(4-CHLORO-BENZYL)-METHYL-AMINE

Product Name: (4-CHLORO-BENZYL)-METHYL-AMINE
CAS No.: 104-11-0
Chemical Name: (4-CHLORO-BENZYL)-METHYL-AMINE
Synonyms: AKOS BC-2745;TIMTEC-BB SBB010371;(4-CHLORO-BENZYL)-ME;4-Chloro-N-methylbenzylamine;N-Methyl-4-chlorobenzylamine;P-CHLORO-N-METHYLBENZYLAMINE;N-METHYL-P-CHLOROBENZYLAMINE;(4-CHLORO-BENZYL)-METHYL-AMINE;-(4-CHLOROBENZYL)-N-METHYLAMINE;4-Chloro-N-methylbenzylamine>
CBNumber: CB4358253
Molecular Formula: C8H10ClN
Formula Weight: 155.62
MOL File: 104-11-0.mol

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(4-CHLORO-BENZYL)-METHYL-AMINE Property

Boiling point:: 77 °C
Density: 1.088±0.06 g/cm3(Predicted)
refractive index: 1.5380 to 1.5420
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: clear liquid
pka: 9.50±0.10(Predicted)
color: Colorless to Light yellow to Light orange
EPA Substance Registry System: Benzenemethanamine, 4-chloro-N-methyl- (104-11-0)

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Safety

Hazard Codes: Xi,C,Xn
Risk Statements: 22-34-52-41-37/38
Safety Statements: 23-26-36/37/39-45-39
RIDADR: 2735
TSCA: Yes
HazardClass: 8
HazardClass: IRRITANT
PackingGroup: Ⅲ
HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical

Product number: C2885
Product name: 4-Chloro-N-methylbenzylamine
Purity: >97.0%(GC)(T)
Packaging: 1g
Price: $50
Updated: 2025/07/31

TCI Chemical

Product number: C2885
Product name: 4-Chloro-N-methylbenzylamine
Purity: >97.0%(GC)(T)
Packaging: 5g
Price: $201
Updated: 2025/07/31

Apolloscientific

Product number: OR16428
Product name: 4-Chloro-N-methylbenzylamine
Packaging: 1g
Price: $29
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3731-5-X1
Product name: 4-Chloro-N-methylbenzylamine
Packaging: 1g
Price: $32
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC134347
Product name: (4-Chlorobenzyl)methylamine
Packaging: 500mg
Price: $50
Updated: 2021/12/16

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(4-CHLORO-BENZYL)-METHYL-AMINE Chemical Properties,Usage,Production

Definition

ChEBI: N-(4-chlorobenzyl)-N-methylamine is an aromatic amine.

Synthesis

104-83-6

74-89-5

104-11-0

General procedure for the synthesis of N-(4-chlorobenzyl)-N-methylamine from 4-chlorobenzyl chloride and monomethylamine: an aqueous solution of methylamine (40% v/v, 9.03 ml, 93.48 mmol) was slowly added to a stirred tetrahydrofuran (THF, 300 ml) solution of 4-chlorobenzyl chloride (3.00 g, 18.63 mmol) under nitrogen protection and at 0 °C. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the solvent was removed by rotary evaporation and residual water was removed by azeotropy with toluene. The crude product was purified directly by column chromatography, first using ethyl acetate (100%) as eluent, followed by a solvent mixture of ethyl acetate: methanol: triethylamine (92:5:3) as eluent, to afford the target compound, N-(4-chlorobenzyl)-N-methylamine (30), as a yellow oil (2.49 g, 81% yield). The structure of the product was determined by NMR hydrogen spectrum (1H NMR, CDCl3, 300 MHz) δ 7.25-7.18 (4H, m), 3.66 (2H, s), 2.38 (3H, s), 1.65 (1H, s); NMR carbon spectrum (13C NMR, CDCl3, 100 MHz) δ 138.6, 132.6, 129.5 (2C ), 128.4 (2C), 55.2, 35.8; high-resolution mass spectrometry (HRMS, ESI): measured value 156.0580 (M+), theoretical value of 156.0556 for C8H10NCl (M+).

