ChemicalBook > CAS DataBase List > 3-METHOXYPICOLINIC ACID METHYL ESTER

3-METHOXYPICOLINIC ACID METHYL ESTER

Product Name: 3-METHOXYPICOLINIC ACID METHYL ESTER
CAS No.: 24059-83-4
Chemical Name: 3-METHOXYPICOLINIC ACID METHYL ESTER
Synonyms: methyl 3-methoxypicolinate;3-METHOXYPICOLINIC ACID METHYL ESTER;Methyl 3-methoxypyridine-2-carboxylate;3-Methoxy-pyridin-2-carboxylic acid methyl ester;3-methoxy-2-pyridinecarboxylic acid methyl ester;3-Methoxy-pyridine-2-carboxylic acid methyl ester;2-PYRIDINECARBOXYLIC ACID, 3-METHOXY-, METHYL ESTER
CBNumber: CB3317929
Molecular Formula: C8H9NO3
Formula Weight: 167.16
MOL File: 24059-83-4.mol

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3-METHOXYPICOLINIC ACID METHYL ESTER Property

Boiling point:: 280.4±20.0 °C(Predicted)
Density: 1.156±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 1.16±0.10(Predicted)
Appearance: Colorless to yellow Liquid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P330Rinse mouth.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B451543
Product name: Methyl3-Methoxypyridine-2-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 073443
Product name: Methyl 3-methoxypyridine-2-carboxylate
Purity: 95+%
Packaging: 1g
Price: $958
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0078248
Product name: 3-METHOXYPICOLINIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 250MG
Price: $1066.07
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0078248
Product name: 3-METHOXYPICOLINIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 1G
Price: $1630.86
Updated: 2021/12/16

AK Scientific

Product number: W4763
Product name: Methyl3-methoxypyridine-2-carboxylate
Packaging: 250mg
Price: $143
Updated: 2021/12/16

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3-METHOXYPICOLINIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

62733-99-7

74-88-4

24059-83-4

In a 50 mL round-bottomed flask equipped with a magnetic stirrer, methyl 3-hydroxy-2-pyridinecarboxylate (3.5 g, 22.80 mmol), potassium carbonate (3.46 g, 25.0 mmol), iodomethane (4.87 g, 34.3 mmol), and N,N-dimethylformamide (20 mL) were added sequentially. The reaction mixture was stirred at room temperature for 18 h under nitrogen protection. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (30 mL) and water (10 mL). The organic phase was separated and the aqueous phase was extracted with ethyl acetate (3 × 10 mL). The organic phases were combined, dried with anhydrous sodium sulfate, and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography with the eluent being a hexane solution of 30% ethyl acetate to give 2.1 g of methyl 3-methoxypyridine-2-carboxylate in 54% yield.

References

[1] ChemMedChem, 2016, vol. 11, # 23, p. 2607 - 2620
[2] Patent: WO2007/16525, 2007, A2. Location in patent: Page/Page column 50
[3] Patent: US2013/281396, 2013, A1. Location in patent: Paragraph 0310
[4] Patent: WO2018/52903, 2018, A1. Location in patent: Page/Page column 70-71

3-METHOXYPICOLINIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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24059-83-4, 3-METHOXYPICOLINIC ACID METHYL ESTERRelated Search:

Trimethoprim 3-METHOXYPYRIDINE Methyl 6-methoxynicotinate 4-METHOXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER 3-[(2,3-DIHYDRO-5-OXO-(1H,5H)-BENZO[IJ]QUINOLIZIN-6-YL)METHOXY]PYRIDINE-2-CARBOXYLIC ACID, METHYL ESTER 3-N-PROPOXYPICOLINIC ACID N-PROPYL ESTER 3-Hydroxypicolinic acid 3-METHOXYPICOLINIC ACID METHYL ESTER 3-HYDROXY-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER (3-METHOXY-PYRIDIN-2-YL)-METHANOL 3-METHOXY-2-PYRIDINECARBOXYLIC ACID

2-PYRIDINECARBOXYLIC ACID, 3-METHOXY-, METHYL ESTER

3-Methoxy-pyridine-2-carboxylic acid methyl ester

3-METHOXYPICOLINIC ACID METHYL ESTER

3-methoxy-2-pyridinecarboxylic acid methyl ester

Methyl 3-methoxypyridine-2-carboxylate

methyl 3-methoxypicolinate

3-Methoxy-pyridin-2-carboxylic acid methyl ester

24059-83-4

Heterocycles

Heterocycle-Pyridine series