3-(9H-Carbazol-9-yl)phenylboronic acid
- Product Name
- 3-(9H-Carbazol-9-yl)phenylboronic acid
- CAS No.
- 864377-33-3
- Chemical Name
- 3-(9H-Carbazol-9-yl)phenylboronic acid
- Synonyms
- 3-NBAPC;-9-yL;PF23A;(3-(9H-CarbazoL;3-(9-Carbazolyl)benzeneboronic acid;3-(9H-Carbazol-9-yl)phenylboronic acid;3-(9H-Carbazol-9-yl)phenylboromic acid;3-(9-Carbazolyl)benzeneboronicacid,98%;3-(9H-carbazole-9-yl)phenylboronic acid;3-(9H-Carbazol-9-yl)benzeneboronic Acid
- CBNumber
- CB32548099
- Molecular Formula
- C18H14BNO2
- Formula Weight
- 287.12
- MOL File
- 864377-33-3.mol
3-(9H-Carbazol-9-yl)phenylboronic acid Property
- Boiling point:
- 472.6±51.0 °C(Predicted)
- Density
- 1.20
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- Powder
- pka
- 8.30±0.10(Predicted)
- color
- Off-white
- InChI
- InChI=1S/C18H14BNO2/c21-19(22)13-6-5-7-14(12-13)20-17-10-3-1-8-15(17)16-9-2-4-11-18(16)20/h1-12,21-22H
- InChIKey
- IDQUIFLAFFZYEX-UHFFFAOYSA-N
- SMILES
- B(C1=CC=CC(N2C3=C(C=CC=C3)C3=C2C=CC=C3)=C1)(O)O
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C2967
- Product name
- 3-(9H-Carbazol-9-yl)phenylboronic Acid (contains varying amounts of Anhydride)
- Packaging
- 1g
- Price
- $37
- Updated
- 2025/07/31
- Product number
- C2967
- Product name
- 3-(9H-Carbazol-9-yl)phenylboronic Acid (contains varying amounts of Anhydride)
- Packaging
- 5g
- Price
- $109
- Updated
- 2025/07/31
- Product number
- C176073
- Product name
- 3-(9H-Carbazol-9-yl)phenylboronicacid
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- C176073
- Product name
- 3-(9H-Carbazol-9-yl)phenylboronicacid
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C176073
- Product name
- 3-(9H-Carbazol-9-yl)phenylboronicacid
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
3-(9H-Carbazol-9-yl)phenylboronic acid Chemical Properties,Usage,Production
Chemical Properties
off-white solid
Uses
suzuki reaction
Synthesis
185112-61-2
121-43-7
864377-33-3
General procedure for the synthesis of 3-(9H-carbazol-9-yl)phenylboronic acid from 9-(3-bromophenyl)-9H-carbazole and trimethyl borate: (2) Dissolve 4.00 g of 9-(3-bromophenyl)-9H-carbazole in dry 50 mL of THF, and cool to -78 °C. 6mL (2.4M) of n-butyllithium solution was slowly added and reacted for 1 hour. Subsequently, 1.8 mL of trimethyl borate was added and the reaction continued for 2 hours. The reaction mixture was warmed to room temperature and stirred overnight. After cooling to 0°C, 40 mL of 2.0 M HCl was added for hydrolysis. The reaction mixture was extracted with dichloromethane and the solvent was evaporated to give 2.96 g of 3-(9H-carbazol-9-yl)phenylboronic acid in 83% yield.
References
[1] Patent: CN103588770, 2016, B. Location in patent: Paragraph 0047
[2] Patent: CN107686484, 2018, A. Location in patent: Paragraph 0129-0132
[3] Patent: WO2013/12298, 2013, A1. Location in patent: Paragraph 103-104
3-(9H-Carbazol-9-yl)phenylboronic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-(9H-Carbazol-9-yl)phenylboronic acid manufacturers
- Product
- 3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-17
- Product
- 3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
- Price
- US $50.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-22
- Product
- 3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%Min
- Supply Ability
- 1000kg
- Release date
- 2023-03-12