ChemicalBook > CAS DataBase List > 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER

5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER

Product Name: 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER
CAS No.: 30766-12-2
Chemical Name: 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER
Synonyms: H57157;methyl 5-hydroxypicolinate;Methyl 5-hydroxypyridine-...;Methyl 5-hydroxy-2-picolinate;Methyl 5-hydroxypyridine-2-ca;Methyl 5-hydroxypyridine-2-carboxylate;5-HDROXY-PYRIDINE-2-CARBOXYLIC ACID METHY;Methyl 5-hydroxypyridine-2-carboxylate ,97%;Methyl 5-hydroxypyridine-2-carboxylate 95+%;5-Hydroxy-2-pyridinecarboxylic acid methyl ester
CBNumber: CB31010807
Molecular Formula: C7H7NO3
Formula Weight: 153.14
MOL File: 30766-12-2.mol

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5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER Property

Melting point:: 193.5-195.5℃
Boiling point:: 374.2±22.0 °C(Predicted)
Density: 1.287±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
form: solid
pka: 8.29±0.10(Predicted)
color: Pale yellow

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Safety

Risk Statements: 20/21/22
Safety Statements: 24/25-36/37
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B585303
Product name: methyl5-hydroxypyridine-2-carboxylate
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Usbiological

Product number: 455730
Product name: methyl 5-hydroxypyridine-2-carboxylate
Packaging: 100mg
Price: $305
Updated: 2021/12/16

Apolloscientific

Product number: OR51766
Product name: Methyl5-hydroxypyridine-2-carboxylate
Purity: 95+%
Packaging: 1g
Price: $47
Updated: 2021/12/16

ChemScene

Product number: CS-W005963
Product name: Methyl5-hydroxypyridine-2-carboxylate
Purity: 99.76%
Packaging: 1g
Price: $50
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-1-W8
Product name: Methyl 5-hydroxypyridine-2-carboxylate
Purity: 95.0%
Packaging: 1g
Price: $52
Updated: 2021/12/16

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5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production

Chemical Properties

Yellow solid

Uses

Methyl 5-hydroxypyridine-2-carboxylate is a phenolic acid that can found in the stems of Mahonia fortune. Methyl 5-hydroxypyridine-2-carboxylate exhibits NO inhibitory effects in vitro[1].

Synthesis

67-56-1

15069-92-8

30766-12-2

1. add methanol (70 mL) to 5-hydroxypyridine-2-carboxylic acid (5.01 g, 36.0 mmol). 2. sulfuric acid (5.8 mL, 110 mmol) was added slowly and dropwise to the above mixture. 3. The reaction mixture was stirred overnight at 75 °C. 4. 4. Upon completion of the reaction, the solvent was removed by evaporation under reduced pressure. 5. 5. The residue was dissolved in ethyl acetate (EtOAc). 6. 6. Saturated aqueous sodium bicarbonate (NaHCO?) is added to the solution and the pH is adjusted to 3. 7. 7. The precipitate was collected by filtration and dried under vacuum. 8. 8. The remaining aqueous phase was extracted with ethyl acetate. 9. The organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate (Na?SO?). 10. The organic phases were concentrated under pressure to give the solid product methyl 5-hydroxy-2-pyridinecarboxylate (5.3 g, 96% yield), which could be used for subsequent reactions without further purification. 11. LCMS analysis: calculated value C?H?NO?([M+H]?) m/z = 154.1; measured value: 154.1.

References

[1] Liu L, et, al. Simultaneous characterisation of multiple Mahonia fortunei bioactive compounds in rat plasma by UPLC-MS/MS for application in pharmacokinetic studies and anti-inflammatory activity in vitro. J Pharm Biomed Anal. 2020 Feb 5;179:113013. DOI:10.1016/j.jpba.2019.113013

5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER 30766-12-2
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-14

Career Henan Chemical Co

Product: 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER 30766-12-2
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 200KG
Release date: 2018-12-23

30766-12-2, 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTERRelated Search:

tert-butyl 5-hydroxy-2-azabicyclo[2.2.1]heptane-2-carboxylate TERT-BUTYL 5-HYDROXYHEXAHYDRO-1H-ISOINDOLE-2(3H)-CARBOXYLATE 5-Hydroxypyrimidine METHYL-5-METHOXY-2-METHYLBENZOATE 1,2,3,4-TETRAHYDRO-ISOQUINOLIN-5-OL 5-HYDROXY-2H-1,4-BENZOXAZIN-3(4H)-ONE 5-HYDROXY-3,4-DIHYDRO-2H-ISOQUINOLIN-1-ONE Ethyl 5-hydroxypyrazine-2-carboxylate 5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER methyl 6-bromo-5-hydroxy-2-pyridinecarboxylate Picolinic acid, 5-(p-chlorophenoxy)-, 5-indanyl ester methyl 5-(allyloxy)-6-bromo-2-pyridinecarboxylate 2-Pyridinecarboxylic acid, 5-(2-(trifluoromethyl)phenoxy)-, 2,3-dihydr o-1H-inden-5-yl ester METHYL 2-BENZYL-7-HYDROXY-1,3-DIOXO-2,3-DIHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-4-CARBOXYLATE Methyl 6-amino-5-hydroxy-2-pyridinecarboxylate methyl 6-bromo-5-[(3-methylbenzyl)oxy]-2-pyridinecarboxylate methyl 6-bromo-5-methoxy-2-pyridinecarboxylate Methyl 5,6-dihydroxypicolinate

Methyl 5-hydroxypyridine-2-carboxylate 95+%

H57157

Methyl 5-hydroxypyridine-2-carboxylate ,97%

Methyl 5-hydroxypyridine-2-carboxylate

5-Hydroxy-2-pyridinecarboxylic acid methyl ester

Methyl 5-hydroxypyridine-...

Methyl 5-hydroxypicolinate, 5-Hydroxy-2-(methoxycarbonyl)pyridine

methyl 5-hydroxypicolinate

2-Pyridinecarboxylic acid, 5-hydroxy-, methyl ester

5-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER ISO 9001：2015 REACH

5-HDROXY-PYRIDINE-2-CARBOXYLIC ACID METHY

2-Pyridinecarboxylic acid, 5-hydroxy-, methyl ester (9CI, ACI)

5-hydroxy-2-Pyridinecarboxylic acid methyl ester (9CI ACI)

Methyl 5-hydroxy-2-picolinate

Methyl 5hydroxypyridine2carboxylate,acid,Inhibitor,inhibit,Methyl 5 hydroxypyridine 2 carboxylate,phenolic

5-Hydroxy-pyridin-2-carboxylic acid methyl ester

Methyl 5-hydroxypyridine-2-ca

Methyl 5-hydroxypyridine-2-carboxylate, 10 mM in DMSO

30766-12-2