N-(2-AMINOETHYL)METHANESULFONAMIDE
- Product Name
- N-(2-AMINOETHYL)METHANESULFONAMIDE
- CAS No.
- 202197-61-3
- Chemical Name
- N-(2-AMINOETHYL)METHANESULFONAMIDE
- Synonyms
- N-(2-AMINOETHYL)METHANESULFONAMIDE;Methanesulfonamide, N-(2-aminoethyl)-, hydrochloride (1:1)
- CBNumber
- CB31491703
- Molecular Formula
- C3H11ClN2O2S
- Formula Weight
- 174.64
- MOL File
- 202197-61-3.mol
N-(2-AMINOETHYL)METHANESULFONAMIDE Property
- storage temp.
- Storage temp. 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 4112DA
- Product name
- N-(2-Aminoethyl)methanesulfonamidehydrochloride
- Packaging
- 1g
- Price
- $392
- Updated
- 2021/12/16
- Product number
- BB-4029868
- Product name
- N-(2-aminoethyl)methanesulfonamidehydrochloride
- Purity
- 95%
- Packaging
- 5G
- Price
- $460
- Updated
- 2021/12/16
- Product number
- CD13018843
- Product name
- N-(2-Aminoethyl)methanesulfonamidehydrochloride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $540
- Updated
- 2021/12/16
- Product number
- AR2420
- Product name
- N-(2-AMINOETHYL)METHANESULFONAMIDEHCL
- Purity
- 95%
- Packaging
- 5/ G
- Price
- $704
- Updated
- 2021/12/16
- Product number
- BB-4029868
- Product name
- N-(2-aminoethyl)methanesulfonamidehydrochloride
- Purity
- 95%
- Packaging
- 10g
- Price
- $745
- Updated
- 2021/12/16
N-(2-AMINOETHYL)METHANESULFONAMIDE Chemical Properties,Usage,Production
Synthesis
1190044-23-5
202197-61-3
N-(2-Aminoethyl)methane sulfonamide hydrochloride was synthesized from tert-butyl {2-[(methylsulfonyl)amino]ethyl}carbamate (4.44 g) by the method of Example 17. The steps were as follows: the raw material was dissolved in a solvent mixture of ethyl acetate (40 mL) and THF (20 mL), and a 4M HCl-ethyl acetate solution (23 mL) was slowly added at room temperature. The reaction mixture was stirred at room temperature for 23 hours. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure, and the resulting residue was washed with ethyl acetate to give the final N-(2-aminoethyl)methane sulfonamide hydrochloride (3.02 g, 93% yield) as white crystals. The product was characterized by 1H NMR (300 MHz, DMSO-d6) with chemical shifts of δ 2.90 (2H, t, J = 6.4 Hz), 2.96 (3H, s), 3.20 (2H, t, J = 6.2 Hz), 7.35 (1H, br.s.), 8.06 (3H, s).
References
[1] Patent: EP2261213, 2010, A1. Location in patent: Page/Page column 44
[2] Patent: EP2484678, 2012, A1. Location in patent: Page/Page column 19
[3] Patent: US2012/208833, 2012, A1. Location in patent: Page/Page column 13
[4] Patent: WO2018/39621, 2018, A1. Location in patent: Paragraph 00364-00365
N-(2-AMINOETHYL)METHANESULFONAMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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