1-Bromo-2,3-dichlorobenzene

Product Name: 1-Bromo-2,3-dichlorobenzene
CAS No.: 56961-77-4
Chemical Name: 1-Bromo-2,3-dichlorobenzene
Synonyms: 2,3-DICHLOROBROMOBENZENE;1-Bromo-2,3-dichL;1-Bromo-2,3-dichloro;2,3-Dichlorophenyl Bromide;1,2-Dichloro-3-bromobenzene;1-Bromo-2,2-dichlorobenzene;1-BROMO-2,3-DICHLOROBENZENE;2,3-DICHLORO-1-BROMOBENZENE;Benzene, 1-bromo-2,3-dichloro-;1-BROMO-2,3-DICHLOROBENZENE 98%
CBNumber: CB2376392
Molecular Formula: C6H3BrCl2
Formula Weight: 225.9
MOL File: 56961-77-4.mol

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1-Bromo-2,3-dichlorobenzene Property

Melting point:: 58-61 °C(lit.)
Boiling point:: 243 °C765 mm Hg(lit.)
Density: 1.6351 (rough estimate)
refractive index: 1.5700 (estimate)
Flash point:: 243°C
storage temp.: 2-8°C
form: powder to crystal
color: White to Light yellow to Light orange
Water Solubility: insoluble
BRN: 2246806
InChIKey: HVKCZUVMQPUWSX-UHFFFAOYSA-N
CAS DataBase Reference: 56961-77-4(CAS DataBase Reference)
NIST Chemistry Reference: 1-Bromo-2,3-dichlorobenzene(56961-77-4)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39-28A-24/25
WGK Germany: 3
HS Code: 29039990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B0980
Product name: 1-Bromo-2,3-dichlorobenzene
Packaging: 5G
Price: $17
Updated: 2025/07/31

TCI Chemical

Product number: B0980
Product name: 1-Bromo-2,3-dichlorobenzene
Packaging: 25G
Price: $41
Updated: 2025/07/31

TRC

Product number: B687435
Product name: 1-Bromo-2,3-dichlorobenzene
Packaging: 10g
Price: $55
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0016010
Product name: 1-BROMO-2,3-DICHLOROBENZENE
Purity: 95.00%
Packaging: 25G
Price: $1062.79
Updated: 2021/12/16

AK Scientific

Product number: L030
Product name: 2,3-Dichlorobromobenzene
Packaging: 500g
Price: $321
Updated: 2021/12/16

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1-Bromo-2,3-dichlorobenzene Chemical Properties,Usage,Production

Chemical Properties

LIGHT YELLOW CRYSTALLINE FLAKES

Uses

1-Bromo-2,3-dichlorobenzene is a reagent used in the preparation of selective nonpeptidic inhibitors of striatal-enriched protein tryosine phosphatase.

Synthesis

608-27-5

56961-77-4

Example P4: Preparation of 1-bromo-2,3-dichlorobenzene (compound AD). 163 g of 2,3-dichloroaniline (1.0 mol) was added to a mixture of 3250 g of 30% HBr aqueous solution (12.0 mol) with 25.4 g of copper powder. The mixture was stirred at 35-37 °C for 15 min, followed by the slow addition of 766 g of 40% NaNO2 aqueous solution (4.44 mol) by subsurface addition, which was maintained for 3 hours. Simultaneously with the addition of NaNO2, 489 g of 2,3-dichloroaniline (3.0 mol) was added over 2.5 hours at the same temperature. Fifteen minutes after the start of NaNO2 addition, the addition of dichloroquinoline was started. After all additions were completed, the reaction mixture was continued to be stirred at 35°C for 30 minutes. Subsequently, the reaction mixture was heated to 60-65°C and the organic phase containing the reaction product was separated from the aqueous phase. The aqueous phase was discarded and the crude product was washed twice with 200 ml of water. 792.2 g of crude 1-bromo-2,3-dichlorobenzene was finally obtained (yield 87.7% of the theoretical value, purity 86.2%).

