1-Iodo-3,5-dimethylbenzene

ChemicalBook > CAS DataBase List > 1-Iodo-3,5-dimethylbenzene

1-Iodo-3,5-dimethylbenzene

Product Name: 1-Iodo-3,5-dimethylbenzene
CAS No.: 22445-41-6
Chemical Name: 1-Iodo-3,5-dimethylbenzene
Synonyms: 5-IODO-M-XYLENE;5-Iodo-m-xylene,99%;1-Iodo-3,5-dimethyL;3,5-DIMETHYLIODOBENZENE;3,5-Dinethyliodobenzene;3,5-dimethylphenyl iodide;5-Iodo-M-xylene, 99% 25ML;3,5-diMethyl-1-iodobenzene;1-IODO-3,5-DIMETHYLBENZENE;1,3-DIMETHYL-5-IODOBENZENE
CBNumber: CB2135658
Molecular Formula: C8H9I
Formula Weight: 232.06
MOL File: 22445-41-6.mol

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1-Iodo-3,5-dimethylbenzene Property

Melting point:: -2.9°C (estimate)
Boiling point:: 92-94 °C3 mm Hg(lit.)
Density: 1.608 g/mL at 25 °C(lit.)
refractive index: n20/D 1.594(lit.)
Flash point:: >230 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: Sparingly soluble (0.014 g/L) (25°C), Calc.
form: Liquid
Specific Gravity: 1.608
color: Clear light yellow
Sensitive: Light Sensitive
BRN: 2039353
InChIKey: ZLMKEENUYIUKKC-UHFFFAOYSA-N
CAS DataBase Reference: 22445-41-6(CAS DataBase Reference)
NIST Chemistry Reference: Benzene, 1-iodo-3,5-dimethyl-(22445-41-6)

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Safety

Hazard Codes: Xi,C
Risk Statements: 36/37/38
Safety Statements: 26-36-37/39
WGK Germany: 3
Hazard Note: Irritant
HS Code: 29039990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 392510
Product name: 1-Iodo-3,5-dimethylbenzene
Purity: 99%
Packaging: 5ml
Price: $23.96
Updated: 2024/03/01

Sigma-Aldrich

Product number: 392510
Product name: 1-Iodo-3,5-dimethylbenzene
Purity: 99%
Packaging: 25ml
Price: $77.4
Updated: 2024/03/01

TCI Chemical

Product number: I0548
Product name: 5-Iodo-m-xylene
Packaging: 5G
Price: $60
Updated: 2024/03/01

TCI Chemical

Product number: I0548
Product name: 5-Iodo-m-xylene
Packaging: 25G
Price: $180
Updated: 2024/03/01

Alfa Aesar

Product number: A18413
Product name: 5-Iodo-m-xylene, 97%
Packaging: 10g
Price: $46.65
Updated: 2024/03/01

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1-Iodo-3,5-dimethylbenzene Chemical Properties,Usage,Production

Chemical Properties

clear light yellow liquid

Uses

suzuki reaction

Uses

1-Iodo-3,5-dimethylbenzene (5-iodo-m-xylene) is suitable for use in the synthesis of N-(3,5-xylyl)-N-ethyl aniline, an aryl amine, It is also used in the following studies; α-Arylation of ketones, Copper-catalyzed N-arylation of imidazoles, Cyanation of 5-iodo-m-xylene to form 3,5-dimethylbenzonitrile, synthesis of 1,3-Dimethyl-5-phenoxybenzene by nano-CuFe2O4 catalyzed C-O cross-coupling with phenol, CuBr-catalyzed amination of 1-iodo-3,5-dimethylbenzene to form N-Allyl-3,5-dimethylbenzenamine, copper-catalyzed C-S bond-formation between 5-iodo-m-xylene and thiophenol. It is also employed as a starting material in the synthesis of biphenyl-3,3?,5,5?-tetracarboxylic acid, radical bromination of 5-iodo-m-xylene by N-bromosuccinimide to form 1,3-bis(bromomethyl)-5-iodobenzene.

