2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER
- Product Name
- 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER
- CAS No.
- 53662-83-2
- Chemical Name
- 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER
- Synonyms
- Diethyl 2,5-furandicarboxylate;Diethyl furan-2,5-dicarboxylate;2,5-Furandicarboxylic diethyl ester;Diethyl furan-2,5-dicarboxylate 99%;2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER;Furan-2,5-dicarboxylic Acid Diethyl Ester;2,5-Furandicarboxylic acid, 2,5-diethyl ester
- CBNumber
- CB2496908
- Molecular Formula
- C10H12O5
- Formula Weight
- 212.2
- MOL File
- 53662-83-2.mol
2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER Property
- Melting point:
- 46-48°C
- Boiling point:
- 167-1680C/15Torr
- Density
- 1.172±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Solid
- color
- White
Safety
- HS Code
- 2932190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- F863760
- Product name
- 2,5-FurandicarboxylicAcidDiethylEster
- Packaging
- 100mg
- Price
- $105
- Updated
- 2021/12/16
- Product number
- F863760
- Product name
- 2,5-FurandicarboxylicAcidDiethylEster
- Packaging
- 2.5g
- Price
- $1185
- Updated
- 2021/12/16
- Product number
- 2H23-1-72
- Product name
- Diethylfuran-2,5-dicarboxylate
- Purity
- 99%
- Packaging
- 25g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- CHM0008156
- Product name
- 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1815
- Updated
- 2021/12/16
- Product number
- 114669
- Product name
- Diethyl furan-2,5-dicarboxylate
- Purity
- 97%
- Packaging
- 1g
- Price
- $623
- Updated
- 2021/12/16
2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER Chemical Properties,Usage,Production
Chemical Properties
White Solid
Uses
2,5-Furandicarboxylic Acid Diethyl Ester (cas# 53662-83-2) is a compound useful in organic synthesis.
Synthesis
3238-40-2
64-17-5
53662-83-2
To a solution of 2,5-furandicarboxylic acid (1.00 g, 6.41 mmol) in anhydrous ethanol (50 mL) was slowly added 98% aqueous sulfuric acid (0.05 mL), and the reaction mixture was heated and refluxed under nitrogen protection for 18 hours. Upon completion of the reaction, the solution was cooled to room temperature and subsequently concentrated under reduced pressure to remove the solvent. The concentrated residue was separated by filtration and washed sequentially with saturated aqueous sodium bicarbonate solution (3 x 10 mL) and deionized water (3 x 10 mL) to afford finally diethyl furan-2,5-dicarboxylate as a white solid (1.33 g, 98% yield). The structure of the product was confirmed by nuclear magnetic resonance hydrogen spectroscopy (1H NMR, 500 MHz, CDCl3) and carbon spectroscopy (13C NMR, 125 MHz, CDCl3) with the following data: 1H NMR δ 1.38 (t, J = 7.1 Hz, 6H), 4.39 (q, J = 7.1 Hz, 4H), 7.19 (s, 2H); 13C NMR δ 14.2, 61.6, 118.2, 146.9, 158.1.
References
[1] Patent: WO2016/202858, 2016, A1. Location in patent: Page/Page column 57
[2] Bioorganic and Medicinal Chemistry Letters, 2018,
[3] Patent: WO2012/101015, 2012, A1. Location in patent: Page/Page column 19-20
[4] Polish Journal of Chemistry, 2001, vol. 75, # 12, p. 1943 - 1946
[5] Organic and Biomolecular Chemistry, 2014, vol. 12, # 46, p. 9324 - 9328
2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER manufacturers
- Product
- 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER 53662-83-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-19
- Product
- 2,5-FURANDICARBOXYLIC ACID DIETHYL ESTER 53662-83-2
- Price
- US $7.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2018-12-14