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ISOPROPAMIDE IODIDE

Product Name
ISOPROPAMIDE IODIDE
CAS No.
71-81-8
Chemical Name
ISOPROPAMIDE IODIDE
Synonyms
r79;isamid;darbid;5579md;skf4740;dipramid;priamide;sanulcin;Tyrimide;dipramide
CBNumber
CB3123931
Molecular Formula
C23H33IN2O
Formula Weight
480.43
MOL File
71-81-8.mol
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ISOPROPAMIDE IODIDE Property

Melting point:
199℃ (Decomposition)
Density 
1.2711 (estimate)
storage temp. 
Store at -20°C
solubility 
DMSO: 250 mg/mL (520.37 mM)
Water Solubility 
Practically insoluble in water
form 
powder to crystal
color 
White to Almost white
Merck 
14,5202
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
2
RTECS 
BP0693200
HS Code 
2924296000
Toxicity
LD50 oral in rat: > 10gm/kg
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
1350002
Product name
Isopropamide iodide
Purity
United States Pharmacopeia (USP) Reference Standard
Packaging
200mg
Price
$358
Updated
2024/03/01
TCI Chemical
Product number
I1048
Product name
Isopropamide Iodide
Purity
>95.0%(HPLC)(T)
Packaging
1g
Price
$33
Updated
2024/03/01
TCI Chemical
Product number
I1048
Product name
Isopropamide Iodide
Purity
>95.0%(HPLC)(T)
Packaging
5g
Price
$101
Updated
2024/03/01
TRC
Product number
I822775
Product name
Isopropamide iodide
Packaging
25mg
Price
$210
Updated
2021/12/16
Chem-Impex
Product number
37978
Product name
Isopropamideiodide,95%(HPLC)
Purity
95%(HPLC)
Packaging
1G
Price
$221.76
Updated
2021/12/16
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ISOPROPAMIDE IODIDE Chemical Properties,Usage,Production

Originator

Darbid,SKF,US,1957

Uses

Isopropamide Iodide acts as an anticholinergic compound with inhibitory activity. Also acts as a muscarinic receptor antagonist which can be applied to treatment of diseases affecting cognition including Alzheimer’s disease.

Uses

Isopropamide inhibits muscarinic action of acetylcholine on postganglionic parasympathetic effector regions. It is used for treating stomach ulcers and inflamed intestine.

Definition

ChEBI: Isopropamide iodide is a diarylmethane.

Manufacturing Process

γ-Diisopropylamino-α,α-diphenylbutyronitrile (60 g) was added in several portions to a mixture of sulfuric acid (150 ml) and water (15 ml) and the solution was heated 3% hours on the steam bath and then poured on ice and made basic with NH4OH. The γ-diisopropylamino-α,α-diphenylbutyramide precipitated as a solid, which was taken up in methylene chloride from an aqueous slurry. The methylene chloride was separated and dried by filtering through anhydrous K2CO3. The solvent was removed by distillation, leaving the amide which was crystallized from Skellysolve B five times and found then to have MP 87.0° to 88.5°C.
γ-Diisopropylamino-α,α-diphenylbutyramide in propanol was refluxed 4 hours in the presence of excess methyl iodide. Upon dilution of the solution with ethyl acetate (100 ml per 50 ml isopropyl alcohol) and cooling γ- diisopropylamino-α,α-diphenylbutyramide methiodide precipitated, was collected by filtration and recrystallized (9.0 g) by dissolving in a hot mixtureof 100 ml isopropyl alcohol and 10 ml methanol and then diluting with 90 ml Skellysolve B, to give 8.3 g recrystallized product, MP 182° to 184°C.

brand name

Darbid (GlaxoSmithKline).

Therapeutic Function

Spasmolytic

General Description

Isopropamide iodide, 3-carbamoyl-3,3-diphenylpropyl)diisopropylmethylammoniumiodide (Darbid), occurs as a bitter, white to pale yellow, crystallinepowder that is only sparingly soluble in water butfreely soluble in chloroform and alcohol.
This drug, introduced in 1957, is a potent anticholinergic,producing atropine-like effects peripherally. Even with itsquaternary nature, it does not cause sympathetic blockade atthe ganglionic level except at high dosages. Its principal distinguishingfeature is its long duration of action. A singledose can provide antispasmodic and antisecretory effects foras long as 12 hours.

