ChemicalBook > CAS DataBase List > 3-(Acetylamino)-5-bromopyridine

3-(Acetylamino)-5-bromopyridine

Product Name
3-(Acetylamino)-5-bromopyridine
CAS No.
15862-46-1
Chemical Name
3-(Acetylamino)-5-bromopyridine
Synonyms
N-(5-Bromopyridin-3-yl);N-(5-Bromo-3-pyridyl)acetamide;3-(Acetylamino)-5-bromopyridine;N-(5-bromopyridin-3-yl)acetamide;Acetamide, N-(5-bromo-3-pyridinyl)-
CBNumber
CB22194679
Molecular Formula
C7H7BrN2O
Formula Weight
215.05
MOL File
15862-46-1.mol
More
Less

3-(Acetylamino)-5-bromopyridine Property

storage temp. 
Inert atmosphere,Room Temperature
Appearance
Light yellow to brown Solid
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TRC
Product number
B704203
Product name
N-(5-Bromopyridin-3-yl)acetamide
Packaging
10mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0369737
Product name
N-(5-BROMOPYRIDIN-3-YL)ACETAMIDE
Purity
95.00%
Packaging
5MG
Price
$502.67
Updated
2021/12/16
AK Scientific
Product number
2727AQ
Product name
N-(5-BROMOPYRIDIN-3-YL)ACETAMIDE
Packaging
1g
Price
$503.6
Updated
2021/12/16
Chemenu
Product number
CM173276
Product name
N-(5-bromopyridin-3-yl)acetamide
Purity
95%
Packaging
5g
Price
$707
Updated
2021/12/16
Crysdot
Product number
CD11245962
Product name
N-(5-Bromopyridin-3-yl)acetamide
Purity
95+%
Packaging
5g
Price
$756
Updated
2021/12/16
More
Less

3-(Acetylamino)-5-bromopyridine Chemical Properties,Usage,Production

Synthesis

13535-01-8

108-24-7

15862-46-1

To a solution of 3-amino-5-bromopyridine (1.0 g, 5.78 mmol) and pyridine (1.3 mL, 12.9 mmol) in dichloromethane (DCM, 5 mL) was added acetic anhydride (0.6 mL, 6.358 mmol) dropwise. The reaction mixture was stirred at room temperature for 17 hours. Upon completion of the reaction, the mixture was concentrated and the crude product was purified by normal-phase column chromatography with an elution gradient of 0-75% ethyl acetate (EtOAc)/heptane to afford N-(5-bromopyridin-3-yl)acetamide (1.18 g, 95% yield).

References

[1] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014, vol. 53, # 1, p. 83 - 89
[2] Patent: US2014/323468, 2014, A1. Location in patent: Paragraph 0601
[3] Patent: CN103601745, 2017, B. Location in patent: Paragraph 0035; 0036
[4] Recueil des Travaux Chimiques des Pays-Bas, 1955, vol. 74, p. 1062,1068
[5] Journal fuer Praktische Chemie (Leipzig), 1933, vol. <2> 138, p. 244,257

