METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE

Product Name: METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE
CAS No.: 550998-53-3
Chemical Name: METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE
Synonyms: METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE;7-Bromo-benzo[b]thiophene-2-carboxylic acid methyl ester;Benzo[b]thiophene-2-carboxylic acid, 7-bromo-, methyl ester
CBNumber: CB2798383
Molecular Formula: C10H7BrO2S
Formula Weight: 271.13
MOL File: Mol file

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METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE Property

Melting point:: 99-102°C
storage temp.: 2-8°C(protect from light)
form: solid
color: Off-white

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2934999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

SynQuest Laboratories

Product number: 6H23-9-05
Product name: Methyl 7-bromobenzo[b]thiophene-2-carboxylate
Packaging: 1g
Price: $104
Updated: 2021/12/16

Matrix Scientific

Product number: 047092
Product name: Methyl 7-bromo-1-benzothiophene-2-carboxylate
Purity: >95%
Packaging: 500mg
Price: $109
Updated: 2021/12/16

Matrix Scientific

Product number: 047092
Product name: Methyl 7-bromo-1-benzothiophene-2-carboxylate
Purity: >95%
Packaging: 1g
Price: $145
Updated: 2021/12/16

AK Scientific

Product number: 8024AB
Product name: Methyl7-bromobenzo[b]thiophene-2-carboxylate
Packaging: 250mg
Price: $154
Updated: 2021/12/16

AK Scientific

Product number: 8024AB
Product name: Methyl7-bromobenzo[b]thiophene-2-carboxylate
Packaging: 1g
Price: $176
Updated: 2021/12/16

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METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

149947-15-9

2365-48-2

550998-53-3

GENERAL METHOD: Under stirring conditions, 3-bromo-2-fluorobenzaldehyde (9.90 mmol) was dissolved in DMF (20 mL) and methyl mercaptoacetate (10.9 mmol) and potassium carbonate (39.6 mmol) were added sequentially. The reaction mixture was stirred continuously at 60 °C for 15 hours. After completion of the reaction, the DMF solvent was removed by distillation under reduced pressure. Water (50 mL) was added to the residue, which was subsequently extracted with ethyl acetate (2 x 40 mL). The organic phases were combined, dried with anhydrous sodium sulfate, filtered, and concentrated under reduced pressure to remove the solvent to afford the target product, methyl 7-bromobenzo[b]thiophene-2-carboxylate.

References

[1] European Journal of Medicinal Chemistry, 2017, vol. 125, p. 538 - 550
[2] Patent: KR2015/117318, 2015, A. Location in patent: Paragraph 0181; 0187; 0188; 0189

METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE Suppliers

China 45 India 1 United Kingdom 2 United States 7 Global 55

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550998-53-3, METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATERelated Search:

Coumarin 7-BROMO-ISOQUINOLIN-1-YLAMINE 7-BROMO-1-CHLOROISOQUINOLINE 7-BROMO-1-HYDROXYISOQUINOLINE 7-BROMO-1-METHYL-1H-INDAZOLE

METHYL 7-BROMO-1-BENZOTHIOPHENE-2-CARBOXYLATE

7-Bromo-benzo[b]thiophene-2-carboxylic acid methyl ester

Benzo[b]thiophene-2-carboxylic acid, 7-bromo-, methyl ester

550998-53-3