3-(Boc-amino)-3-methylpip...

Product Name: 3-(Boc-amino)-3-methylpip...
CAS No.: 169750-96-3
Chemical Name: 3-(Boc-amino)-3-methylpip...
Synonyms: 3-(Boc-amino)-3-methylpip...;3-(Boc-aMino)-3-Methylpiperidine;3-Amino-3-methylpiperidine, 3-BOC protected;tert-Butyl 3-methylpiperidin-3-yl-carbamate;tert-butyl n-(3-methylpiperidin-3-yl)carbamate;(3-Methyl-piperidin-3-yl)-carbamic acid tert-butyl ester;(3-Methyl-3-piperidinyl)carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-(3-methyl-3-piperidinyl)-, 1,1-dimethylethyl ester;tert-Butyl (3-methylpiperidin-3-yl)carbamate, 3-[(tert-Butoxycarbonyl)amino]-3-methylpiperidine
CBNumber: CB22525095
Molecular Formula: C11H22N2O2
Formula Weight: 214.3
MOL File: 169750-96-3.mol

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3-(Boc-amino)-3-methylpip... Property

Boiling point:: 308.4±31.0 °C(Predicted)
Density: 1.01±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 12?+-.0.20(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B630050
Product name: 3-(Boc-amino)-3-methylpiperidine
Packaging: 100mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: Y1662
Product name: 3-(Boc-amino)-3-methylpiperidine
Packaging: 1g
Price: $167
Updated: 2021/12/16

AK Scientific

Product number: Y1662
Product name: 3-(Boc-amino)-3-methylpiperidine
Packaging: 5g
Price: $402
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM1052023
Product name: TERT-BUTYL N-(3-METHYLPIPERIDIN-3-YL)CARBAMATE
Purity: 95.00%
Packaging: 5MG
Price: $450.59
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H51-1-2V
Product name: 3-Amino-3-methylpiperidine, 3-Boc protected
Packaging: 1g
Price: $525
Updated: 2021/12/16

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3-(Boc-amino)-3-methylpip... Chemical Properties,Usage,Production

Synthesis

1196506-86-1

169750-96-3

General procedure for the synthesis of tert-butyl (3-methylpiperidin-3-yl)carbamate from the compound (CAS:1196506-86-1): benzyl 3-((tert-butoxycarbonyl)amino)-3-methylpiperidine-1-carboxylate (78 mg, 0.22 mmol, prepared according to the method described in WO09/140320) was dissolved in EtOH (5 mL) , which was degassed by bubbling N2 (g) into the solution for 10 min. Pd/C (10 wt%, 24 mg, 0.022 mmol) was added. A gas bladder attached to a three-way cork filled with H2 was connected to the flask. The flask was evacuated and backfilled with H2 (repeated 3 times). The mixture was stirred at room temperature for 2 hours. Degassing was again carried out by bubbling N2 (g) into the solution for 10 min, followed by filtration through diatomaceous earth. The filtrate was concentrated to give racemic-tert-butyl (3-methylpiperidin-3-yl) carbamate (42 mg, 0.20 mmol, 88% yield) as a clear, colorless oil.MS (ESI, cationic) m/z: 215.1 (M + 1).

References

[1] Patent: WO2012/148775, 2012, A1. Location in patent: Page/Page column 124; 125
[2] Patent: WO2009/140320, 2009, A1. Location in patent: Page/Page column 73

3-(Boc-amino)-3-methylpip... Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(Boc-amino)-3-methylpip... Suppliers

China 44 India 1 United Kingdom 1 United States 5 Global 51

Aemon Chemical

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Shanghai Huaxing Biological Technology Co., Ltd.

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Aikon International Limited

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View Lastest Price from 3-(Boc-amino)-3-methylpip... manufacturers

Career Henan Chemical Co

Product: tert-butyl (3-methylpiperidin-3-yl)carbamate 169750-96-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-09

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3-(Boc-aMino)-3-Methylpiperidine

3-Amino-3-methylpiperidine, 3-BOC protected

tert-Butyl (3-methylpiperidin-3-yl)carbamate, 3-[(tert-Butoxycarbonyl)amino]-3-methylpiperidine

(3-Methyl-3-piperidinyl)carbamic acid 1,1-dimethylethyl ester

(3-Methyl-piperidin-3-yl)-carbamic acid tert-butyl ester

Carbamic acid, N-(3-methyl-3-piperidinyl)-, 1,1-dimethylethyl ester

169750-96-3