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Ethanedioic acid,1-methyl ester, potassium salt (1:1)

Product Name
Ethanedioic acid,1-methyl ester, potassium salt (1:1)
CAS No.
10304-09-3
Chemical Name
Ethanedioic acid,1-methyl ester, potassium salt (1:1)
Synonyms
Methyl potassium oxalate 95%;Potassium methoxy(oxo)acetate;Potassium 2-methoxy-2-oxoacetate;potassium methyl hydrogen oxalate;potassium oxalate monomethyl ester;Tiotropium Bromide Impurity 8 Potassium Salt;Ethanedioic acid,1-methyl ester, potassium salt;Ethanedioicacid,monomethylester,potassiumsalt(1:1);Ethanedioic acid, monomethyl ester, potassium salt;Ethanedioic acid,1-methyl ester, potassium salt (1:1)
CBNumber
CB23177664
Molecular Formula
C3H3KO4
Formula Weight
142.15182
MOL File
10304-09-3.mol
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Ethanedioic acid,1-methyl ester, potassium salt (1:1) Property

Melting point:
197 °C
storage temp. 
Inert atmosphere,Room Temperature
form 
solid
color 
White
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Safety

HS Code 
2917110099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
M339363
Product name
Methylpotassiumoxalate
Packaging
50mg
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
102023
Product name
Methyl potassium oxalate
Purity
>95%
Packaging
500mg
Price
$33
Updated
2021/12/16
Matrix Scientific
Product number
102023
Product name
Methyl potassium oxalate
Purity
>95%
Packaging
1g
Price
$50
Updated
2021/12/16
Apolloscientific
Product number
OR303344
Product name
Methylpotassiumoxalate
Purity
95%
Packaging
500mg
Price
$160
Updated
2021/12/16
Apolloscientific
Product number
OR303344
Product name
Methylpotassiumoxalate
Purity
95%
Packaging
1g
Price
$189
Updated
2021/12/16
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Ethanedioic acid,1-methyl ester, potassium salt (1:1) Chemical Properties,Usage,Production

Synthesis

553-90-2

10304-09-3

General procedure for the synthesis of potassium 2-methoxy-2-oxoacetate from dimethyl oxalate: 1.2 g of dimethyl oxalate and 0.98 g of potassium acetate were dissolved in a mixed solvent of 10 mL of methanol and 10 mL of water. The reaction mixture was stirred at 80 °C for 3 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. A white solid product was obtained in quantitative yield.

References

[1] Patent: WO2005/53609, 2005, A2. Location in patent: Page/Page column 25-26
[2] Patent: WO2005/53609, 2005, A2. Location in patent: Page/Page column 25-26
[3] Patent: CN105439883, 2016, A. Location in patent: Paragraph 0051
[4] Chemical and Pharmaceutical Bulletin, 1998, vol. 46, # 3, p. 514 - 517
[5] Journal of the American Chemical Society,

Ethanedioic acid,1-methyl ester, potassium salt (1:1) Preparation Products And Raw materials

Raw materials

Preparation Products

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Ethanedioic acid,1-methyl ester, potassium salt (1:1) Suppliers

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