ChemicalBook > CAS DataBase List > 5-Pyrimidinemethanol, 2-amino- (9CI)

5-Pyrimidinemethanol, 2-amino- (9CI)

Product Name
5-Pyrimidinemethanol, 2-amino- (9CI)
CAS No.
120747-85-5
Chemical Name
5-Pyrimidinemethanol, 2-amino- (9CI)
Synonyms
2-Aminopyrimidine-5-methanol;2-AMINO-55PYRIMIDINEMETHANOL;2-Amino-5-pyrimidinemethanol;5-Pyrimidinemethanol, 2-amino-;(2-AMino-pyriMidin-5-yl)-Methanol;5-Pyrimidinemethanol, 2-amino- (9CI);5-Pyrimidinemethanol, 2-amino- (9CI) ISO 9001：2015 REACH
CBNumber
CB31082266
Molecular Formula
C5H7N3O
Formula Weight
125.13
MOL File
120747-85-5.mol
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5-Pyrimidinemethanol, 2-amino- (9CI) Property

Boiling point:
396.3±34.0 °C(Predicted)
Density 
1.360±0.06 g/cm3(Predicted)
storage temp. 
2-8°C(protect from light)
pka
13.36±0.10(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H225Highly Flammable liquid and vapour

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P241Use explosion-proof electrical/ventilating/lighting/…/equipment.

P242Use only non-sparking tools.

P243Take precautionary measures against static discharge.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
A629420
Product name
(2-Aminopyrimidin-5-yl)methanol
Packaging
500mg
Price
$265
Updated
2021/12/16
AK Scientific
Product number
3624AA
Product name
(2-Aminopyrimidin-5-yl)methanol
Packaging
1g
Price
$277
Updated
2021/12/16
Apolloscientific
Product number
OR345712
Product name
(2-Aminopyrimidin-5-yl)methanol
Packaging
1g
Price
$358
Updated
2021/12/16
SynQuest Laboratories
Product number
4H58-1-620
Product name
(2-Aminopyrimidin-5-yl)methanol
Packaging
1g
Price
$424
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0093401
Product name
2-AMINO-5-PYRIMIDINEMETHANOL
Purity
95.00%
Packaging
5MG
Price
$499.76
Updated
2021/12/16
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5-Pyrimidinemethanol, 2-amino- (9CI) Chemical Properties,Usage,Production

Synthesis

120747-84-4

120747-85-5

General procedure for the synthesis of (2-aminopyrimidin-5-yl)methanol from 2-amino-5-pyrimidinecarboxaldehyde: To a stirred solution of 2-amino-5-pyrimidinecarboxaldehyde (500 mg, 4.06 mmol) in methanol (6 mL) was added sodium borohydride (200 mg, 5.28 mmol) in batches. The reaction mixture was slowly warmed up to 0 °C, followed by returning to room temperature and continued stirring for 3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) (unfolding agent: dichloromethane solution in 5% methanol, Rf value 0.3). Upon completion of the reaction, the reaction was quenched by the addition of saturated aqueous ammonium chloride solution and the mixture was concentrated under reduced pressure. The residue was directly upsampled onto a short silica gel column (100-200 mesh) and eluted using a gradient from dichloromethane to a dichloromethane solution containing 7.5% methanol. The eluate containing the target product was collected and concentrated to give (2-aminopyrimidin-5-yl)methanol as a light yellow solid (340 mg, 67% yield). The product was confirmed by 1H NMR (400 MHz, DMSO-d6): δ 8.16 (s, 2H), 6.50 (br s, 2H), 4.99 (t, 1H), 4.26 (d, 2H).GCMS (m/z): 125.0.

References

[1] Patent: WO2016/193844, 2016, A1. Location in patent: Page/Page column 104
[2] Patent: US2005/187219, 2005, A1. Location in patent: Page/Page column 17
[3] Patent: WO2004/22561, 2004, A1. Location in patent: Page 94
[4] Patent: WO2004/831, 2003, A1. Location in patent: Page 24
[5] Patent: US2009/226398, 2009, A1

5-Pyrimidinemethanol, 2-amino- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Pyrimidinemethanol, 2-amino- (9CI) Suppliers

China 58 Europe 1 India 1 United Kingdom 1 United States 6 Global 67
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
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chenyj@titansci.com
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China
ProdList
14101
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59
Accela ChemBio Co.,Ltd.
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021-50795510 4000665055
Fax
021-50795055
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sales@accelachem.com
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China
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11035
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Shandong Xiya Chemical Co., Ltd
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4009903999 13355009207
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0539-6365991
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3007715519@qq.com
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China
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18729
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Shanghai Keepontech Co.,Ltd
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021-54849683 13601642561
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+86-21-54375689
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sales@keepontech.com
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China
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Bide Pharmatech Ltd.
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400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
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China
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39966
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Shanghai Jovan Biochemical Technology Co. Ltd.
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+86-021-61654350
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+86-021-61654350
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1245958370@qq.com
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China
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2982
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ShangHai Angti Biotechnology Co., Ltd.
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13764913901
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info@angtibio.com
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China
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4985
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Shanghai YuanYe Biotechnology Co., Ltd.
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021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
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60
Changzhou Hopschain Chemical Co.,Ltd.
Tel
0519-85528066 13775048983
Fax
0519-85528066
Email
sales@hopschem.com
Country
China
ProdList
31553
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Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
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China
ProdList
131957
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View Lastest Price from 5-Pyrimidinemethanol, 2-amino- (9CI) manufacturers

Dideu Industries Group Limited
Product
5-Pyrimidinemethanol, 2-amino- (9CI) 120747-85-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-14
Career Henan Chemical Co
Product
5-Pyrimidinemethanol, 2-amino- (9CI) 120747-85-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-09

120747-85-5, 5-Pyrimidinemethanol, 2-amino- (9CI)Related Search:

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  • 2-Amino-5-pyrimidinemethanol
  • (2-AMino-pyriMidin-5-yl)-Methanol
  • 5-Pyrimidinemethanol, 2-amino- (9CI)
  • 2-AMINO-55PYRIMIDINEMETHANOL
  • 2-Aminopyrimidine-5-methanol
  • 5-Pyrimidinemethanol, 2-amino-
  • 5-Pyrimidinemethanol, 2-amino- (9CI) ISO 9001：2015 REACH
  • 120747-85-5
  • PYRIMIDINE
  • AMINEPRIMARY