9,9-Dimethylfluorene
- Product Name
- 9,9-Dimethylfluorene
- CAS No.
- 4569-45-3
- Chemical Name
- 9,9-Dimethylfluorene
- Synonyms
- 9,9-DIMETHYLFLUORENE;9H-Fluorene, 9,9-dimethyl-;9,9-Dimethyl-9H-fluo;9,9'-Dimethylfluorenee;9,9- two Methylfluorene;9,9-dimethyl-fluororene;9,9-Dimethylfluorene>9,9-Dimethyl-9H-fluoren;9,9-Dimethyl-9H-fluorene;9,9-DiMethyl-9H-fluoreneV
- CBNumber
- CB2146845
- Molecular Formula
- C15H14
- Formula Weight
- 194.27
- MOL File
- 4569-45-3.mol
9,9-Dimethylfluorene Property
- Melting point:
- 96°C
- Boiling point:
- 287 °C
- Density
- 1.040±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Almost white
- λmax
- 301nm(EtOH)(lit.)
- InChIKey
- ZHQNDEHZACHHTA-UHFFFAOYSA-N
- CAS DataBase Reference
- 4569-45-3(CAS DataBase Reference)
- NIST Chemistry Reference
- 9H-Fluorene, 9,9-dimethyl-(4569-45-3)
Safety
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 26-37/39
- HS Code
- 2902.90.9000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- D3235
- Product name
- 9,9-Dimethylfluorene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $67
- Updated
- 2024/03/01
- Product number
- D3235
- Product name
- 9,9-Dimethylfluorene
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $196
- Updated
- 2024/03/01
- Product number
- D3810
- Product name
- 9,9-Dimethylfluorene (purified by sublimation)
- Purity
- >99.0%(GC)
- Packaging
- 1g
- Price
- $112
- Updated
- 2024/03/01
- Product number
- D477768
- Product name
- 9,9-Dimethyl-9H-fluorene
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FD62946
- Product name
- 9,9-Dimethylfluorene (purified by sublimation)
- Packaging
- 2g
- Price
- $50
- Updated
- 2021/12/16
9,9-Dimethylfluorene Chemical Properties,Usage,Production
Definition
9,9-Dimethylfluorene is an organic electroluminescent material intermediate. The fluorene derivative is a kind of organic electroluminescent material commercialized at present, wherein 9, 9-dimethyl fluorene is an essential intermediate for synthesizing OLED material.
Synthesis
The method comprises taking dimethyl carbonate as a methylating agent under alkaline substances and reacting with fluorene in an organic solvent system within a certain temperature range to prepare the 9,9-Dimethylfluorene. The method uses dimethyl carbonate as a methylating agent so that the reaction process is stabilized and the economy is greatly improved; meanwhile, the use of dimethyl carbonate avoids the use of low-boiling-point hypertoxic such as methyl iodide, methyl bromide, and the like, is environment-friendly, and the generated wastewater has single component and is convenient to treat.
9,9-Dimethylfluorene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9,9-Dimethylfluorene manufacturers
- Product
- 9,9-Dimethylfluorene 4569-45-3
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30
- Product
- 9,9-Dimethyl-9H-fluorene 4569-45-3
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 5000 Ton
- Release date
- 2022-10-20
- Product
- 9,9-Dimethyl-9H-fluorene 4569-45-3
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 50000KG/month
- Release date
- 2023-07-28