethylamino)phenyl)acetonitrile [3-(2,5-DIOXO-1-PYRROLIDINYL)PHENYL]ACETONITRILE

  • M-AMINOBENZYL CYANIDE
  • 2-(3-Aminophenyl)
  • 3-AMINOBENZYL CYANIDE
  • 2-(3-Aminophenyl)acetonitrile
  • 3-AMino-benzeneacetonitrile
  • m-Aminophenylacetonitrile
  • 3-(Cyanomethyl)aniline
  • Benzeneacetonitrile, 3-amino-
  • 4623-24-9