2-BROMO-4-METHYLQUINOLINE
- Product Name
- 2-BROMO-4-METHYLQUINOLINE
- CAS No.
- 64658-04-4
- Chemical Name
- 2-BROMO-4-METHYLQUINOLINE
- Synonyms
- 2-BROMO-4-METHYLQUINOLINE;Quinoline, 2-bromo-4-methyl-;2-Bromo-4-methylquinoline, 97%, QP-5147
- CBNumber
- CB2838223
- Molecular Formula
- C10H8BrN
- Formula Weight
- 222.08
- MOL File
- 64658-04-4.mol
2-BROMO-4-METHYLQUINOLINE Property
- Melting point:
- 81-81.5 °C
- Boiling point:
- 125-126 °C(Press: 1 Torr)
- Density
- 1.488±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 1.15±0.50(Predicted)
- Appearance
- Brown to reddish brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- B405275
- Product name
- 2-Bromo-4-methylquinoline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B405275
- Product name
- 2-Bromo-4-methylquinoline
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FB40676
- Product name
- 2-Bromo-4-methylQuinoline
- Packaging
- 250mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- Y9715
- Product name
- 2-Bromo-4-methylquinoline
- Packaging
- 250mg
- Price
- $122
- Updated
- 2021/12/16
- Product number
- FB40676
- Product name
- 2-Bromo-4-methylQuinoline
- Packaging
- 500mg
- Price
- $125
- Updated
- 2021/12/16
2-BROMO-4-METHYLQUINOLINE Chemical Properties,Usage,Production
Synthesis
4053-40-1
64658-04-4
General method: To a stirred solution of 4-methylquinoline-N-oxide (0.1 M) in anhydrous CH2Cl2 was added POBr3 (1.2 eq.) under argon protection at 0 °C, followed by dropwise addition of DMF (0.5 eq.). The reaction mixture was gradually warmed to 25 °C and stirred continuously for several hours until TLC showed that the reaction was complete. Saturated aqueous sodium carbonate solution was slowly added to the reaction mixture and the pH was adjusted to 7-8. The mixture was separated and the aqueous phase was thoroughly extracted with CH2Cl2. The organic phases were combined, washed with brine, dried with Na2SO4, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by fast column chromatography with PE/EA (100:1) as eluent.
References
[1] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768
2-BROMO-4-METHYLQUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
2-BROMO-4-METHYLQUINOLINE Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 2-BROMO-4-METHYLQUINOLINE manufacturers
- Product
- 2-bromo-4-methylquinoline 64658-04-4
- Price
- US $1.60-9.60/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-20
- Product
- 2-BROMO-4-METHYLQUINOLINE 64658-04-4
- Price
- US $30.00-10.00/KG
- Min. Order
- 50KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-10-24