2'-FLUORO-6'-METHOXYACETOPHENONE

Product Name: 2'-FLUORO-6'-METHOXYACETOPHENONE
CAS No.: 120484-50-6
Chemical Name: 2'-FLUORO-6'-METHOXYACETOPHENONE
Synonyms: 2-FLUORO-6-METHOXYACETOPHENONE;2'-Fluoro-6'-methoxyacetophenone;1-(2-FLUORO-6-METHOXYPHENYL)ETHANONE;Ethanone, 1-(2-fluoro-6-methoxyphenyl)-;2′-Fluoro-6′-methoxyacetophenone, CAS 120484-50-6
CBNumber: CB2359807
Molecular Formula: C9H9FO2
Formula Weight: 168.16
MOL File: 120484-50-6.mol

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2'-FLUORO-6'-METHOXYACETOPHENONE Property

Boiling point:: 217℃
Density: 1.127
refractive index: 1.508
Flash point:: 83℃
storage temp.: Sealed in dry,Room Temperature
form: liquid
color: Clear, lemon/pale amber

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Safety

Hazard Codes: Xi
Hazard Note: Irritant
HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: F593410
Product name: 1-(2-Fluoro-6-methoxyphenyl)ethanone
Packaging: 5g
Price: $525
Updated: 2021/12/16

Apolloscientific

Product number: PC4586
Product name: 2'-Fluoro-6'-methoxyacetophenone
Packaging: 1g
Price: $60
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2617-3-45
Product name: 2'-Fluoro-6'-methoxyacetophenone
Packaging: 1g
Price: $66
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0019907
Product name: 2'-FLUORO-6'-METHOXYACETOPHENONE
Purity: 95.00%
Packaging: 250MG
Price: $131.25
Updated: 2021/12/16

AK Scientific

Product number: Z8240
Product name: 1-(2-Fluoro-6-methoxyphenyl)ethanone
Packaging: 5g
Price: $163
Updated: 2021/12/16

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2'-FLUORO-6'-METHOXYACETOPHENONE Chemical Properties,Usage,Production

Uses

1-(2-Fluoro-6-methoxyphenyl)ethanone is a useful synthetic intermediate. It is used to prepare spiro[2H-1-benzopyran-2,4''-piperidine] derivatives as glycine transport inhibitors.

Synthesis

120484-49-3

120484-50-6

General procedure for the synthesis of 2-fluoro-6-methoxyacetophenone from 1-(2-fluoro-6-methoxyphenyl)ethan-1-ol: Pyridinium dichromate (44 g, 0.116 mol) was added to a solution of N,N-dimethylformamide (130 mL) of 1-(2-fluoro-6-methoxyphenyl)ethan-1-ol (13.1 g, 0.077 mol). stirred at room temperature for 12 hours. Upon completion of the reaction, water (300 mL) was added to the reaction mixture, diluted with ethyl acetate and filtered through diatomaceous earth. The organic layer was separated, washed with saturated brine, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford 2-fluoro-6-methoxyacetophenone as a brown liquid (9.2 g, 70% yield).1H-NMR (δ ppm, CDCl3, 400 MHz): 7.73 (dd, J = 15.1, 8.4 Hz, 1H), 6.73 (m, 2H), 3.85 (s, 3H), 2.53 (s, 3H), 3.85 (s, 3H), 3.85 (s, 3H), 3.85 (s, 3H). 3H), 2.53 (s, 3H).

References

[1] Journal of the American Chemical Society, 2016, vol. 138, # 5, p. 1486 - 1489
[2] Patent: US2012/289496, 2012, A1. Location in patent: Page/Page column 100
[3] Patent: WO2012/151525, 2012, A1. Location in patent: Page/Page column 101

2'-FLUORO-6'-METHOXYACETOPHENONE Preparation Products And Raw materials

Raw materials

Preparation Products

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2'-FLUORO-6'-METHOXYACETOPHENONE Suppliers

China 62 Germany 2 India 4 Switzerland 1 The Netherlands 1 United Kingdom 10 United States 9 Global 89

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View Lastest Price from 2'-FLUORO-6'-METHOXYACETOPHENONE manufacturers

Career Henan Chemical Co

Product: 2'-FLUORO-6'-METHOXYACETOPHENONE 120484-50-6
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

120484-50-6, 2'-FLUORO-6'-METHOXYACETOPHENONERelated Search:

2-FLUORO-6-METHOXYACETOPHENONE

1-(2-FLUORO-6-METHOXYPHENYL)ETHANONE

Ethanone, 1-(2-fluoro-6-methoxyphenyl)-

2'-Fluoro-6'-methoxyacetophenone

2′-Fluoro-6′-methoxyacetophenone, CAS 120484-50-6

120484-50-6

Aromatic Acetophenones & Derivatives (substituted)