ChemicalBook > CAS DataBase List > TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE

TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE

Product Name: TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE
CAS No.: 1039055-46-3
Chemical Name: TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE
Synonyms: 5-Amino-2-(N-Boc-N-methylamino)pyridine;TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE;tert-butyl N-(5-aminopyridin-2-yl)-N-methylcarbamate;Carbamic acid, N-(5-amino-2-pyridinyl)-N-methyl-, 1,1-dimethylethyl ester
CBNumber: CB31265865
Molecular Formula: C11H17N3O2
Formula Weight: 223.27
MOL File: 1039055-46-3.mol

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TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Brown to dark brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: A602003
Product name: 5-Amino-2-(boc-aminomethyl)pyridine
Packaging: 50mg
Price: $200
Updated: 2021/12/16

Activate Scientific

Product number: AS27505
Product name: 5-Amino-2-(Boc-aminomethyl)pyridine
Purity: 97+%
Packaging: 100mg
Price: $68
Updated: 2021/12/16

Activate Scientific

Product number: AS27505
Product name: 5-Amino-2-(Boc-aminomethyl)pyridine
Purity: 97+%
Packaging: 250mg
Price: $148
Updated: 2021/12/16

Activate Scientific

Product number: AS27505
Product name: 5-Amino-2-(Boc-aminomethyl)pyridine
Purity: 97+%
Packaging: 1g
Price: $366
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0385394
Product name: TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE
Purity: 95.00%
Packaging: 5MG
Price: $505.64
Updated: 2021/12/16

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TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE Chemical Properties,Usage,Production

Synthesis

1039055-45-2

1039055-46-3

To a solution of methanol (25 mL) containing 0.40 g (1.58 mmol) of tert-butylmethyl (5-nitropyridin-2-yl) carbamate was added 0.4 g of 10% palladium/carbon catalyst. The reaction mixture was stirred under hydrogen atmosphere (40 g Hg pressure) for 4 hours. Upon completion of the reaction, the catalyst was removed by filtration through diatomaceous earth and the filtrate was concentrated to afford 0.36 g (97% yield) of 5-amino-2-(N-Boc-N-methylamino)pyridine, the product being a yellow oil. Its 1H NMR (DMSO-d6) data were as follows: δ 7.70 (dd, J = 2.9,0.5 Hz, 1H), 7.07 (d, J = 8.6 Hz, 1H), 6.93 (dd, J = 8.6,2.9 Hz, 1H), 3.12 (s, 3H), 1.39 (s, 9H).

References

[1] Patent: US2010/249099, 2010, A1. Location in patent: Page/Page column 97
[2] Patent: US2011/9405, 2011, A1. Location in patent: Page/Page column 54-55

TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE manufacturers

Career Henan Chemical Co

Product: TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE 1039055-46-3
Price: US $2.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: ask
Release date: 2020-01-08

1039055-46-3, TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATERelated Search:

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TERT-BUTYL-5-AMINOPYRIDIN-2-YLMETHYLCARBAMATE

tert-butyl N-(5-aminopyridin-2-yl)-N-methylcarbamate

Carbamic acid, N-(5-amino-2-pyridinyl)-N-methyl-, 1,1-dimethylethyl ester

5-Amino-2-(N-Boc-N-methylamino)pyridine

1039055-46-3

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