2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER

Product Name: 2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER
CAS No.: 391-93-5
Chemical Name: 2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER
Synonyms: UKRORGSYN-BB BBV-199988;2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER;Benzoic acid, 2-aMino-5-fluoro-, ethyl ester
CBNumber: CB31484286
Molecular Formula: C9H10FNO2
Formula Weight: 183.18
MOL File: 391-93-5.mol

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2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER Property

Boiling point:: 280.2±25.0 °C(Predicted)
Density: 1.218±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 2.09±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2922498590

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 4725CS
Product name: Ethyl2-amino-5-fluorobenzoate
Packaging: 1g
Price: $181
Updated: 2021/12/16

AK Scientific

Product number: 4725CS
Product name: Ethyl2-amino-5-fluorobenzoate
Packaging: 5g
Price: $431
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0101126
Product name: ETHYL 2-AMINO-5-FLUOROBENZOATE
Purity: 95.00%
Packaging: 5MG
Price: $502.78
Updated: 2021/12/16

Alichem

Product number: 391935
Product name: Ethyl2-amino-5-fluorobenzoate
Packaging: 500mg
Price: $847.6
Updated: 2021/12/16

Chemenu

Product number: CM252682
Product name: Ethyl2-amino-5-fluorobenzoate
Purity: 95+%
Packaging: 25g
Price: $916
Updated: 2021/12/16

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2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER Chemical Properties,Usage,Production

Synthesis

446-08-2

391-93-5

A. Synthesis of ethyl 2-amino-5-fluorobenzoate 2-Amino-5-fluorobenzoic acid (1.0 g, 6.4 mmol) was dissolved in a mixed solvent of ethanol (15 mL) and toluene (10 mL). Several drops of concentrated sulfuric acid (H2SO4) were added as a catalyst. A Dean-Stark splitter was installed and the reaction mixture was refluxed overnight. After completion of the reaction, it was cooled to room temperature and the solvent was removed by distillation under reduced pressure. The product was purified by silica gel column chromatography (4×15 cm), and the target product was obtained in 50% yield by sequential gradient elution with chloroform/methanol (98:2, v/v, 500 mL) and (95:5, v/v, 500 mL) as eluents. Mass spectrum (ES+): m/z 184.0 ([M+H]+); 1H NMR (CDCl3) δ 7.55 (d, 1H, ArH), 7.03 (m, 1H, ArH), 6.61 (dd, 1H, ArH), 5.6 (bs, 2H, NH2), 4.33 (q, 2H, CH2), 1.40 (t, 3H, CH3).

References

[1] Patent: US2003/69271, 2003, A1

2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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391-93-5, 2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTERRelated Search:

Butyl benzoate Hexyl benzoate 2-Amino-5-fluorobenzoic acid AURORA KA-2355 5-FLUORO-2-NITROBENZOIC ACID ETHYL ESTER 4,5-DIFLUORO-2-NITROBENZOIC ACID ETHYL ESTER 2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER 2-Amino-5-fluorobenzoic acid methyl ester

UKRORGSYN-BB BBV-199988

Benzoic acid, 2-aMino-5-fluoro-, ethyl ester

2-AMINO-5-FLUOROBENZOIC ACID ETHYL ESTER

391-93-5

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