3-METHOXYPICOLINIC ACID METHYL ESTER
- Product Name
- 3-METHOXYPICOLINIC ACID METHYL ESTER
- CAS No.
- 24059-83-4
- Chemical Name
- 3-METHOXYPICOLINIC ACID METHYL ESTER
- Synonyms
- methyl 3-methoxypicolinate;3-METHOXYPICOLINIC ACID METHYL ESTER;Methyl 3-methoxypyridine-2-carboxylate;3-Methoxy-pyridin-2-carboxylic acid methyl ester;3-methoxy-2-pyridinecarboxylic acid methyl ester;3-Methoxy-pyridine-2-carboxylic acid methyl ester;2-PYRIDINECARBOXYLIC ACID, 3-METHOXY-, METHYL ESTER
- CBNumber
- CB3317929
- Molecular Formula
- C8H9NO3
- Formula Weight
- 167.16
- MOL File
- 24059-83-4.mol
3-METHOXYPICOLINIC ACID METHYL ESTER Property
- Boiling point:
- 280.4±20.0 °C(Predicted)
- Density
- 1.156±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 1.16±0.10(Predicted)
- Appearance
- Colorless to yellow Liquid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P330Rinse mouth.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B451543
- Product name
- Methyl3-Methoxypyridine-2-carboxylate
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 073443
- Product name
- Methyl 3-methoxypyridine-2-carboxylate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $958
- Updated
- 2021/12/16
- Product number
- CHM0078248
- Product name
- 3-METHOXYPICOLINIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $1066.07
- Updated
- 2021/12/16
- Product number
- CHM0078248
- Product name
- 3-METHOXYPICOLINIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1630.86
- Updated
- 2021/12/16
- Product number
- W4763
- Product name
- Methyl3-methoxypyridine-2-carboxylate
- Packaging
- 250mg
- Price
- $143
- Updated
- 2021/12/16
3-METHOXYPICOLINIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
62733-99-7
74-88-4
24059-83-4
In a 50 mL round-bottomed flask equipped with a magnetic stirrer, methyl 3-hydroxy-2-pyridinecarboxylate (3.5 g, 22.80 mmol), potassium carbonate (3.46 g, 25.0 mmol), iodomethane (4.87 g, 34.3 mmol), and N,N-dimethylformamide (20 mL) were added sequentially. The reaction mixture was stirred at room temperature for 18 h under nitrogen protection. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (30 mL) and water (10 mL). The organic phase was separated and the aqueous phase was extracted with ethyl acetate (3 × 10 mL). The organic phases were combined, dried with anhydrous sodium sulfate, and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography with the eluent being a hexane solution of 30% ethyl acetate to give 2.1 g of methyl 3-methoxypyridine-2-carboxylate in 54% yield.
References
[1] ChemMedChem, 2016, vol. 11, # 23, p. 2607 - 2620
[2] Patent: WO2007/16525, 2007, A2. Location in patent: Page/Page column 50
[3] Patent: US2013/281396, 2013, A1. Location in patent: Paragraph 0310
[4] Patent: WO2018/52903, 2018, A1. Location in patent: Page/Page column 70-71
3-METHOXYPICOLINIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
3-METHOXYPICOLINIC ACID METHYL ESTER Suppliers
- Tel
- 021-31261262/ 49 (0)17662837245
- Fax
- (0)21-33250524
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- Germany
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