Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate

ChemicalBook > CAS DataBase List > Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate

Product Name: Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate
CAS No.: 147531-11-1
Chemical Name: Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate
Synonyms: Diphenyl(trifluoromethyl);diphenyl(trifluoromethyl)sulfanium;sulfonium trifluoromethanesulfonate;diphenyl-(trifluoroMethyl)-sulfoniuM;(S)-(trifluoroMethyl)diphenylsulfoniuM triflate;Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfot;Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonat;diphenyl(trifluoromethyl)sulfanium trifluoromethanesulfonate;diphenyl-(trifluoromethyl)-sulfonium trifluoromethanesulfonate;Diphenyl-(trifluoroMethyle)-sulfoniuM trifluoroMethancesulfonate
CBNumber: CB22470708
Molecular Formula: C13H10F3S.CF3O3S
Formula Weight: 404.35
MOL File: 147531-11-1.mol

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Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate Property

Melting point:: 84-85 °C
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: D492063
Product name: Diphenyl(trifluoromethyl)sulfoniumtrifluoromethanesulfonate
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: D492063
Product name: Diphenyl(trifluoromethyl)sulfoniumtrifluoromethanesulfonate
Packaging: 500mg
Price: $220
Updated: 2021/12/16

ChemScene

Product number: CS-0049606
Product name: Diphenyl(trifluoromethyl)sulfoniumtrifluoromethanesulfonate
Purity: >97.0%
Packaging: 5g
Price: $409
Updated: 2021/12/16

Apolloscientific

Product number: PC905034
Product name: Diphenyl(trifluoromethyl)sulfoniumtrifluoromethanesulfonate
Purity: 98%
Packaging: 250mg
Price: $77
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK1415797
Product name: Diphenyl(trifluoromethyl)sulfoniumtrifluoromethanesulfonate
Purity: 99%
Packaging: 100mg
Price: $120
Updated: 2021/12/16

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Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate Chemical Properties,Usage,Production

Uses

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate can be used as a raw material for organic synthesis with styrene derivatives to synthesise 2-arylazo pyridine at low temperature^[1].

Synthesis

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate is synthesised using phenyl trifluoromethyl sulfoxide as a raw material by chemical reaction. The specific synthesis steps are as follows:
Trifluoromethyl sulfoxide (0.4 g, 2.1 mmol) and then benzene (4.9 g, 64 mmol) are introduced, under an inert atmosphere and at approximately 0° C. (lower limit below which benzene crystallizes), into a Schlenck tube purged beforehand with argon. Five equivalents of triflic anhydride (2.82 g, 10 mmol) are gradually added. The mixture is stirred for 1 h at 0° C. and then for 24 h at ambient temperature. The medium is evaporated and the residue is purified by chromatography with the CH3CN/CH2Cl2 (1/4) mixture as eluent. White crystals (Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate), having a melting point of 69-70° C., are obtained with a yield of 40%.

References

[1] J. MATSUO. A Convenient Method for the Synthesis of 2-Arylaziridines from Styrene Derivatives via 2-Arylethenyl(diphenyl)sulfonium Salts[J]. Chemistry Letters, 2003. DOI:10.1246/CL.2003.392.

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonate manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: diphenyl-(trifluoromethyl)-sulfonium trifluoromethanesulfonate 147531-11-1
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-09

147531-11-1, Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonateRelated Search:

2-CYANOPROP-2-ENOIC ACID (4-bromophenyl)diphenylphosphine diphenyl(2,2,2-trifluoroethyl)sulfanium trifluoromethanesulfonate (perfluoroethyl)diphenylsulfonium trifluoromethanesulfonate Mesityl(2,2,2-trifluoroethyl)iodonium trifluoromethanesulfonate (difluoromethyl)(2,4-dimethylphenyl)(phenyl)sulfonium tetrafluoroborate Iodonium, (1,1,2,2,3,3,4,4,4-nonafluorobutyl)phenyl-,1,1,1-trifluoromethanesulfonate (2,2-difluoroethyl)diphenylsulfonium trifluoromethanesulfonate 1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent 2,2,2-trifluoroethyl(phenyl)iodonium trifluoromethanesulfonate (Difluoromethyl)bis(2,5-dimethylphenyl)sulfonium Tetrafluoroborate 1-TrifluoroMethyl-1,2-benziodoxol-3(1H)-one (PERFLUORO-N-HEXYL)PHENYLIODONIUM TRIFLUOROMETHANESULFONATE

diphenyl-(trifluoromethyl)-sulfonium trifluoromethanesulfonate

diphenyl-(trifluoroMethyl)-sulfoniuM

Diphenyl-(trifluoroMethyle)-sulfoniuM trifluoroMethancesulfonate

(S)-(trifluoroMethyl)diphenylsulfoniuM triflate

diphenyl(trifluoromethyl)sulfanium trifluoromethanesulfonate

diphenyl(trifluoromethyl)sulfanium

Diphenyl(trifluoromethyl)

sulfonium trifluoromethanesulfonate

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfonat

Diphenyl(trifluoromethyl)sulfonium trifluoromethanesulfot

Sulfonium, diphenyl(trifluoromethyl)-, 1,1,1-trifluoromethanesulfonate (1:1)

147531-11-1

C14H10F6O3S2