10-Bromodecanol

Product Name: 10-Bromodecanol
CAS No.: 53463-68-6
Chemical Name: 10-Bromodecanol
Synonyms: 10-BROMODECAN-1-OL;10-BROMODECANOL;10-Bromo-1-decan;10-bromo-1-decano;10-BROMO-1-DECANOL;1-bromo-10-decanol;1-Decanol, 10-bromo-;10-Bromo-1-decanol,95%;10-Bromo-1-decanol >10-BROMO-1-DECANOL 85+%
CBNumber: CB2490678
Molecular Formula: C10H21BrO
Formula Weight: 237.18
MOL File: 53463-68-6.mol

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10-Bromodecanol Property

Boiling point:: 165-169 °C/10 mmHg (lit.)
Density: 1.19 g/mL at 25 °C (lit.)
refractive index: n20/D 1.476(lit.)
Flash point:: >230 °F
storage temp.: Inert atmosphere,Store in freezer, under -20°C
solubility: Chloroform (Sparingly)
form: Liquid
pka: 15.20±0.10(Predicted)
color: Clear yellow
Water Solubility: It is miscible with water.
BRN: 1738593
Stability:: Moisture Sensitive
InChIKey: LGZMUUBPTDRQQM-UHFFFAOYSA-N
CAS DataBase Reference: 53463-68-6(CAS DataBase Reference)
EPA Substance Registry System: 1-Decanol, 10-bromo- (53463-68-6)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
TSCA: Yes
HS Code: 29055900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 310891
Product name: 10-Bromo-1-decanol
Purity: technical grade, 90%
Packaging: 5g
Price: $105.45
Updated: 2025/07/31

TCI Chemical

Product number: B1730
Product name: 10-Bromo-1-decanol
Purity: >85.0%(GC)
Packaging: 5g
Price: $95
Updated: 2025/07/31

TCI Chemical

Product number: B1730
Product name: 10-Bromo-1-decanol
Purity: >85.0%(GC)
Packaging: 25g
Price: $290
Updated: 2025/07/31

Usbiological

Product number: 411597
Product name: 10-Bromo-1-decanol
Packaging: 1g
Price: $312
Updated: 2021/12/16

TRC

Product number: B688690
Product name: 10-Bromo-1-decanol
Packaging: 25g
Price: $225
Updated: 2021/12/16

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10-Bromodecanol Chemical Properties,Usage,Production

Chemical Properties

Clear yellow liquid

Uses

10-Bromo-1-decanol is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff. It was also used in the synthesis of (11Z,13Z)-11,13-hexadecadienal, the female sex pheromone of the navel orangeworm (Amyelois transitella).

Uses

10-Bromodecanol can be used to synthesize rotaxane dendrimers. It can also be used to synthesize J2326, a molecule that induces neurite outgrowth in neuronal cells.

Definition

ChEBI: 10-Bromo-1-decanol is a primary alcohol.

Synthesis

112-47-0

53463-68-6

General procedure for the synthesis of 10-bromo-1-decanol from 1,10-decanediol: 1,10-decanediol (10 g, 57.47 mmol) was dissolved in toluene (600 mL) and transferred to a 1 L two-necked, round-bottomed flask fitted with a Dean-Stark separator. 48% hydrobromic acid (7.15 mL, 63.21 mmol) was slowly added to the reaction system and subsequently heated to reflux for 16 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was washed sequentially with 1 N hydrochloric acid, 2 M aqueous sodium hydroxide, deionized water and saturated saline. The organic phase was separated, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: 15% ethyl acetate/hexane) to afford 10-bromo-1-decanol as a colorless transparent oil (12.7 g, 93% yield). Thin layer chromatography (TLC) Rf = 0.45 (unfolding agent: 20% ethyl acetate/hexane); 1H NMR (500 MHz, CDCl3): δ 3.63 (t, J = 5.8 Hz, 2H), 3.39 (t, J = 6.8 Hz, 2H), 1.85 (m, 2H), 1.56 (m, 2H), 1.42 (m, 2H), 1.38- 1.27 (m, 10H); 13C NMR (125 MHz, CDCl3): δ 62.9, 33.9, 32.7, 32.6, 29.3, 29.2, 29.2, 28.6, 28.0, 25.6; infrared spectra (neat sample): νmax 2927, 2856, 1738, 1593, 1449, 1367, 1241 cm-1; high-resolution mass spectrum (ESI): calculated value C10H22BrO [M + H]+ 237.0854, measured value 237.0845.

