BUTTPARK 80\07-66
- Product Name
- BUTTPARK 80\07-66
- CAS No.
- 50419-88-0
- Chemical Name
- BUTTPARK 80\07-66
- Synonyms
- BUTTPARK 80\07-66;4-Chloro-5-bromoanthranilic acid;2-AMINO-5-BROMO-4-CHLOROBENZOIC ACID;BENZOIC ACID, 2-AMINO-5-BROMO-4-CHLORO-;2-amino-5-bromo-4-chlorobenzene carboxylic acid
- CBNumber
- CB2712246
- Molecular Formula
- C7H5BrClNO2
- Formula Weight
- 250.48
- MOL File
- 50419-88-0.mol
BUTTPARK 80\07-66 Property
- Boiling point:
- 385.0±42.0 °C(Predicted)
- Density
- 1.892
- storage temp.
- 2-8°C, protect from light
- pka
- 4.32±0.10(Predicted)
- Appearance
- Off-white to light brown Solid
N-Bromosuccinimide Price
- Product number
- A602063
- Product name
- 2-Amino-5-bromo-4-chlorobenzoicAcid
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FB45152
- Product name
- 5-Bromo-4-chloroanthranilic acid
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FB45152
- Product name
- 5-Bromo-4-chloroanthranilic acid
- Packaging
- 5G
- Price
- $400
- Updated
- 2021/12/16
- Product number
- HCH0363010
- Product name
- 2-AMINO-5-BROMO-4-CHLOROBENZOIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.65
- Updated
- 2021/12/16
- Product number
- FB45152
- Product name
- 5-Bromo-4-chloroanthranilic acid
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
BUTTPARK 80\07-66 Chemical Properties,Usage,Production
Synthesis
89-77-0
50419-88-0
2-Amino-4-chlorobenzoic acid (I; 20.00 g, 116.6 mmol) and acetonitrile (300 mL) were added to a 500 mL single-necked round-bottomed flask with rapid stirring to form a beige-colored suspension. At room temperature, N-bromosuccinimide (NBS; 20.75 g, 116.6 mmol) was added slowly in batches. After addition, the reaction mixture was continued to be stirred for 1 hour. Subsequently, the reaction mixture was placed in a 45 °C water bath and the solvent was removed by rotary evaporation. Water was added to the residue, stirred and the filter cake was washed by filtration. Finally, the product was dried under vacuum at 60 °C to afford 2-amino-5-bromo-4-chlorobenzoic acid (II; 28.62 g, 98% yield).
References
[1] Patent: CN106986809, 2017, A. Location in patent: Paragraph 0024; 0025; 0026; 0027; 0028; 0029; 0030
[2] Patent: CN106966914, 2017, A. Location in patent: Paragraph 0019; 0020; 0028; 0029; 0036; 0037
[3] Patent: US2015/119405, 2015, A1. Location in patent: Paragraph 0407; 0408; 0409
[4] Patent: WO2005/54238, 2005, A1. Location in patent: Page/Page column 70
[5] Organic and Biomolecular Chemistry, 2014, vol. 12, # 27, p. 5031 - 5037
BUTTPARK 80\07-66 Preparation Products And Raw materials
Raw materials
Preparation Products
BUTTPARK 80\07-66 Suppliers
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