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tert-Butyl 3-(methylamino)propylcarbamate

Product Name
tert-Butyl 3-(methylamino)propylcarbamate
CAS No.
442514-22-9
Chemical Name
tert-Butyl 3-(methylamino)propylcarbamate
Synonyms
N-Boc-3-(methylamino)propanamine;Boc-3-methylamino-propylcarbamate;3-N-Boc-N1-methylpropane-1,3-diamine;Boc-3-MethylaMino-propylcarbaMate HCl;1-BOC-AMINO-3-METHYLAMINO-PROPANE-HCl;tert-Butyl 3-(methylamino)propylcarbamate;Tert-butyl N-[3-(MethylaMino)propyl]carbaMate;(3-Methylamino-propyl)-carbamic acid tert-butyl ester;Carbamic acid, N-[3-(methylamino)propyl]-, 1,1-dimethylethyl ester
CBNumber
CB2970930
Molecular Formula
C9H20N2O2
Formula Weight
188.27
MOL File
442514-22-9.mol
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tert-Butyl 3-(methylamino)propylcarbamate Property

Boiling point:
280.3±23.0 °C(Predicted)
Density 
0.949±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
12.82±0.46(Predicted)
Appearance
Colorless to light yellow Liquid
InChI
InChI=1S/C9H20N2O2/c1-9(2,3)13-8(12)11-7-5-6-10-4/h10H,5-7H2,1-4H3,(H,11,12)
InChIKey
YIMSPDZAVBIXRT-UHFFFAOYSA-N
SMILES
C(OC(C)(C)C)(=O)NCCCNC
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Safety

HS Code 
2924297099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
T205808
Product name
tert-Butyl3-(Methylamino)propylcarbamate
Packaging
100mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-B0432
Product name
Boc-3-methylamino-propylcarbamate
Purity
≥97.0%
Packaging
1g
Price
$52
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB139798
Product name
tert-Butyl (3-(methylamino)propyl)carbamate
Packaging
100mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB139798
Product name
tert-Butyl (3-(methylamino)propyl)carbamate
Packaging
250mg
Price
$110
Updated
2021/12/16
ChemScene
Product number
CS-B0432
Product name
Boc-3-methylamino-propylcarbamate
Purity
≥97.0%
Packaging
5g
Price
$173
Updated
2021/12/16
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tert-Butyl 3-(methylamino)propylcarbamate Chemical Properties,Usage,Production

Synthesis

1158721-71-1

442514-22-9

The general procedure for the synthesis of tert-butyl 2-(methylamino)propylcarbamate using the compound (CAS:1158721-71-1) as starting material was as follows: compound 20 (12 g, 0.037 mol) was dissolved in 100 mL of methanol and 0.5 g of 5% Pd/C catalyst was added. The hydrogenation reaction was carried out at 60 psi hydrogen pressure for 45 minutes. Upon completion of the reaction, the catalyst was removed by filtration and the solvent was removed by distillation under reduced pressure to afford the target product tert-butyl 2-(methylamino)propylcarbamate as a colorless oil (6 g, 65% yield).

References

[1] Patent: US2009/137618, 2009, A1. Location in patent: Page/Page column 12-13

tert-Butyl 3-(methylamino)propylcarbamate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from tert-Butyl 3-(methylamino)propylcarbamate manufacturers

Career Henan Chemical Co
Product
tert-Butyl 3-(methylamino)propylcarbamate 442514-22-9
Price
US $6.68/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg-1000kg
Release date
2020-01-10

442514-22-9, tert-Butyl 3-(methylamino)propylcarbamateRelated Search:

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  • Boc-3-MethylaMino-propylcarbaMate HCl
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  • 442514-22-9