2-bromo-3-methylacetophenone

Product Name: 2-bromo-3-methylacetophenone
CAS No.: 51012-64-7
Chemical Name: 2-bromo-3-methylacetophenone
Synonyms: 2-Bromo-1-(m-tolyl);Zolpidem Impurity 37;Zolpidem Acid Impurity 6;2-bromo-3-methylacetophenone;2-Bromo-1-(m-tolyl)ethan-1-one;2-bromo-1-(3-methylphenyl)ethanone;Ethanone, 2-broMo-1-(3-Methylphenyl)-;2-broMo-1-(3-Methylphenyl)ethan-1-one
CBNumber: CB2947152
Molecular Formula: C9H9BrO
Formula Weight: 213.07
MOL File: 51012-64-7.mol

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2-bromo-3-methylacetophenone Property

Boiling point:: 120-122 °C(Press: 1.5 Torr)
Density: 1.416±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Colorless to light yellow ＜47℃ Solid,＞48℃ Liquid
InChI: InChI=1S/C9H9BrO/c1-7-3-2-4-8(5-7)9(11)6-10/h2-5H,6H2,1H3
InChIKey: BANFRNTVKCHZDE-UHFFFAOYSA-N
SMILES: C(=O)(C1=CC=CC(C)=C1)CBr

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H304May be fatal if swallowed and enters airways

Precautionary statements

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P331Do NOT induce vomiting.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

TRC

Product number: B614805
Product name: 2-Bromo-1-(m-tolyl)ethanone
Packaging: 500mg
Price: $350
Updated: 2021/12/16

Matrix Scientific

Product number: 144361
Product name: 2-Bromo-1-(3-methylphenyl)ethanone
Purity: 95%
Packaging: 1g
Price: $385
Updated: 2021/12/16

AK Scientific

Product number: 7064AB
Product name: 2-Bromo-1-(m-tolyl)ethanone
Packaging: 5g
Price: $640
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0011209
Product name: 2-BROMO-3'-METHYLACETOPHENONE
Purity: 95.00%
Packaging: 1G
Price: $808.89
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0011209
Product name: 2-BROMO-3'-METHYLACETOPHENONE
Purity: 95.00%
Packaging: 2.5G
Price: $1147.43
Updated: 2021/12/16

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2-bromo-3-methylacetophenone Chemical Properties,Usage,Production

Synthesis

33675-43-3

51012-64-7

General procedure for the synthesis of 2-bromo-1-(3-methylphenyl)ethyl-1-one from 1-(bromoethynyl)-3-methylbenzene: A mixed solution of 1-(bromoethynyl)-3-methylbenzene (0.5 mmol), AgF (5 mol%), and water (1 eq.) in TFA (1 mL) was stirred and reacted for 6 hours at 40 °C. Upon completion of the reaction, the TFA was recovered by distillation for reuse. The reaction mixture was purified by column chromatography to afford the target product 2-bromo-1-(3-methylphenyl)ethyl-1-one.

References

[1] European Journal of Organic Chemistry, 2016, vol. 2016, # 1, p. 116 - 121
[2] Tetrahedron Letters, 2014, vol. 55, # 7, p. 1373 - 1375
[3] Journal of Organic Chemistry, 2013, vol. 78, # 18, p. 9190 - 9195
[4] Tetrahedron Letters, 2016, vol. 57, # 45, p. 4983 - 4986
[5] Tetrahedron, 2016, vol. 72, # 27-28, p. 3818 - 3822

2-bromo-3-methylacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

3-M-TOLYL-ISOXAZOL-5-YLAMINE

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2-bromo-3-methylacetophenone Suppliers

China 69 Europe 2 Germany 1 India 1 United Kingdom 2 United States 8 Global 83

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51012-64-7, 2-bromo-3-methylacetophenone Related Search:

2-bromo-2-methylacetophenone 2,2-DIBROMO-1-P-TOLYLETHANONE Zolpidem Impurity 29 Zolpidem Impurity 18 Methyl 6-methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine-3-acetate Tolyloyl propionamide 8-methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine Zolpidem Impurity 31 Zolpidem Impurity 35 6-Methyl-2-(4-methylphenyl)imidazol[1,2-a]-pyridine-3-acetic acid Benzenebutanamide, β-bromo-N,N,4-trimethyl-γ-oxo- Zolpidem Impurity 46 Hydroxy[6-methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridin-3-yl]acetic acid Zolpidem Impurity 38 7-methyl-2-(p-tolyl)imidazo[1,2-a]pyridine 6-Methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine Zolpidem tartrate 6-Methyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine-3-acetamide

2-bromo-3-methylacetophenone

2-broMo-1-(3-Methylphenyl)ethan-1-one

Ethanone, 2-broMo-1-(3-Methylphenyl)-

2-Bromo-1-(m-tolyl)

2-bromo-1-(3-methylphenyl)ethanone

Zolpidem Acid Impurity 6

Zolpidem Impurity 37

2-Bromo-1-(m-tolyl)ethan-1-one

51012-64-7

Adehydes, Acetals & Ketones

Bromine Compounds