3-METHYLAZETIDINE HYDROCHLORIDE
- Product Name
- 3-METHYLAZETIDINE HYDROCHLORIDE
- CAS No.
- 935669-28-6
- Chemical Name
- 3-METHYLAZETIDINE HYDROCHLORIDE
- Synonyms
- EOS-60406;3-Methylazetidine;3-Methylazetidine HCl;3-Methylazetidine hydroch...;METHYLAZETIDINE HYDROCHLORIDE;3-METHYLAZETIDINE HYDROCHLORIDE;3-Methylazetidine hydrochlorate;3-methylazetidinium hydrochloride;3-METHYLAZETIDINE BENZENESULFONATE;Azetidine, 3-methyl-, hydrochloride
- CBNumber
- CB32449875
- Molecular Formula
- C4H10ClN
- Formula Weight
- 107.58
- MOL File
- 935669-28-6.mol
3-METHYLAZETIDINE HYDROCHLORIDE Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Colorless to light yellow <150 °C Solid,>151 °C Liquid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- M286718
- Product name
- 3-MethylazetidineBenzenesulfonicAcidSalt
- Packaging
- 1g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- CHM0382588
- Product name
- 3-METHYLAZETIDINE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.75
- Updated
- 2021/12/16
- Product number
- 3H31-5-32
- Product name
- 3-Methylazetidinehydrochloride
- Packaging
- 5G
- Price
- $620
- Updated
- 2021/12/16
- Product number
- W9623
- Product name
- 3-Methylazetidinehydrochloride
- Packaging
- 250mg
- Price
- $82
- Updated
- 2021/12/16
- Product number
- 069355
- Product name
- 3-Methylazetidine hydrochloride
- Purity
- >95%
- Packaging
- 1g
- Price
- $109
- Updated
- 2021/12/16
3-METHYLAZETIDINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
934664-23-0
935669-28-6
General procedure for the synthesis of 3-methylazetidine hydrochloride from benzyl 3-methylene azetidine-1-carboxylate: the product of step (iii) (14.1 g) was dissolved in ethanol (100 mL), 10% Pd/C (JM type 87L) (1.48 g) was added and treated under hydrogen atmosphere. The reaction mixture was stirred for 40 h at 20 °C under hydrogen pressure of 4.50 bar to remove the Cbz protecting groups. Subsequently, the mixture was transferred to ethanol (100 mL) containing palladium hydroxide (2 g) and continued to be hydrogenated at 4.50 bar hydrogen pressure for 24 hours. Upon completion of the reaction, the mixture was filtered through a pad of diatomaceous earth and the filtrate was cooled to 0°C in an ice bath. To the cooled filtrate was added dropwise a dioxane solution (26.0 mL) of 4 M HCl, followed by evaporation of the solution to dryness to give the title product 3-methylazetidine hydrochloride (7.46 g) as a light brown oil. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 9.24 (s, 2H), 3.95 (ddd, J = 7.4, 9.8, 11.4 Hz, 2H), 3.55-3.45 (m, 2H), 2.85 (dt, J = 6.7, 14.2 Hz, 1H), 1.16 (d, 3H).
References
[1] Patent: EP2740458, 2016, B1. Location in patent: Paragraph 0052
3-METHYLAZETIDINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-METHYLAZETIDINE HYDROCHLORIDE manufacturers
- Product
- 3-METHYLAZETIDINE HYDROCHLORIDE 935669-28-6
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02