3-(Acetylamino)-5-bromopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

3-(Acetylamino)-5-bromopyridine Suppliers

Tetranov Biopharm
Tel
13526569071
Email
sales@leadmedpharm.com
Country
China
ProdList
7892
Advantage
64
shanghai Rainbow MediTech.Co.Ltd.
Tel
021-64968085,64968086-5815,5812; 13472757003
Fax
+86 21 64968087
Email
xiaoxia.zeng@rainbowpharma.cn
Country
China
ProdList
961
Advantage
65
Cantotech Chemicals, Ltd.
Tel
86-0755-86635001
Fax
86-0755-22642228
Email
cantotech@126.com
Country
China
ProdList
4566
Advantage
55
Zhengzhou TRIZ Pharmaceutical Technology Co., Ltd.
Tel
19943855286
Fax
0371-53392065
Email
triz-4@trizpharma.cn
Country
China
ProdList
1936
Advantage
56
Changsha Luxing Bio-Chem Technology Co., Ltd.
Tel
0731-88827538 15873153880
Fax
0731-88827238
Email
luxingbc@126.com
Country
China
ProdList
1999
Advantage
65
SuZhou ShiYa Biopharmaceuticals, Inc.
Tel
0512-0512-52358471 17715136450
Fax
05125235 6881
Email
sales@shiyabiopharm.com
Country
China
ProdList
12127
Advantage
58
Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
Advantage
60
Chengdu Xiaojia Technology Co., Ltd.
Tel
15902830537
Email
zhanghao@happysyn.com
Country
China
ProdList
3180
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Sichuan BaiPeng Biotechnology Co., Ltd.
Tel
028-65791793 18140026355
Fax
QQ568470422
Email
568470422@qq.com
Country
China
ProdList
9997
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-(0)57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Aikon International Limited
Tel
025-58859352 18068836627
Fax
(5)02557626880
Email
dt3@aikonchem.com
Country
China
ProdList
15493
Advantage
58
Henan Alfachem Co.,Ltd.
Tel
0371-55051623 18137891487
Fax
QQ:2853979817
Email
2853979817@qq.com
Country
China
ProdList
9981
Advantage
58
Hefei TNJ Chemical Industry Co.,Ltd.
Tel
+86-0551-65418671 +8618949823763
Fax
0551-65418697
Email
sales@tnjchem.com
Country
China
ProdList
34563
Advantage
58
LEADMEDPHARM CO.,LTD
Tel
13674959855 13674959855
Email
sales@synthontech.com
Country
China
ProdList
3035
Advantage
58
Accela ChemBio Co.,Ltd.
Tel
021-50795510 4000665055
Email
sales@accelachem.com
Country
China
ProdList
10467
Advantage
58
Changzhou Kechem Bio-Scientific Co., LTD.
Tel
0519-68985668 13685222090
Fax
qq735434464
Email
sales@kechem.cn
Country
China
ProdList
26028
Advantage
58
Shanghai Fine Biotech Co.,Ltd
Tel
18717800556
Email
sales@finebiotech.com
Country
China
ProdList
2182
Advantage
58
Energy Chemical
Tel
021-58432009 400-005-6266
Fax
021-58436166
Email
marketing@energy-chemical.com
Country
China
ProdList
44918
Advantage
58
Shanghai Haohong Pharmaceutical Co., Ltd.
Tel
400-8210725 4008210725
Email
malulu@leyan.com
Country
China
ProdList
40000
Advantage
58
Hefei Mokai Pharmaceutical Technology Co., Ltd
Tel
18130062233
Email
3362556465@qq.com
Country
China
ProdList
8100
Advantage
58
PharmaBlock Sciences (Nanjing), Inc.
Tel
4000255188
Fax
025 86918232
Email
sales_china@pharmablock.com
Country
China
ProdList
10000
Advantage
58
Bide Pharmatech Ltd.
Tel
400-1647117 13681763483
Email
product02@bidepharm.com
Country
China
ProdList
59936
Advantage
58
Bide Pharmatech Ltd.
Tel
400-6005915
Email
sales@picasso-e.com
Country
China
ProdList
39653
Advantage
58
Qingzhou dafeng import and export Co. LTD
Tel
16773308882
Email
927608786@qq.com
Country
China
ProdList
3051
Advantage
58
Beijing InnoChem Science & Technology Co., Ltd.
Tel
15652467323
Email
sales@inno-chem.com.cn
Country
China
ProdList
8293
Advantage
58
Henan Dobe Chemical Co. , Ltd.
Tel
0370-6999054 17550096163
Email
3189729795@qq.com
Country
China
ProdList
7172
Advantage
58
Shanghai Yanbang Pharmaceutical Technology Co., Ltd
Tel
15618536883
Email
1228181347@qq.com
Country
China
ProdList
7951
Advantage
58
Beijing Solarbio Science & Tecnology Co., Ltd.
Tel
010-50973130 17801761073
Email
Gsiyu@solarbio.com
Country
China
ProdList
50464
Advantage
58
PharmaBlock Sciences (Nanjing), Inc.
Tel
4000255188
Email
marketing@pharmablock.com
Country
China
ProdList
9126
Advantage
58
Zhuhai Aobokai Biomedical Technology Co., Ltd.
Tel
400-0628126 18736790110;
Email
sales-team@aobchem.com.cn
Country
China
ProdList
50000
Advantage
58
https://hanhongsci.com/
Tel
021-54306202 18917919676
Email
info@hanhongsci.com
Country
China
ProdList
29995
Advantage
58
Jilin Chinese Academy of Sciences-yanshen Technology
Tel
18143011203
Email
ET-market@chemextension.com
Country
China
ProdList
32048
Advantage
58
Shanghai Ken chemical Technology Co.,ltd
Tel
02152215958
Email
47697177@qq.com
Country
China
ProdList
10011
Advantage
58
Ningbo Chaoming Biotechnology Co., Ltd
Tel
13301662590
Email
mandy@atkchemical.com
Country
China
ProdList
9343
Advantage
58
Suzhou ARTK Medchem Co., Ltd.
Tel
+86-512-68323658 +86-18168183658
Email
sales1@artkmedchem.com
Country
China
ProdList
39002
Advantage
58
Jilin Chinese Academy of Sciences-yanshen Technology
Tel
+undefined18143011203
Email
info@chemextension.com
Country
China
ProdList
42056
Advantage
58
Guangzhou Aoz Biotechnology Co., Ltd.
Tel
18022383332
Country
CHINA
ProdList
0
Advantage
58