Uses

1-Iodo-3,5-dimethylbenzene (5-iodo-m-xylene) is suitable for use in the synthesis of N-(3,5-xylyl)-N-ethylaniline, an arylamine.
It may be used in the following studies:

α-Arylation of ketones.
Copper-catalyzed N-arylation of imidazoles.
Cyanation of 5-iodo-m-xylene to form 3,5-dimethylbenzonitrile.
Synthesis of 1,3-Dimethyl-5-phenoxybenzene by nano-CuFe₂O₄ catalyzed C-O cross-coupling with phenol.
CuBr-catalyzed amination of 1-iodo-3,5-dimethylbenzene to form N-Allyl-3,5-dimethylbenzenamine.
Copper-catalyzed C-S bond-formation between 5-iodo-m-xylene and thiophenol.
As a starting material in the synthesis of biphenyl-3,3′,5,5′-tetracarboxylic acid.
Radical bromination of 5-iodo-m-xylene by N-bromosuccinimide to form 1,3-bis(bromomethyl)-5-iodobenzene.

General Description

1-Iodo-3,5-dimethylbenzene (5-Iodo-m-xylene) is an aryl halide. It can be obtained from 5-bromo-m-xylene, via copper-catalyzed halogen exchange reaction, in the presence of NaI or KI in n-BuOH or DMF (solvents). It undergoes reaction with phenol in the presence of CuFe₂O₄nano powder as a recyclable catalyst to afford 1,3-dimethyl-5-phenoxybenzene.

1-Iodo-3,5-dimethylbenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-Iodo-3,5-dimethylbenzene manufacturers

Speranza Chemical Co., Ltd.

Product: 1-iodo-3,5-dimethylbenzene 22445-41-6
Price: US $460.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 300MT/year
Release date: 2019-12-24

Henan Fengda Chemical Co., Ltd

Product: 1-Iodo-3,5-dimethylbenzene 22445-41-6
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-24

Hebei Mojin Biotechnology Co., Ltd

Product: 1-Iodo-3,5-dimethylbenzene 22445-41-6
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-07-28

22445-41-6, 1-Iodo-3,5-dimethylbenzeneRelated Search:

Poly(dimethylsiloxane) 1,4-Diiodobenzene 1,3-Dimethylbarbituric acid 1,2-Diiodobenzene Xylene (Diacetoxyiodo)benzene Dimethyl sulfoxide m-Xylene Musk xylene N,N-Dimethylformamide 3,5-BIS(TRIFLUOROMETHYL)IODOBENZENE PENTAMETHYLIODOBENZENE 1-IODO-2,3,4,5-TETRAMETHYLBENZENE 2,3,5,6-Tetramethyliodobenzene DIMETHYL 5-IODOISOPHTHALATE 1-IODO-2,4-DIMETHYLBENZENE,4-IODO-1,3-DIMETHYLBENZENE 2,6-DIMETHYL-4-IODOPHENOL OTAVA-BB BB7018670077

3,5-dimethylphenyl iodide

1,3-DIMETHYL-5-IODOBENZENE

1-IODO-3,5-DIMETHYLBENZENE

3,5-DIMETHYLIODOBENZENE

5-IODO-M-XYLENE

5-Iodo-m-xylene (stabilized with Copper chip)

5-Iodo-m-xylene,99%

Benzene, 1-Iodo-3,5-dimethyl-

4-Iodo-3,5-dimethylbenzoic acidamide

1,3-Dimethyl-5-iodobenzene, 5-Iodo-m-xylene

3,5-diMethyl-1-iodobenzene

5-Iodo-M-xylene, 99% 25ML

3,5-Dimethyliodobenzene 1-Iodo-3,5-dimethylbenzene

1-Iodo-3,5-dimethylbenzene 99%

3,5-Dinethyliodobenzene

5-Iodo-m-xylene(stabilizedwithCopperchip)&gt

1-Iodo-3,5-dimethyL

1-Iodo-3,5-dimethylbenzene ISO 9001：2015 REACH

22445-41-6

CH32C6H3I

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