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Xylometazoline hydrochloride

Product Name
Xylometazoline hydrochloride
CAS No.
1218-35-5
Chemical Name
Xylometazoline hydrochloride
Synonyms
XYLOMETAZOLINE HCL;Olynth;Novorin;XyMelin;Therapin;Brizolin;Galazolin;Neo-Rinoleina;Neo-Synephrine II;XYLONETAZOLINEHCL
CBNumber
CB3257614
Molecular Formula
C16H25ClN2
Formula Weight
280.84
MOL File
1218-35-5.mol
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Xylometazoline hydrochloride Property

Melting point:
131-133 C
storage temp. 
2-8°C
solubility 
Freely soluble in water, in ethanol (96 per cent) and in methanol.
form 
Solid
color 
Crystals
Merck 
14,10086
CAS DataBase Reference
1218-35-5(CAS DataBase Reference)
EPA Substance Registry System
1H-Imidazole, 2-[[4-(1,1-dimethylethyl)-2,6-dimethylphenyl]methyl]-4,5-dihydro-, monohydrochloride (1218-35-5)
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Safety

Hazard Codes 
Xn,Xi
Risk Statements 
22-36/37/38
Safety Statements 
36-26
RIDADR 
UN 2811 6.1/PG 3
WGK Germany 
3
RTECS 
NJ2390000
HazardClass 
6.1
PackingGroup 
III
HS Code 
29332900
Toxicity
LD50 orl-rat: 230 mg/kg KSRNAM 5,555,71
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

Precautionary statements

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
1721002
Product name
Xylometazoline hydrochloride
Purity
United States Pharmacopeia (USP) Reference Standard
Packaging
250mg
Price
$436
Updated
2024/03/01
Sigma-Aldrich
Product number
BP353
Product name
Xylometazoline hydrochloride
Purity
British Pharmacopoeia (BP) Reference Standard
Packaging
100MG
Price
$221
Updated
2023/06/20
Sigma-Aldrich
Product number
07297
Product name
Xylometazoline hydrochloride
Purity
analytical standard
Packaging
100mg
Price
$108
Updated
2022/05/15
TCI Chemical
Product number
X0063
Product name
Xylometazoline Hydrochloride
Purity
>98.0%(HPLC)(N)
Packaging
1g
Price
$44
Updated
2024/03/01
TCI Chemical
Product number
X0063
Product name
Xylometazoline Hydrochloride
Purity
>98.0%(HPLC)(N)
Packaging
5g
Price
$112
Updated
2024/03/01
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Xylometazoline hydrochloride Chemical Properties,Usage,Production

Chemical Properties

Xylometazoline hydrochloride is white or almost white, crystalline powder.

Originator

Otrivin,Geigy,US,1959

Uses

anthelmintic

Uses

Xylometazoline hydrochloride may be used as a reference standard in determining the xylometazoline hydrochloride content in samples of nasal drops using high performance liquid chromatography (HPLC).

Uses

Xylometazoline hydrochloride is used as a nasal decongestant.

Manufacturing Process

62 grams of para-tertiany-butyl-ortho,ortho'-dimethyl-phenyl-acetonitrile [obtainable, for example, by the method of Buu-Hoi and P. Cagniant, Bulletin de la Societe Chimique de France, volume 9, page 891 (1942)], 20.6 grams of ethylenediamine of 96% purity and 1.55 cc of carbon disulfide are heated together in a distillation flask with the exclusion of moisture for 48 hours on a boiling water bath. Ammonia is evolved. Upon cooling the reaction product solidifies and is then dissolved in benzene, the solution is filtered while hot with the addition of animal charcoal and petroleum ether is added. The mixture is filtered to remove the impurities that are first precipitated and by the further addition of petroleum ether 2-(para-tertiary-butyl-ortho,ortho'- dimethyl-phenyl-methyl)-imidazoline is caused to crystallize out.
The product melts at 131° to 133°C after being recrystallized from a mixture of benzene and petroleum ether. It can be converted into its hydrochloride as follows:
189 grams of 2-(para-tertiary-butyl-ortho,ortho'-dimethyl-phenyl-methyl)- imidazoline are dissolved in 400 cc of absolute ethanol, the solution is rendered acid by the addition of 104 cc of an ethanolic solution of hydrochloric acid of 30% strength, the mixture is filtered with the addition of animal charcoal, and dry ethyl acetate and absolute ether are added until crystallization sets in. After cooling the mixture, the salt is filtered off with suction and crystallized several times from absolute ethanol with the use of animal charcoal and the addition of dry mixture of ethyl acetate and ether. The hydrochloride so obtained melts at 327° to 329°C (with decomposition).

brand name

Neo-Synephrine II (Sterling Winthrop); Otrivin Hydrochloride (Ciba-Geigy).

Therapeutic Function

Adrenergic (vasopressor)

General Description

Xylometazoline hydrochloride is a derivative of imidazole, and a representative of the class of α1 agonists. It is commonly used in nasal decongestants, which works on the principle of constricting the blood vessels in the mucous membranes.

Biochem/physiol Actions

α-adrenoceptor agonist; imidazoline binding site ligand.

Safety Profile

Poison by ingestion, subcutaneous, intravenous, and intraperitoneal routes. When heated to decomposition it emits toxic fumes of NOx and HCl.

Xylometazoline hydrochloride Preparation Products And Raw materials

Raw materials

Preparation Products

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Xylometazoline hydrochloride Suppliers

wuhan dingxingtong Chemical Technology Co., Ltd Co., Ltd
Tel
027-59207796 13429867250
Fax
027-59207796
Email
w13429867250@163.com
Country
China
ProdList
1989
Advantage
58
Hubei wei shi reagent group ltd., company
Tel
027-59105166 13125137732
Email
2853863890@qq.com
Country
China
ProdList
3310
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
94657
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44688
Advantage
61
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14103
Advantage
59
Chemsky (shanghai) International Co.,Ltd
Tel
021-50135380
Email
shchemsky@sina.com
Country
China
ProdList
15402
Advantage
60
XiaoGan ShenYuan ChemPharm co,ltd
Tel
15527768850
Email
1791901229@qq.com
Country
China
ProdList
8836
Advantage
52
Tianjin heowns Biochemical Technology Co., Ltd.
Tel
400 638 7771
Email
sales@heowns.com
Country
China
ProdList
14435
Advantage
57
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View Lastest Price from Xylometazoline hydrochloride manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
Xylometazoline hydrochloride 1218-35-5
Price
US $0.00-0.00/KG
Min. Order
100g
Purity
99.0%-101%
Supply Ability
100 KGS
Release date
2021-06-08
BEIJING SJAR TECHNOLOGY DEVELOPMENT CO., LTD.
Product
Xylometazoline Hydrochloride 1218-35-5
Price
US $0.00/g
Min. Order
1g
Purity
More Than 99%
Supply Ability
100kg/Month
Release date
2024-11-13
Wuhan Senwayer Century Chemical Co.,Ltd
Product
Xylometazoline hydrochloride 1218-35-5
Price
US $0.00/g
Min. Order
5g
Purity
98%
Supply Ability
500kg
Release date
2023-02-08

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