ChemicalBook > CAS DataBase List > Aprindine

Aprindine

Product Name
Aprindine
CAS No.
37640-71-4
Chemical Name
Aprindine
Synonyms
AC-1802;aprindin;Aprindine;aprinidine;Lilly-83846;Aprindine USP/EP/BP;3-(diethylamino)propyl-indan-2-yl-phenyl-amine;N,N'-Diethyl-N'-2-indanyl-N'-phenyl-1,3-Prop-anediamine;n-(2,3-dihydro-1h-inden-2-yl)-n',n'-diethyl-n-phenyl-3-propanediamine;n-(2,3-dihydro-1h-inden-2-yl)-n',n'-diethyl-n-phenyl-1,3-propanediamine
CBNumber
CB2875279
Molecular Formula
C22H30N2
Formula Weight
322.49
MOL File
37640-71-4.mol
More
Less

Aprindine Property

Melting point:
120-121 °C
Boiling point:
450.9±45.0 °C(Predicted)
Density 
1.046±0.06 g/cm3(Predicted)
pka
pKa 4.53 (H2O) (Uncertain);10.16(H2O) (Uncertain)
More
Less

Hazard and Precautionary Statements (GHS)

More
Less

N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
API0009102
Product name
APRINDINE
Purity
95.00%
Packaging
5MG
Price
$504.56
Updated
2021/12/16
More
Less

Aprindine Chemical Properties,Usage,Production

Originator

Amidonal,Madaus,W. Germany,1976

Uses

depressant (anti-arrhythmic).

Definition

ChEBI: Aprindine is a member of indanes.

Manufacturing Process

104.6 g (0.5 mol) N-phenyl-2-aminoindane and 2.5 liters benzene are introduced into a reaction vessel of 5 liters, under an atmosphere of nitrogen. 37 g (0.95 mol) sodium amide are added and the mixture is stirred during 3 hours at room temperature.
119.7 g (0.8 mol) of γ-chloropropyl diethylamine are then quickly added. After agitation during 1 hour at room temperature, the reaction mixture is refluxed and stirred under nitrogen during 21 hours. The mixture is then allowed to cool and poured onto ice. The obtained aqueous phase is extracted by means of 500 cm3 of benzene. The benzene extract is washed two times with 200 cm3 of water and the benzene is then evaporated.
The residue is treated with 500 cm3 of hydrochloric acid (2 N). The obtained solution is evaporated to dryness and the oily residue is recrystallized from ethanol. 176.9 g (yield 89.4%) of dihydrochloride of N-phenyl-Ndiethylaminopropyl- 2-aminoindane are obtained, MP 208° to 210°C.
The dihydrochloride is converted into monohydrochloride by dissolving 26.36 g (0.066 mol) of dihydrochloride into 158 cm3 of water, adding drop by drop a suitable amount (0.066 mol) of caustic soda (1 N), evaporating the aqueous solution to dryness, drying by means of benzene, filtering the formed sodium chloride (3.8 g) and crystallizing the cooled obtained benzene solution. 22.6 g (95%) of monohydrochloride are obtained, MP 120° to 121°C.

brand name

Fibocil (Lilly).

Therapeutic Function

Antiarrhythmic

Side effects

Aprindine has a sustained activity. Because of serious side effects (agranulocytosis), aprindine should only be used for life-threatening arrhythmias otherwise refractory to therapy .

Aprindine Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

Aprindine Suppliers

Wuhan Magic Biological Technology Co., Ltd.
Tel
18872289958、027-52304252、3400508168
Fax
027-52304252
Email
3400508168@qq.com
Country
China
ProdList
1910
Advantage
55
Dideu Industries Group Limited
Tel
+86-29-89586680 +86-15129568250
Email
1026@dideu.com
Country
China
ProdList
22883
Advantage
58
Hubei Jusheng Technology Co.,Ltd.
Tel
18871490254
Fax
027-59599243
Email
linda@hubeijusheng.com
Country
CHINA
ProdList
28172
Advantage
58
QUALITY CONTROL SOLUTIONS LTD.
Tel
0755-66853366; 13670046396
Email
ORDERS@QCSRM.COM
Country
China
ProdList
24326
Advantage
58
Shaanxi Xihua Chemical Industry Co., Ltd
Tel
17691182729 15529505138
Email
1021@dideu.com
Country
China
ProdList
9969
Advantage
58
Shanghai Trustin Chemical Co., Ltd
Tel
--
Fax
--
Email
sales@etrustin.com
Country
China
ProdList
5362
Advantage
51
Xingtai Yancheng Chemical Auxiliaries Co., Ltd
Tel
--
Fax
--
Email
15933711390@163.com
Country
China
ProdList
107
Advantage
50
Shanghai New Union Textra Import & Export Co., Ltd
Tel
--
Fax
--
Email
zhou@pharmchemical.com
Country
China
ProdList
2748
Advantage
60
Yick-Vic Chemicals & Pharmaceuticals (HK) Ltd
Tel
--
Fax
--
Email
sales@yickvic.com
Country
China
ProdList
6206
Advantage
58
More
Less

View Lastest Price from Aprindine manufacturers

Dideu Industries Group Limited
Product
Aprindine
Price
US $1.10/g
Min. Order
1g
Purity
99.9%
Supply Ability
100 Tons min
Release date
2021-08-11

37640-71-4, AprindineRelated Search:


  • Aprindine
  • aprindin
  • aprinidine
  • n-(2,3-dihydro-1h-inden-2-yl)-n',n'-diethyl-n-phenyl-1,3-propanediamine
  • n-(2,3-dihydro-1h-inden-2-yl)-n',n'-diethyl-n-phenyl-3-propanediamine
  • N,N'-Diethyl-N'-2-indanyl-N'-phenyl-1,3-Prop-anediamine
  • AC-1802
  • Lilly-83846
  • N,N-Diethyl-N'-(2,3-dihydro-1H-inden-2-yl)-N'-phenyl-1,3-propanediamine
  • 3-(diethylamino)propyl-indan-2-yl-phenyl-amine
  • N-(2,3-dihydro-1H-inden-2-yl)-N',N'-diethyl-N-phenyl-propane-1,3-diamine
  • N-(2,3-dihydro-1H-inden-2-yl)-N',N'-diethyl-N-phenylpropane-1,3-diamine
  • Aprindine USP/EP/BP
  • 1,3-Propanediamine, N1-(2,3-dihydro-1H-inden-2-yl)-N3,N3-diethyl-N1-phenyl-
  • 37640-71-4