References

[1] Patent: WO2010/18555, 2010, A2. Location in patent: Page/Page column 19; 23
[2] European Journal of Medicinal Chemistry, 2011, vol. 46, # 5, p. 1729 - 1742
[3] Justus Liebigs Annalen der Chemie, 1926, vol. 449, p. 264
[4] Journal of Medicinal Chemistry, 1983, vol. 26, # 3, p. 309 - 312
[5] Bioorganic and Medicinal Chemistry, 2009, vol. 17, # 13, p. 4693 - 4707

(4-CHLORO-BENZYL)-METHYL-AMINE Preparation Products And Raw materials

Raw materials

4-Chlorobenzaldehyde Sodium sulfate Methylamine Sodium borohydride Dichloromethane Methanol

Preparation Products

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(4-CHLORO-BENZYL)-METHYL-AMINE Suppliers

Americas 1 Belgium 1 China 108 Europe 1 Germany 3 India 2 Japan 1 Russia 1 Switzerland 1 Ukraine 1 United Kingdom 4 United States 19 Global 143

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View Lastest Price from (4-CHLORO-BENZYL)-METHYL-AMINE manufacturers

Career Henan Chemical Co

Product: (4-CHLORO-BENZYL)-METHYL-AMINE 104-11-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 25kg
Release date: 2019-07-12

104-11-0, (4-CHLORO-BENZYL)-METHYL-AMINERelated Search:

(4-CHLORO-BENZYL)-METHYL-AMINE 1-(4-Chlorobenzhydryl)piperazine (3,4-Dichlorobenzyl)methylamine Tecloftalam CHLORCYCLIZINE HYDROCHLORIDE Tetrachlorophthalimide (2-CHLORO-BENZYL)-METHYL-AMINE 4-Chlorobenzylamine BENZAMIDE, 4-CHLORO-N-(2-METHYLPHENYL)- 2-CHLORO-N-(4-CHLOROBENZYL)ACETAMIDE 4-CHLOROBENZANILIDE 4-[(4-CHLOROPHENYL)PHENYLMETHYL]-1-PIPERAZINEETHANOL DIHYDROCHLORIDE 3-amino-4-chloro-N-phenylbenzamide 4,5-DICHLOROPHTHALIMIDE EPSILON-AMINOCAPROYL-P-CHLORO-BENZYLAMIDE HYDROCHLORIDE AURORA 52 4-CHLORO-N-(4-ETHOXYPHENYL)BENZAMIDE N-(4-AMINO-2-METHYLPHENYL)-4-CHLOROPHTHALIMIDE

(4-Chloro-benzyl)-methyl-amine ,97%

4-Chloro-N-methylbenzylamine

4-Chloro-N-methylbenzenemethanamine

N-Methyl-4-chlorobenzylamine

Description: N-(4-chlorobenzyl)-N-methylamine

(4-CHLORO-BENZYL)-ME

(4-Chlorophenyl)-N-methylmethylamine

1-(4-chlorophenyl)-N-MethylMethanaMine

Benzenemethanamine, 4-chloro-N-methyl-

4-Chloro-<i>N</i>-methylbenzylamine

N-(4-CHLOROBENZYL)-N-METHYLAMINE

P-CHLORO-N-METHYLBENZYLAMINE

N-METHYL-P-CHLOROBENZYLAMINE

TIMTEC-BB SBB010371

N-Methyl-4-chlorobenzylamine Hydrochloride

AKOS BC-2745

(4-CHLORO-BENZYL)-METHYL-AMINE

-(4-CHLOROBENZYL)-N-METHYLAMINE

4-Chloro-N-methylbenzylamine&gt

104-11-0

Polyamines

Halides

Amines and Anilines

amine|alkyl chloride