N-Methyl-1-amino-hex-5-ene
- Product Name
- N-Methyl-1-amino-hex-5-ene
- CAS No.
- 55863-02-0
- Chemical Name
- N-Methyl-1-amino-hex-5-ene
- Synonyms
- N-methyl-5-hexen-1-amine;N-methylhex-5-en-1-amine;N-Methyl-1-amino-hex-5-ene;5-HEXEN-1-AMINE, N-METHYL-;5-Hexen-1-aMine, N-Methyl-N-Methylhex-5-en-1-aMine;N-Methylhex-5-en-1-amine,98% (stabilized with MEHQ)
- CBNumber
- CB21856543
- Molecular Formula
- C7H15N
- Formula Weight
- 113.2
- MOL File
- 55863-02-0.mol
N-Methyl-1-amino-hex-5-ene Property
- Boiling point:
- 146.5±19.0 °C(Predicted)
- Density
- 0.764±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- pka
- 10.74±0.10(Predicted)
- form
- Oil
- color
- Colourless
- Stability:
- Volatile
- InChI
- InChI=1S/C7H15N/c1-3-4-5-6-7-8-2/h3,8H,1,4-7H2,2H3
- InChIKey
- KKIMETYRXLWWSD-UHFFFAOYSA-N
- SMILES
- C(NC)CCCC=C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
H413May cause long lasting harmful effects to aquatic life
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P337+P313IF eye irritation persists: Get medical advice/attention.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M312090
- Product name
- N-Methylhex-5-en-1-amine
- Packaging
- 25g
- Price
- $1485
- Updated
- 2021/12/16
- Product number
- 47491
- Product name
- N-Methylhex-5-en-1-amine
- Packaging
- 1g
- Price
- $610
- Updated
- 2021/12/16
- Product number
- 8160AB
- Product name
- N-Methylhex-5-en-1-amine
- Packaging
- 5g
- Price
- $718
- Updated
- 2021/12/16
- Product number
- CHM0385192
- Product name
- N-METHYL-1-AMINO-HEX-5-ENE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.07
- Updated
- 2021/12/16
- Product number
- A812097
- Product name
- N-Methylhex-5-en-1-amine
- Purity
- 95%
- Packaging
- 10g
- Price
- $556
- Updated
- 2021/12/16
N-Methyl-1-amino-hex-5-ene Chemical Properties,Usage,Production
Uses
N-Methylhex-5-en-1-amine can be used as a reagent to prepare quinazoline substituted cyclopentane and proline-urea based macrocycles as Hepatitis C virus (HCV) NS3/4A protease inhibitors.
Synthesis
2695-47-8
74-89-5
55863-02-0
The following step: To a reaction flask was added a methanol solution containing 25% methylamine in an amount of 10 equivalents of methylamine. Subsequently 1 equivalent of 6-bromo-1-hexene was added to the reaction flask and mixed with stirring. The reaction mixture was heated to 40°C in an oil bath and kept at this temperature for 3 hours. Upon completion of the reaction, the mixture was cooled to 20 °C and 0.1 equivalent of p-methoxyphenol was added as a stabilizer, along with 1 equivalent of sodium hydroxide. The excess methylamine methanol solution was recovered under negative pressure. Next, the mixture was heated to 50 °C and a colorless liquid product, N-methyl-5-hexen-1-amine, was obtained by distillation under reduced pressure. The yield of this step was 67% and the purity of the product was 96.5%.
References
[1] Patent: CN108003037, 2018, A. Location in patent: Paragraph 0014-0028
[2] Bulletin de la Societe Chimique de France, 1975, p. 2315 - 2320
N-Methyl-1-amino-hex-5-ene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-Methyl-1-amino-hex-5-ene manufacturers
- Product
- N-Methyl-1-amino-hex-5-ene 55863-02-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-07-07
- Product
- N-Methyl-5-hexen-1-amine 55863-02-0
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 50kg
- Release date
- 2025-06-24
- Product
- N-Methylhex-5-en-1-amine 55863-02-0
- Price
- US $590.00/g
- Min. Order
- 1g
- Purity
- 95
- Supply Ability
- 500 Kg
- Release date
- 2024-02-11