tert-Butyl 3-(methylamino)propylcarbamate
- Product Name
- tert-Butyl 3-(methylamino)propylcarbamate
- CAS No.
- 442514-22-9
- Chemical Name
- tert-Butyl 3-(methylamino)propylcarbamate
- Synonyms
- N-Boc-3-(methylamino)propanamine;Boc-3-methylamino-propylcarbamate;3-N-Boc-N1-methylpropane-1,3-diamine;Boc-3-MethylaMino-propylcarbaMate HCl;1-BOC-AMINO-3-METHYLAMINO-PROPANE-HCl;tert-Butyl 3-(methylamino)propylcarbamate;Tert-butyl N-[3-(MethylaMino)propyl]carbaMate;(3-Methylamino-propyl)-carbamic acid tert-butyl ester;Carbamic acid, N-[3-(methylamino)propyl]-, 1,1-dimethylethyl ester
- CBNumber
- CB2970930
- Molecular Formula
- C9H20N2O2
- Formula Weight
- 188.27
- MOL File
- 442514-22-9.mol
tert-Butyl 3-(methylamino)propylcarbamate Property
- Boiling point:
- 280.3±23.0 °C(Predicted)
- Density
- 0.949±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 12.82±0.46(Predicted)
- Appearance
- Colorless to light yellow Liquid
- InChI
- InChI=1S/C9H20N2O2/c1-9(2,3)13-8(12)11-7-5-6-10-4/h10H,5-7H2,1-4H3,(H,11,12)
- InChIKey
- YIMSPDZAVBIXRT-UHFFFAOYSA-N
- SMILES
- C(OC(C)(C)C)(=O)NCCCNC
Safety
- HS Code
- 2924297099
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- T205808
- Product name
- tert-Butyl3-(Methylamino)propylcarbamate
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- CS-B0432
- Product name
- Boc-3-methylamino-propylcarbamate
- Purity
- ≥97.0%
- Packaging
- 1g
- Price
- $52
- Updated
- 2021/12/16
- Product number
- FB139798
- Product name
- tert-Butyl (3-(methylamino)propyl)carbamate
- Packaging
- 100mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- FB139798
- Product name
- tert-Butyl (3-(methylamino)propyl)carbamate
- Packaging
- 250mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- CS-B0432
- Product name
- Boc-3-methylamino-propylcarbamate
- Purity
- ≥97.0%
- Packaging
- 5g
- Price
- $173
- Updated
- 2021/12/16
tert-Butyl 3-(methylamino)propylcarbamate Chemical Properties,Usage,Production
Synthesis
1158721-71-1
442514-22-9
The general procedure for the synthesis of tert-butyl 2-(methylamino)propylcarbamate using the compound (CAS:1158721-71-1) as starting material was as follows: compound 20 (12 g, 0.037 mol) was dissolved in 100 mL of methanol and 0.5 g of 5% Pd/C catalyst was added. The hydrogenation reaction was carried out at 60 psi hydrogen pressure for 45 minutes. Upon completion of the reaction, the catalyst was removed by filtration and the solvent was removed by distillation under reduced pressure to afford the target product tert-butyl 2-(methylamino)propylcarbamate as a colorless oil (6 g, 65% yield).
References
[1] Patent: US2009/137618, 2009, A1. Location in patent: Page/Page column 12-13
tert-Butyl 3-(methylamino)propylcarbamate Preparation Products And Raw materials
Raw materials
Preparation Products
tert-Butyl 3-(methylamino)propylcarbamate Suppliers
- Tel
- --
- Fax
- --
- Country
- Europe
- ProdList
- 1780
- Advantage
- 38
View Lastest Price from tert-Butyl 3-(methylamino)propylcarbamate manufacturers
- Product
- tert-Butyl 3-(methylamino)propylcarbamate 442514-22-9
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-10