ETHYL 3,4-DIMETHOXYPHENYLACETATE
- Product Name
- ETHYL 3,4-DIMETHOXYPHENYLACETATE
- CAS No.
- 18066-68-7
- Chemical Name
- ETHYL 3,4-DIMETHOXYPHENYLACETATE
- Synonyms
- ethyl homoveratrate;Ethyl dimethoxyphenylacetate;HOMOVERATRIC ACID ETHYL ESTER;ETHYL 3,4-DIMETHOXYPHENYLACETATE;ETHYL 2-(3,4-DIMETHOXYPHENYL)ACETATE;Ethyl 3,4-dimethoxyphenylacetate, 98+%;3,4-dimethoxy-benzeneaceticaciethylester;3,4-Dimethoxybenzeneacetic acid ethyl ester;2-(3,4-dimethoxyphenyl)acetic acid ethyl ester;Benzeneacetic acid, 3,4-dimethoxy-, ethyl ester
- CBNumber
- CB3233807
- Molecular Formula
- C12H16O4
- Formula Weight
- 224.25
- MOL File
- 18066-68-7.mol
ETHYL 3,4-DIMETHOXYPHENYLACETATE Property
- Boiling point:
- 191 °C
- Density
- 1.084±0.06 g/cm3(Predicted)
- refractive index
- 1.5180
- Flash point:
- 159-160°C/4mm
- storage temp.
- Sealed in dry,Room Temperature
- form
- liquid
- color
- Brown
- BRN
- 2697968
- CAS DataBase Reference
- 18066-68-7(CAS DataBase Reference)
- EPA Substance Registry System
- Benzeneacetic acid, 3,4-dimethoxy-, ethyl ester (18066-68-7)
Safety
- TSCA
- Yes
- HS Code
- 2915390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- PH011221
- Product name
- ethyl (3,4-dimethoxyphenyl)acetate
- Purity
- AldrichCPR
- Packaging
- 500mg
- Price
- $172
- Updated
- 2023/06/20
- Product number
- B125020
- Product name
- Ethyl2-(3,4-Dimethoxyphenyl)acetate
- Packaging
- 2.5g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- E006
- Product name
- Ethyl2-(3,4-dimethoxyphenyl)acetate
- Packaging
- 5g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- 119718
- Product name
- Ethyl 2-(3,4-dimethoxyphenyl)acetate
- Purity
- 98%
- Packaging
- 10g
- Price
- $46
- Updated
- 2021/12/16
- Product number
- 2623-1-X2
- Product name
- Ethyl 3,4-dimethoxyphenylacetate
- Purity
- 98%
- Packaging
- 25g
- Price
- $120
- Updated
- 2021/12/16
ETHYL 3,4-DIMETHOXYPHENYLACETATE Chemical Properties,Usage,Production
Synthesis
93-40-3
64-17-5
18066-68-7
In a typical reaction, 3,4-dimethoxyphenylacetic acid (332 g, 0.6 mol), ethanol (1.5-2 mol), and AMA 2:3 were mixed in a provided reaction glass tube equipped with a screw cap and magnetic stirrer until a wet mixture was formed. The reaction mixture was placed in a microwave reactor (Anton Parr Monowave 300) and irradiated at 80°C for 8 min or 120°C for 20 min. Upon completion of the reaction, the mixture was cooled, diluted with dichloromethane (41 mL), filtered by gravity and the filtrate was washed with dichloromethane. Subsequently, the filtrate was washed with saturated sodium carbonate solution and water. The organic layer was separated, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give ethyl 3,4-dimethoxyphenylacetate.
References
[1] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 4, p. 1586 - 1605
[2] Journal of Organic Chemistry, 2003, vol. 68, # 3, p. 1165 - 1167
[3] Synthetic Communications, 2014, vol. 44, # 16, p. 2386 - 2392
[4] Journal of Organic Chemistry, 2010, vol. 75, # 19, p. 6549 - 6562
[5] Tetrahedron, 1997, vol. 53, # 30, p. 10555 - 10564
ETHYL 3,4-DIMETHOXYPHENYLACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from ETHYL 3,4-DIMETHOXYPHENYLACETATE manufacturers
- Product
- ETHYL 3,4-DIMETHOXYPHENYLACETATE 18066-68-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- MIn98%HPLC/LC
- Supply Ability
- 100KGS
- Release date
- 2020-10-29