References

[1] Patent: WO2008/49507, 2008, A1. Location in patent: Page/Page column 8
[2] Patent: WO2008/49507, 2008, A1. Location in patent: Page/Page column 7
[3] Patent: WO2008/49507, 2008, A1. Location in patent: Page/Page column 7-8
[4] Patent: WO2008/49507, 2008, A1. Location in patent: Page/Page column 7

1-Bromo-2,3-dichlorobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Bromo-2,3-dichlorobenzene Suppliers

Americas 1 China 180 Europe 4 France 1 Germany 5 India 10 Japan 4 Slovakia 1 Switzerland 3 The Netherlands 1 Ukraine 1 United Kingdom 18 United States 24 Global 253

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View Lastest Price from 1-Bromo-2,3-dichlorobenzene manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 1-Bromo-2,3-dichlorobenzene 56961-77-4
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-25

Speranza Chemical Co., Ltd.

Product: 1-Bromo-2,3-dichlorobenzene 56961-77-4
Price: US $120.00/KG
Min. Order: 1KG
Purity: 98%+
Supply Ability: 56961-77-4
Release date: 2019-12-24

Henan Fengda Chemical Co., Ltd

Product: 1-Bromo-2,3-dichlorobenzene 56961-77-4
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-26

56961-77-4, 1-Bromo-2,3-dichlorobenzeneRelated Search:

2-Bromobenzonitrile 4'-Bromopropiophenone 1,2-Dichlorobenzene 3-Bromoanisole 2-Bromofluorobenzene 1-BROMO-3,5-DICHLOROBENZENE 1,4-Dichlorobenzene 4-Bromobenzaldehyde Bromoxynil octanoate 1-Bromo-3,4-dichlorobenzene, 98+%,4-Bromo-1,2-dichlorobenzene, 98+%,4-BROMO-1,2-DICHLOROBENZENE,1-BROMO-3,4-DICHLOROBENZENE p-Dichlorobenzene 1-BROMO-2,4-DICHLOROBENZENE / 2,4-DICHLOROBROMOBENZENE,1-BROMO-2,4-DICHLOROBENZENE,BROMO(2-)-4-DICHLOROBENZENE,1-Bromo-2,4-dichlorobenzene, 98+% 1-BROMO-2,3,5-TRICHLOROBENZENE Bromine 6-BROMO-2,4,5-TRICHLOROPHENOL Pigment Green 36 4,6-DIBROMO-2,3-DICHLOROANILINE 1-BROMO-2,6-DICHLOROBENZENE,2-BROMO-1,3-DICHLOROBENZENE,BROMO-2 6-DICHLOROBENZENE 99%

2,3-DICHLOROBROMOBENZENE

2,3-DICHLORO-1-BROMOBENZENE

1-BROMO-2,3-DICHLOROBENZENE

Benzene, 1-bromo-2,3-dichloro-

1-BROMO-2,3-DICHLOROBENZENE 98%

1-Bromo-2,3-Dichlorobenzene,>98%

1,2-Dichloro-3-bromobenzene

1-Bromo-2,3-dichlorobenzene,99%

1-Bromo-2,2-dichlorobenzene

1-Bromo-2,3-dichloro

6-broMo-5,5-dichlorocyclohexa-1,3-diene

2,3-Dichlorophenyl Bromide

1-Bromo-2,3-dichlorobenzene 2,3-Dichlorobromobenzene

1-Bromo-2,3-dichlorobenzene &gt

1-Bromo-2,3-dichL

1-Bromo-2,3-dichlorobenzene ISO 9001：2015 REACH

56961-77-4

ARYL HALIDE

Aryl

Building Blocks

Organic Building Blocks

Halogenated Hydrocarbons

C6

Aryl

Halogenated Hydrocarbons

Bromine Compounds

Chlorine Compounds

Aromatic Hydrocarbons (substituted) & Derivatives

C6