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1-Butylpyrrolidine

Product Name
1-Butylpyrrolidine
CAS No.
767-10-2
Chemical Name
1-Butylpyrrolidine
Synonyms
1-butyl-pyrrolidin;1-BUTYLPYRROLIDINE;N-BUTYL PYRROLIDINE;Pyrrolidine, 1-butyl-;N-butyl-Tetrahydropyrrole;1-BUTYLPYRROLIDINE FOR SYNTHESIS
CBNumber
CB3238589
Molecular Formula
C8H17N
Formula Weight
127.23
MOL File
767-10-2.mol
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1-Butylpyrrolidine Property

Boiling point:
155-157 °C/754 mmHg (lit.)
Density 
0.814 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.44(lit.)
Flash point:
97 °F
storage temp. 
Refrigerator, Under inert atmosphere
solubility 
Chloroform (Sparingly), Ethyl Acetate (Slightly)
pka
10.62±0.20(Predicted)
form 
Oil
color 
Colourless
LogP
2.209 (est)
CAS DataBase Reference
767-10-2(CAS DataBase Reference)
NIST Chemistry Reference
1-Butylpyrrolidine(767-10-2)
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Safety

Hazard Codes 
T
Risk Statements 
10-24/25
Safety Statements 
16-36/37-45
RIDADR 
UN 2929 6.1/PG 2
WGK Germany 
2
RTECS 
UX9800000
HazardClass 
3.2
PackingGroup 
III
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H226Flammable liquid and vapour

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P240Ground/bond container and receiving equipment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
280372
Product name
1-Butylpyrrolidine
Purity
98%
Packaging
100ml
Price
$402
Updated
2024/03/01
TRC
Product number
B700948
Product name
1-Butylpyrrolidine
Packaging
100mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
Q329
Product name
1-Butylpyrrolidine
Packaging
1ml
Price
$67
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB45924
Product name
1-Butylpyrrolidine
Packaging
5G
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB45924
Product name
1-Butylpyrrolidine
Packaging
10g
Price
$125
Updated
2021/12/16
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1-Butylpyrrolidine Chemical Properties,Usage,Production

Uses

1-Butylpyrrolidine can be used in the composition for alcohol recovery solution.

Uses

1-Butylpyrrolidine has been used in:
microwave-assisted synthesis of ionic liquid precursor, 1-butyl-1-methylpyrrolidinium methylcarbonate.
[N,N-methylbutylpyrrolidinium] thiosalicylate, ionic liquid.
The reaction of 1-butylpyrrolidine with dimethyl carbonate to yield the ionic liquid precursor, 1-butyl-1-methylpyrrolidinium methylcarbonate, has been investigated under microwave heating conditions and the reaction parameters optimised to achieve 100% yield of the pyrrolidinium salt with no by-products in under 1h.

Preparation

The synthesis of 1-butylpyrrolidine and its derivatives (1-butylpyrrolidine with a little of 1-butenylpyrrolidines) was developed via a one-pot method from ammonia and 1,4-butandiol. Here, the product of 1-butylpyrrolidine was emphatically investigated, and the yield was 76% under the optimized conditions. Such a route was realized through successive N-alkylation using aqueous ammonia as the nitrogen source over the CuNiPd/ZSM-5 catalyst, which was prepared by a simple incipient wetness method. In this route, 1,4-butandiol not only participated in the formation of the N-heterocycle, but also acted as an alkylating reagent. This work offers a straightforward, economical route for 1-butylpyrrolidine and its derivatives.

One-pot synthesis of 1-butylpyrrolidine and its derivatives from aqueous ammonia and 1,4-butandiol over CuNiPd/ZSM-5 catalysts

1-Butylpyrrolidine Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Butylpyrrolidine Suppliers

Wuxi Helen Biotechnology Co., Ltd.,
Tel
0510-85629785 18013409632
Fax
0510-85625359
Email
sales@reading-chemicals.com
Country
China
ProdList
14092
Advantage
58
Shanghai Boyle Chemical Co., Ltd.
Tel
021-50182298 021-50180596
Fax
+86-21-57758967
Email
sales@boylechem.com
Country
China
ProdList
2210
Advantage
55
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44751
Advantage
61
Capot Chemical Co., Ltd
Tel
+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
Email
sales@capotchem.com
Country
China
ProdList
18217
Advantage
66
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
zhangsn@titansci.com
Country
China
ProdList
14113
Advantage
59
Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
17988
Advantage
64
T&W GROUP
Tel
021-61551611 13296011611
Fax
+86 21-50676805
Email
contact@trustwe.com
Country
China
ProdList
9900
Advantage
58
Suzhou Sibian Chemical Technology Co.,Ltd.
Tel
0512-65617459 18915409046
Fax
0512-65617459
Email
sales@sibian-chem.com
Country
China
ProdList
1927
Advantage
55
Shanghai T&W Pharmaceutical Co., Ltd.
Tel
+86 21 61551611
Fax
+86 21 50676805
Country
China
ProdList
9901
Advantage
58
Nanjing Norris-Pharm Technology Co., Ltd
Tel
13901585132
Fax
+86-25-52131256
Email
799750417@qq.com
Country
China
ProdList
8888
Advantage
55
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View Lastest Price from 1-Butylpyrrolidine manufacturers

Henan Fengda Chemical Co., Ltd
Product
1-Butylpyrrolidine 767-10-2
Price
US $8.00-2.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-04-24

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