2-METHOXY-5-METHYLBENZALDEHYDE

Product Name: 2-METHOXY-5-METHYLBENZALDEHYDE
CAS No.: 7083-19-4
Chemical Name: 2-METHOXY-5-METHYLBENZALDEHYDE
Synonyms: 5-Methyl-2-methoxybenzaldehyde;Benzaldehyde, 2-methoxy-5-methyl-
CBNumber: CB31489913
Molecular Formula: C9H10O2
Formula Weight: 150.17
MOL File: 7083-19-4.mol

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2-METHOXY-5-METHYLBENZALDEHYDE Property

Density: 1.08
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Colorless to light yellow Liquid

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M330848
Product name: 2-Methoxy-5-methylbenzaldehyde
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: Z0802
Product name: 2-Methoxy-5-methylbenzaldehyde
Packaging: 500mg
Price: $74
Updated: 2021/12/16

Rieke Metals

Product number: 8077
Product name: 2-Methoxy-5-methylbenzaldehyde
Purity: 97%
Packaging: 5g
Price: $714
Updated: 2021/12/16

ChemScene

Product number: CS-M1298
Product name: 2-methoxy-5-methylbenzaldehyde
Purity: ≥98.0%
Packaging: 10g
Price: $217
Updated: 2021/12/16

Rieke Metals

Product number: 8077
Product name: 2-Methoxy-5-methylbenzaldehyde
Purity: 97%
Packaging: 1g
Price: $251
Updated: 2021/12/16

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2-METHOXY-5-METHYLBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

613-84-3

74-88-4

7083-19-4

Step 1: Suspend 5-methylsalicylaldehyde (2-hydroxy-5-methylbenzaldehyde, CAS No. 613-84-3) in a solvent mixture of 5 mL dichloromethane and 5 mL water. 1.47 mL (4.4 mmol, 3 eq.) of 1 N sodium hydroxide solution and 1.52 g (2.94 mmol, 2 eq.) of 50% aqueous tetrabutylammonium hydroxide were added sequentially, followed by iodomethane (457 μL, 5 eq.). The reaction mixture was stirred at room temperature for 3 hours. After completion of the reaction, the reaction mixture was extracted with dichloromethane three times, the organic phases were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel fast column chromatography (eluent: cyclohexane/ethyl acetate, 9/1, v/v) to afford 215 mg (97% yield) of the target compound 2-methoxy-5-methylbenzaldehyde.

References

[1] Canadian Journal of Chemistry, 2012, vol. 90, # 11, p. 965 - 974
[2] Journal of Medicinal Chemistry, 2002, vol. 45, # 19, p. 4188 - 4201
[3] Patent: WO2010/66847, 2010, A1. Location in patent: Page/Page column 70
[4] Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990, vol. 29, # 9, p. 876 - 878
[5] Beilstein Journal of Organic Chemistry, 2018, vol. 14, p. 734 - 746

2-METHOXY-5-METHYLBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHOXY-5-METHYLBENZALDEHYDE Suppliers

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7083-19-4, 2-METHOXY-5-METHYLBENZALDEHYDERelated Search:

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5-Methyl-2-methoxybenzaldehyde

Benzaldehyde, 2-methoxy-5-methyl-

7083-19-4