2-BROMO-4-METHYLQUINOLINE

Product Name: 2-BROMO-4-METHYLQUINOLINE
CAS No.: 64658-04-4
Chemical Name: 2-BROMO-4-METHYLQUINOLINE
Synonyms: 2-BROMO-4-METHYLQUINOLINE;Quinoline, 2-bromo-4-methyl-;2-Bromo-4-methylquinoline, 97%, QP-5147
CBNumber: CB2838223
Molecular Formula: C10H8BrN
Formula Weight: 222.08
MOL File: 64658-04-4.mol

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2-BROMO-4-METHYLQUINOLINE Property

Melting point:: 81-81.5 °C
Boiling point:: 125-126 °C(Press: 1 Torr)
Density: 1.488±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.15±0.50(Predicted)
Appearance: Brown to reddish brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B405275
Product name: 2-Bromo-4-methylquinoline
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B405275
Product name: 2-Bromo-4-methylquinoline
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB40676
Product name: 2-Bromo-4-methylQuinoline
Packaging: 250mg
Price: $85
Updated: 2021/12/16

AK Scientific

Product number: Y9715
Product name: 2-Bromo-4-methylquinoline
Packaging: 250mg
Price: $122
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB40676
Product name: 2-Bromo-4-methylQuinoline
Packaging: 500mg
Price: $125
Updated: 2021/12/16

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2-BROMO-4-METHYLQUINOLINE Chemical Properties,Usage,Production

Synthesis

4053-40-1

64658-04-4

General method: To a stirred solution of 4-methylquinoline-N-oxide (0.1 M) in anhydrous CH2Cl2 was added POBr3 (1.2 eq.) under argon protection at 0 °C, followed by dropwise addition of DMF (0.5 eq.). The reaction mixture was gradually warmed to 25 °C and stirred continuously for several hours until TLC showed that the reaction was complete. Saturated aqueous sodium carbonate solution was slowly added to the reaction mixture and the pH was adjusted to 7-8. The mixture was separated and the aqueous phase was thoroughly extracted with CH2Cl2. The organic phases were combined, washed with brine, dried with Na2SO4, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography with PE/EA (100:1) as eluent.

References

[1] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768

2-BROMO-4-METHYLQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-METHYLQUINOLINE Suppliers

China 50 Germany 1 India 1 United Kingdom 2 United States 9 Global 63

Baiyin Chengze Chemical Technology Co., Ltd.

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View Lastest Price from 2-BROMO-4-METHYLQUINOLINE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-bromo-4-methylquinoline 64658-04-4
Price: US $1.60-9.60/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-20

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-BROMO-4-METHYLQUINOLINE 64658-04-4
Price: US $30.00-10.00/KG
Min. Order: 50KG
Purity: 99%
Supply Ability: 500000kg
Release date: 2024-10-24

64658-04-4, 2-BROMO-4-METHYLQUINOLINERelated Search:

2-Methylnaphthalene 2-BROMOQUINOLINE-4-CARBOXYLIC ACID 2-BROMO-4-(TRIFLUOROMETHYL)QUINOLINE-8-CARBOXYLIC ACID 2-BROMOQUINOLINE-4-CARBOXALDEHYDE 2-Bromo-6-fluoro-4-(trifluoromethyl)quinoline 2-BROMO-4-(TRIFLUOROMETHYL)QUINOLINE 2-BROMO-8-IODO-4-(TRIFLUOROMETHYL)QUINOLINE 2-BROMO-4-CYANOQUINOLINE 2-BROMO-4-(TRIFLUOROMETHYL)QUINOLINE-3-CARBOXYLIC ACID 2-BROMO-4-METHYLQUINOLINE

2-BROMO-4-METHYLQUINOLINE

Quinoline, 2-bromo-4-methyl-

2-Bromo-4-methylquinoline, 97%, QP-5147

64658-04-4