Ethanedioic acid,1-methyl ester, potassium salt (1:1)
- Product Name
- Ethanedioic acid,1-methyl ester, potassium salt (1:1)
- CAS No.
- 10304-09-3
- Chemical Name
- Ethanedioic acid,1-methyl ester, potassium salt (1:1)
- Synonyms
- Methyl potassium oxalate 95%;Potassium methoxy(oxo)acetate;Potassium 2-methoxy-2-oxoacetate;potassium methyl hydrogen oxalate;potassium oxalate monomethyl ester;Tiotropium Bromide Impurity 8 Potassium Salt;Ethanedioic acid,1-methyl ester, potassium salt;Ethanedioicacid,monomethylester,potassiumsalt(1:1);Ethanedioic acid, monomethyl ester, potassium salt;Ethanedioic acid,1-methyl ester, potassium salt (1:1)
- CBNumber
- CB23177664
- Molecular Formula
- C3H3KO4
- Formula Weight
- 142.15182
- MOL File
- 10304-09-3.mol
Ethanedioic acid,1-methyl ester, potassium salt (1:1) Property
- Melting point:
- 197 °C
- storage temp.
- Inert atmosphere,Room Temperature
- form
- solid
- color
- White
Safety
- HS Code
- 2917110099
N-Bromosuccinimide Price
- Product number
- M339363
- Product name
- Methylpotassiumoxalate
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 102023
- Product name
- Methyl potassium oxalate
- Purity
- >95%
- Packaging
- 500mg
- Price
- $33
- Updated
- 2021/12/16
- Product number
- 102023
- Product name
- Methyl potassium oxalate
- Purity
- >95%
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- OR303344
- Product name
- Methylpotassiumoxalate
- Purity
- 95%
- Packaging
- 500mg
- Price
- $160
- Updated
- 2021/12/16
- Product number
- OR303344
- Product name
- Methylpotassiumoxalate
- Purity
- 95%
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
Ethanedioic acid,1-methyl ester, potassium salt (1:1) Chemical Properties,Usage,Production
Synthesis
553-90-2
10304-09-3
General procedure for the synthesis of potassium 2-methoxy-2-oxoacetate from dimethyl oxalate: 1.2 g of dimethyl oxalate and 0.98 g of potassium acetate were dissolved in a mixed solvent of 10 mL of methanol and 10 mL of water. The reaction mixture was stirred at 80 °C for 3 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. A white solid product was obtained in quantitative yield.
References
[1] Patent: WO2005/53609, 2005, A2. Location in patent: Page/Page column 25-26
[2] Patent: WO2005/53609, 2005, A2. Location in patent: Page/Page column 25-26
[3] Patent: CN105439883, 2016, A. Location in patent: Paragraph 0051
[4] Chemical and Pharmaceutical Bulletin, 1998, vol. 46, # 3, p. 514 - 517
[5] Journal of the American Chemical Society,
Ethanedioic acid,1-methyl ester, potassium salt (1:1) Preparation Products And Raw materials
Raw materials
Preparation Products
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