7-broMoquinolin-3-aMine
- Product Name
- 7-broMoquinolin-3-aMine
- CAS No.
- 1266322-58-0
- Chemical Name
- 7-broMoquinolin-3-aMine
- Synonyms
- 7-broMoquinolin-3-aMine;3-Amino-7-bromoquinoline;3-Quinolinamine, 7-bromo-
- CBNumber
- CB32582897
- Molecular Formula
- C9H7BrN2
- Formula Weight
- 223.07
- MOL File
- 1266322-58-0.mol
7-broMoquinolin-3-aMine Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- White to light brown Solid
N-Bromosuccinimide Price
- Product number
- B998985
- Product name
- 7-bromoquinolin-3-amine
- Packaging
- 100mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- 5261AA
- Product name
- 7-Bromoquinolin-3-amine
- Packaging
- 1g
- Price
- $475
- Updated
- 2021/12/16
- Product number
- 5261AA
- Product name
- 7-Bromoquinolin-3-amine
- Packaging
- 250mg
- Price
- $219
- Updated
- 2021/12/16
- Product number
- 1266322580
- Product name
- 7-Bromoquinolin-3-amine
- Packaging
- 1g
- Price
- $589.36
- Updated
- 2021/12/16
- Product number
- 1266322580
- Product name
- 7-Bromoquinolin-3-amine
- Packaging
- 5g
- Price
- $1633.66
- Updated
- 2021/12/16
7-broMoquinolin-3-aMine Chemical Properties,Usage,Production
Synthesis
1375108-38-5
1266322-58-0
b) Synthesis of 7-bromoquinolin-3-amine: 2-(7-bromoquinolin-3-yl)isoindoline-1,3-dione (10 g, 28.3 mmol) was suspended in ethanol (200 mL), hydrazine (1.777 mL, 56.6 mmol) was added, followed by heating and refluxing for 1 hour. After completion of the reaction, the mixture was allowed to cool to room temperature and the precipitate was collected and washed with a small amount of ethanol. The filtrate was concentrated to dryness to give a gray solid. The resulting solid was dissolved in warm ethanol and adsorbed on silica gel. Purification by silica gel column chromatography (eluent: 50-100% ethyl acetate/hexane gradient) afforded the target compound 7-bromoquinolin-3-amine (3.5 g, 56% yield).1H NMR (400 MHz, DMSO-d6) δ ppm: 5.83 (s, 2H), 7.14 (d, J = 2.53 Hz, 1H), 7.49 (dd, J = 8.84, 2.02Hz, 1H), 7.54-7.65 (m, 1H), 7.94 (d, J = 1.77Hz, 1H), 8.46 (d, J = 2.78Hz, 1H).
References
[1] Patent: WO2017/32840, 2017, A1. Location in patent: Page/Page column 265; 266
[2] Patent: WO2013/28447, 2013, A1. Location in patent: Page/Page column 117
[3] Patent: WO2013/52716, 2013, A1. Location in patent: Page/Page column 63
[4] Patent: WO2013/177253, 2013, A2. Location in patent: Page/Page column 64
[5] Patent: WO2014/8223, 2014, A2. Location in patent: Page/Page column 71-72
7-broMoquinolin-3-aMine Preparation Products And Raw materials
Raw materials
Preparation Products
7-broMoquinolin-3-aMine Suppliers
- Tel
- 021-50182298 021-50180596
- Fax
- +86-21-57758967
- sales@boylechem.com
- Country
- China
- ProdList
- 2208
- Advantage
- 55
- Tel
- 010-56645598 13366904824
- Fax
- 01062230033
- bjkaida@163.com
- Country
- China
- ProdList
- 1618
- Advantage
- 59
- Tel
- sales@ahpharmatech.com
- Country
- China
- ProdList
- 5734
- Advantage
- 55
- Tel
- 0311-89250318 031166536426
- Fax
- 4000311741
- master@sjzsdyn.com
- Country
- China
- ProdList
- 3495
- Advantage
- 58
- Tel
- 021-61312847; 18021002903
- Fax
- QQ:3008007432
- 3008007409@qq.com
- Country
- China
- ProdList
- 71826
- Advantage
- 60
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 021-20432229
- Fax
- QQ2412110556
- 2412110556@qq.com
- Country
- China
- ProdList
- 6017
- Advantage
- 55
- Tel
- 028-65791793 18140026355
- Fax
- QQ568470422
- 568470422@qq.com
- Country
- China
- ProdList
- 9997
- Advantage
- 58
- Tel
- 025-58859352 18068836627
- Fax
- (5)02557626880
- dt3@aikonchem.com
- Country
- China
- ProdList
- 15493
- Advantage
- 58
- Tel
- 021-50822001
- marketing@medicilon.com.cn
- Country
- China
- ProdList
- 1152
- Advantage
- 58
View Lastest Price from 7-broMoquinolin-3-aMine manufacturers
- Product
- 7-broMoquinolin-3-aMine 1266322-58-0
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 200g
- Release date
- 2020-02-01