References

[1] Tetrahedron, 2015, vol. 71, # 7, p. 1058 - 1067
[2] Bioorganic and Medicinal Chemistry, 2010, vol. 18, # 3, p. 1083 - 1092
[3] ACS Medicinal Chemistry Letters, 2010, vol. 1, # 6, p. 273 - 276
[4] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 1, p. 567 - 579
[5] Patent: EP1818336, 2007, A1. Location in patent: Page/Page column 7

10-Bromodecanol Preparation Products And Raw materials

Raw materials

Preparation Products

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10-Bromodecanol Suppliers

Americas 1 Belgium 1 China 189 Europe 1 France 1 Germany 4 India 2 Japan 2 Switzerland 2 The Netherlands 1 Ukraine 2 United Kingdom 8 United States 23 Global 237

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View Lastest Price from 10-Bromodecanol manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 10-Bromodecanol 53463-68-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-22

Hebei Zhuanglai Chemical Trading Co.,Ltd

Product: 10-Bromodecanol 53463-68-6
Price: US $40.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 5000kg/week
Release date: 2024-05-30

Henan Aochuang Chemical Co.,Ltd.

Product: 10-Bromodecanol 53463-68-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-14

53463-68-6, 10-BromodecanolRelated Search:

Isodecanol 1-Decanol Bronopol 9,10,12,13-TETRABROMOSTEARIC ACID 10-Bromodecanoic acid 9,10-DIBROMOSTEARIC ACID HEXABROMOSTEARIC ACID Bromine METHYL 10-BROMODECANOATE 10-PHENOXYDECYL BROMIDE METHYL 9,10-DIBROMOSTEARATE 16A-BROMOANDROSTERONE 10-Bromodecanol 5-ALPHA-ANDROSTAN-2-ALPHA-BROMO-17-ALPHA-METHYL-17-BETA-OL-3-ONE 16BETA-BROMOANDROSTERONE 16-BROMO-10,13-DIMETHYL-17-OXO-2,3,4,7,8,9,10,11,12,13,14,15,16,17-TETRADECAHYDRO-1H-CYCLOPENTA[A]PHENANTHREN-3-YL ACETATE 5-BETA-PREGNAN-12-ALPHA-BROMO-3-ALPHA, 21-DIOL-11,20-DIONE DIACETATE 4-(BROMOMETHYL)-2-ADAMANTYL 4-NITROBENZENE-1-SULFONATE

10-Bromo-1-decan

DECAMETHYLENE BROMOHYDRIN

10-bromo-1-decano

10-Hydroxydecyl bromide

10-Bromo-1-decanol,95%

10-BROMO-1-DECANOL 85+%

10-BROMO-1-DECANOL, TECH., 90%

10-BROMODECAN-1-OL

1-Decanol, 10-bromo-

10-BROMO-1-DECANOL

10-BROMODECANOL

1-bromo-10-decanol

10-Bromo-1-decanol &gt

10-Hydroxy-1-bromo decane

Fulvestrant Impurity 72

53463-68-6

C10H21BrO

BrCH210OH

Organic Building Blocks

Oxygen Compounds

C9 to C30

蠅-Functional Alkanols, Carboxylic Acids, Amines & Halides

蠅-Bromoalkanols

Alcohols

Building Blocks

omega-Bromoalkanols

omega-Functional Alkanols, Carboxylic Acids, Amines & Halides

Linear hydrocarbon series

Alcohols

Building Blocks

C9 to C10

Chemical Synthesis

Organic Building Blocks

Oxygen Compounds

OLED materials,pharm chemical,electronic