3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4
- Product Name
- 3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4
- CAS No.
- 15197-75-8
- Chemical Name
- 3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4
- Synonyms
- 2-Pyridylpropanoic acid;2-PYRIDINEPROPANOIC ACID;3-(2-Pyridinyl)propanoic acid;3-(2-Pyridyl)propionicacid,97%;2-(3-Pyridyl)propionic acid, 97%;3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4;2-Pyridinepropanoic acid (9CI, ACI);3-Pyridin-2-yl-propionic acid sulfate;3-Pyridin-2-yl-propionic acid H2SO4 ,95%;3-Pyridin-2-yl-propionic acid sulfuric acid
- CBNumber
- CB3335552
- Molecular Formula
- C8H9NO2
- Formula Weight
- 151.16
- MOL File
- 15197-75-8.mol
3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 Property
- Melting point:
- 140-145°C
- Boiling point:
- 287.4±15.0 °C(Predicted)
- Density
- 1.193±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- solid
- pka
- 3.87±0.10(Predicted)
- color
- Light brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H317May cause an allergic skin reaction
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 760226
- Product name
- 2-Pyridinepropionic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $171.35
- Updated
- 2025/07/31
- Product number
- B525688
- Product name
- 3-Pyridin-2-ylpropanoicAcid
- Packaging
- 25mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR909092
- Product name
- 3-(Pyridin-2-yl)propanoicacid
- Purity
- 98%
- Packaging
- 1g
- Price
- $130
- Updated
- 2021/12/16
- Product number
- OR909092
- Product name
- 3-(Pyridin-2-yl)propanoicacid
- Purity
- 98%
- Packaging
- 10g
- Price
- $595
- Updated
- 2021/12/16
- Product number
- V3472
- Product name
- 3-(Pyridin-2-yl)propanoicacid
- Packaging
- 10g
- Price
- $663
- Updated
- 2021/12/16
3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 Chemical Properties,Usage,Production
Synthesis
2859-68-9
15197-75-8
The general procedure for the synthesis of 3-pyridin-2-yl-propanoic acid from 3-(pyridin-2-yl)propan-1-ol was as follows: 3-(2-pyridinyl)-propanol (1 g, 7.6 mmol), water (13 mL), and concentrated sulfuric acid (0.59 mL, 5.1 mmol) were added to a 50 mL round-bottom flask equipped with a stirrer. Potassium permanganate (1.8 g, 11.3 mmol) was added to the stirring reaction mixture in batches over a period of 30 min while the reaction temperature was controlled at 50 °C. After the addition was completed, the reaction continued to be stirred at 50 °C until the color of the mixture changed to brown. Subsequently, the reaction mixture was warmed up to 80 °C and heated for 1 h. After completion of the reaction, it was filtered. The filtrate was concentrated to dryness under reduced pressure to afford the crude product 3-(2-pyridyl)-propionic acid (1.14 g), which could be used directly in the next step of the reaction without further purification. To obtain the pure product, the above crude product was dissolved in ethanol (10 mL), activated charcoal (0.1 g) was added, refluxed for 5 min and then hot filtered. The filtrate was cooled and crystallized to give pure 3-(2-pyridyl)-propionic acid (0.88 g, 78% yield).
References
[1] ACS Catalysis, 2018, vol. 8, # 7, p. 6738 - 6744
[2] Patent: US6162927, 2000, A
[3] Journal of Medicinal Chemistry, 2013, vol. 56, # 22, p. 9156 - 9169
[4] Journal of the American Chemical Society, 1951, vol. 73, p. 3156,3167
[5] Organic Process Research and Development, 2017, vol. 21, # 9, p. 1388 - 1393
3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 Preparation Products And Raw materials
Raw materials
Preparation Products
3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 Suppliers
- Tel
- 0838-5675166 15883665058
- Fax
- 0838-5675535
- nbcxkj@126.com
- Country
- China
- ProdList
- 914
- Advantage
- 55
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 025-86918202 4000255188
- Fax
- 86-025-86918232
- sales@pharmablock.com
- Country
- China
- ProdList
- 5000
- Advantage
- 55
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44734
- Advantage
- 61
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14101
- Advantage
- 59
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11036
- Advantage
- 64
- Tel
- 025-83697070
- Fax
- +86-25-83453306
- info@chemlin.com.cn
- Country
- China
- ProdList
- 14873
- Advantage
- 64
- Tel
- 021-34502253 13391330186
- Fax
- +86-21-23027826
- info@gksci.com
- Country
- China
- ProdList
- 133
- Advantage
- 52
- Tel
- +86-25-68710855, +86-25-68710897
- Fax
- 025-68710856
- sales@springpharma.net
- Country
- China
- ProdList
- 1261
- Advantage
- 62
View Lastest Price from 3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 manufacturers
- Product
- 3-PYRIDIN-2-YL-PROPIONIC ACID H2SO4 15197-75-8
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2019-12-26