Clinical Use

ISOPROPAMIDE IODIDE is used as adjunctive therapy in the treatment of pepticulcer and other conditions of the GI tract associated withhypermotility and hyperacidity. It has the usual side effectsof anticholinergics (dryness of mouth, mydriasis, difficulturination) and is contraindicated in glaucoma, prostatic hypertrophy,etc.

Synthesis

Isopropamide, (3-carbamoyl-3,3-diphenylpropyl)di-iso-propylmethyl ammonium iodide (14.1.25), is synthesized by alkylating diphenylacetonitrile with di-isopropylaminoethylchloride in the presence of sodium amide, and the subsequent hydrolysis of the nitrile group of the resulting compound (14.1.23) to an amide group (14.1.24). Alkylation of this compound with methyliodide gives isopropamide (14.1.25) [19¨C22].

ISOPROPAMIDE IODIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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ISOPROPAMIDE IODIDE Suppliers

Whyte Chemicals
Tel
--
Fax
--
Email
sales@whytechemicals.co.uk
Country
United Kingdom
ProdList
3748
Advantage
50
R.W. Unwin & Co. Ltd
Tel
--
Fax
--
Email
sales@rwunwin.co.uk
Country
United Kingdom
ProdList
238
Advantage
58
Sequoia Research Products Ltd
Tel
--
Fax
--
Country
United Kingdom
ProdList
466
Advantage
58
Sequoia Research Products Ltd.
Tel
--
Fax
--
Email
sales@seqchem.com
Country
United Kingdom
ProdList
3113
Advantage
69
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View Lastest Price from ISOPROPAMIDE IODIDE manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
IsopropaMide Iodide 71-81-8
Price
US $0.00/g
Min. Order
1g
Purity
98.0%
Supply Ability
1kg/month
Release date
2021-12-16
Shaanxi Dideu Medichem Co. Ltd
Product
ISOPROPAMIDE IODIDE 71-81-8
Price
US $0.10/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10
Release date
2024-08-04

71-81-8, ISOPROPAMIDE IODIDERelated Search:


  • LABOTEST-BB LT00772055
  • ISOPROPAMIDE
  • ISOPROPAMIDE IODIDE
  • (3-carbamoyl-3,3-diphenylpropyl)diisopropylmethyl-ammoniuiodide
  • (3-carbamoyl-3,3-diphenylpropyl)diisopropylmethylammoniumiodide
  • 2,2-diphenyl-4-diisopropylaminobutyramidemethiodide
  • 5579md
  • darbid
  • dipramid
  • dipramide
  • isamid
  • marygin-m
  • piaccamide
  • priamide
  • priazimide
  • r79
  • sanulcin
  • skf4740
  • Tyrimide
  • Isopropamide Iodide (200 mg)
  • Benzenepropanaminium, .gamma.-(aminocarbonyl)-N-methyl-N,N-bis(1-methylethyl)-.gamma.-phenyl-, iodide
  • ISOPROPAMIDEIODIDE,USP
  • (4-amino-4-oxo-3,3-diphenylbutyl)-methyl-di(propan-2-yl)azanium:iodide
  • 4-Amino-N,N-diisopropyl-N-methyl-4-oxo-3,3-diphenyl-1-butanaminium Iodide
  • Isopropamide Iodide (1350002)
  • RSYYIsopropamide Iodide
  • Inhibitor,peptic,inhibit,anticholinergic,long-acting,ulcer,hyperacidity,Isopropamide Iodide,gastrointestinal,hypermotility,Isopropamide
  • Benzenepropanaminium,g-(aminocarbonyl)-N-methyl-N,N-bis(1-methylethyl)-g-phenyl-,iodide(1:1)
  • 71-81-8
  • C23H33IN2O
  • C23H33N2OI
  • Analytical Chromatography Product Catalog
  • Analytical Standards
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  • DARBID