ChemicalBook > CAS DataBase List > 3-Iodo-4-hydroxybenzaldehyde

3-Iodo-4-hydroxybenzaldehyde

Product Name
3-Iodo-4-hydroxybenzaldehyde
CAS No.
60032-63-5
Chemical Name
3-Iodo-4-hydroxybenzaldehyde
Synonyms
AKOS B029221;4-Formyl-2-iodophenol;4-Hyroxy-3-iodobenzaldehyde;4-HYDRO-3-IODO-BENZALDEHYDE;3-IODO-4-HYDROXYBENZALDEHYDE;4-HYDROXY-3-IODOBENZALDEHYDE;Benzaldehyde, 4-hydroxy-3-iodo-
CBNumber
CB2670579
Molecular Formula
C7H5IO2
Formula Weight
248.02
MOL File
60032-63-5.mol
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3-Iodo-4-hydroxybenzaldehyde Property

Melting point:
128-130°C
Boiling point:
257.8±25.0 °C(Predicted)
Density 
2.039±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Solid
pka
6.33±0.18(Predicted)
color 
White to Pale Beige
InChI
InChI=1S/C7H5IO2/c8-6-3-5(4-9)1-2-7(6)10/h1-4,10H
InChIKey
KNQVIRRXVOTGGT-UHFFFAOYSA-N
SMILES
C(=O)C1=CC=C(O)C(I)=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
I707250
Product name
3-Iodo-4-hydroxybenzaldehyde
Packaging
5g
Price
$1265
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0012587
Product name
3-IODO-4-HYDROXYBENZALDEHYDE
Purity
95.00%
Packaging
500MG
Price
$808.5
Updated
2021/12/16
Matrix Scientific
Product number
181582
Product name
4-Hydroxy-3-iodobenzaldehyde
Purity
95%
Packaging
10g
Price
$990
Updated
2021/12/16
Matrix Scientific
Product number
181582
Product name
4-Hydroxy-3-iodobenzaldehyde
Purity
95%
Packaging
25g
Price
$1650
Updated
2021/12/16
AK Scientific
Product number
X5653
Product name
4-Hydroxy-3-iodobenzaldehyde
Packaging
25g
Price
$2548
Updated
2021/12/16
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3-Iodo-4-hydroxybenzaldehyde Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

3-Iodo-4-hydroxybenzaldehyde (cas# 60032-63-5) is a compound useful in organic synthesis.

Synthesis

123-08-0

60032-63-5

General procedure for the synthesis of 4-hydroxy-3-iodobenzaldehyde from 4-hydroxybenzaldehyde: To a stirred solution of 4-hydroxybenzaldehyde (2.0 g, 16.39 mmol) in acetic acid (30 mL) was added N-iodosuccinimide (4.5 g, 19.67 mmol). The reaction mixture was stirred at room temperature for 16 hours and then filtered. The filtrate was poured into water (100 mL) and ethyl acetate (50 mL) was added. The aqueous phase was separated and then extracted with ethyl acetate (3 x 50 mL). The organic phases were combined, washed with water (2 × 20 mL), dried over anhydrous sodium sulfate, filtered and concentrated in vacuo to give the title compound (2.0 g, 50% yield) as a white solid, which was ready to be used without further purification.LCMS (ES-) m/z 247.1 ([M-H]-) with a retention time of 1.44 min (Method 9).

References

[1] Organic Preparations and Procedures International, 2002, vol. 34, # 6, p. 647 - 651
[2] Journal of the Brazilian Chemical Society, 2010, vol. 21, # 1, p. 3 - 6
[3] Journal of Organic Chemistry, 2002, vol. 67, # 24, p. 8622 - 8624
[4] Synthesis, 2010, # 9, p. 1467 - 1472
[5] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 2, p. 769 - 772

3-Iodo-4-hydroxybenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodo-4-hydroxybenzaldehyde Suppliers

Beijing Bosennuokang Pharmaceutical Technology Co., Ltd.
Tel
010-86203349 18201082367
Email
bosennuokang@163.com
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China
ProdList
224
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58
J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
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China
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96815
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Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006356688 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
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China
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40228
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3B Pharmachem (Wuhan) International Co.,Ltd.
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821-50328103-801 18930552037
Fax
86-21-50328109
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3bsc@sina.com
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China
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Wuhan Chemwish Technology Co., Ltd
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86-027-67849912
Fax
86-027-87531808
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sales@chemwish.com
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China
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Accela ChemBio Co.,Ltd.
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021-50795510 4000665055
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021-50795055
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sales@accelachem.com
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China
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Chemsky(shanghai)International Co.,Ltd.
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021-50135380
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shchemsky@sina.com
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China
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Shanghai Topbiochem Technology Co., Ltd
Tel
021-58170097
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info@topbiochem.com
Country
China
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9510
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58
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
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55
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
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View Lastest Price from 3-Iodo-4-hydroxybenzaldehyde manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
4-Hydroxy-3-iodobenzaldehyde 60032-63-5
Price
US $0.10-10.00/KG
Min. Order
0.10000000149011612KG
Purity
98%
Supply Ability
200TONS
Release date
2025-08-14
ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
4-Hydroxy-3-iodobenzaldehyde 60032-63-5
Price
US $1.10-9.90/kg
Min. Order
1kg
Purity
99%min
Supply Ability
100kg
Release date
2025-08-14
Career Henan Chemical Co
Product
3-IODO-4-HYDROXYBENZALDEHYDE 60032-63-5
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-09