3-Iodopyridine-2-carboxylic acid methyl ester

Product Name: 3-Iodopyridine-2-carboxylic acid methyl ester
CAS No.: 73841-41-5
Chemical Name: 3-Iodopyridine-2-carboxylic acid methyl ester
Synonyms: Methyl 3-iodopicolinate;Methyl 3-iodo-2-picolinate;Methyl 3-iodopyridine-2-carboxylate 97%;3-Iodo-2-pyridinecarboxylic acid methyl ester;3-Iodopyridine-2-carboxylic acid methyl ester;2-Pyridinecarboxylic acid, 3-iodo-, methyl ester
CBNumber: CB22506652
Molecular Formula: C7H6INO2
Formula Weight: 263.03
MOL File: 73841-41-5.mol

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3-Iodopyridine-2-carboxylic acid methyl ester Property

Boiling point:: 298.5±20.0 °C(Predicted)
Density: 1.844±0.06 g/cm3(Predicted)
Flash point:: >110℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: solid
pka: -0.66±0.10(Predicted)

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Safety

WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 766844
Product name: Methyl 3-iodopyridine-2-carboxylate
Purity: 97%
Packaging: 1g
Price: $106
Updated: 2025/07/31

TRC

Product number: M262738
Product name: Methyl3-Iodopicolinate
Packaging: 1g
Price: $330
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H23-H-02
Product name: Methyl 3-iodopyridine-2-carboxylate
Packaging: 5G
Price: $435
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0261107
Product name: METHYL 3-IODOPYRIDINE-2-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $496.75
Updated: 2021/12/16

AK Scientific

Product number: 7756CD
Product name: Methyl3-iodopicolinate
Packaging: 5g
Price: $849
Updated: 2021/12/16

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3-Iodopyridine-2-carboxylic acid methyl ester Chemical Properties,Usage,Production

Synthesis

67-56-1

73841-32-4

73841-41-5

General procedure for the synthesis of methyl 3-iodopyridinecarboxylate from methanol and 3-iodopyridine-2-carboxylic acid: a mixture of 3-iodopyridine-2-carboxylic acid (D1, 3.0 g, 0.012 mol) and concentrated sulfuric acid (2 mL) in methanol (100 mL) was heated and refluxed for 18 hr at 65 °C. After completion of the reaction, the solvent was removed by rotary evaporator under reduced pressure. The residue was alkalized to neutrality with solid sodium bicarbonate and subsequently extracted with ethyl acetate (3 × 100 mL). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give methyl 3-iodopyridinecarboxylate (2.2 g, 70% yield). NMR hydrogen spectrum (CDCl3, 250 MHz) δH: 4.01 (3H, s), 7.13 (1H, dd), 8.29 (1H, dd), 8.64 (1H, dd). Mass spectrum (electrospray ionization): calculated value of 263 and measured value of 264 (MH+) for C7H6INO2.

References

[1] Patent: US2008/312209, 2008, A1. Location in patent: Page/Page column 13
[2] Patent: WO2007/7018, 2007, A1. Location in patent: Page/Page column 39
[3] Patent: WO2006/25783, 2006, A1. Location in patent: Page/Page column 120-121

3-Iodopyridine-2-carboxylic acid methyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodopyridine-2-carboxylic acid methyl ester Suppliers

China 39 Germany 1 India 1 United Kingdom 1 United States 3 Global 45

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73841-41-5, 3-Iodopyridine-2-carboxylic acid methyl esterRelated Search:

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3-Iodopyridine-2-carboxylic acid methyl ester

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Methyl 3-iodopyridine-2-carboxylate 97%

2-Pyridinecarboxylic acid, 3-iodo-, methyl ester

73841-41-5