1-BOC-2-METHYL-PIPERIDIN-4-ONE

Product Name: 1-BOC-2-METHYL-PIPERIDIN-4-ONE
CAS No.: 190906-92-4
Chemical Name: 1-BOC-2-METHYL-PIPERIDIN-4-ONE
Synonyms: TERT-BUTYL 2-METHYL-4-OXOPIPERIDINE-1-CARBOXYLATE;N-Boc-2-methyl-piperidone;1-Boc-2-Methyl-Piperidinone;1-Boc-2-methyl-4-piperidi...;1-Boc-2-methyl-4-piperidinone;1-BOC-2-METHYL-PIPERIDIN-4-ONE;2-Methyl-4-oxo-piperidine-1-Boc;1-N-BOC-2-METHYL-PIPERIDIN-4-ONE;N-Boc-(+/-)-2-methyl-4-piperidone;2-Methyl-4-oxo-piperidine-1-Boc 97%
CBNumber: CB3358791
Molecular Formula: C11H19NO3
Formula Weight: 213.27
MOL File: 190906-92-4.mol

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1-BOC-2-METHYL-PIPERIDIN-4-ONE Property

Boiling point:: 298.8±33.0 °C(Predicted)
Density: 1.060±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -1.52±0.40(Predicted)
form: solid
color: White to light yellow
InChI: InChI=1S/C11H19NO3/c1-8-7-9(13)5-6-12(8)10(14)15-11(2,3)4/h8H,5-7H2,1-4H3
InChIKey: HQMYWQCBINPHBB-UHFFFAOYSA-N
SMILES: N1(C(OC(C)(C)C)=O)CCC(=O)CC1C
CAS DataBase Reference: 190906-92-4(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
Hazard Note: Irritant
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H310Fatal in contact with skin

H341Suspected of causing genetic defects

H351Suspected of causing cancer

H360May damage fertility or the unborn child

H362May cause harm to breast-fed children

H370Causes damage to organs

H372Causes damage to organs through prolonged or repeated exposure

Precautionary statements

P201Obtain special instructions before use.

P202Do not handle until all safety precautions have been read and understood.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P262Do not get in eyes, on skin, or on clothing.

P263Avoid contact during pregnancy/while nursing.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B423308
Product name: tert-Butyl2-Methyl-4-oxopiperidine-1-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140300
Product name: tert-Butyl 2-methyl-4-oxopiperidine-1-carboxylate
Packaging: 250mg
Price: $50
Updated: 2021/12/16

AK Scientific

Product number: S954
Product name: 1-Boc-2-methyl-4-piperidinone
Packaging: 250mg
Price: $78
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140300
Product name: tert-Butyl 2-methyl-4-oxopiperidine-1-carboxylate
Packaging: 500mg
Price: $80
Updated: 2021/12/16

Apolloscientific

Product number: OR9058
Product name: 2-Methylpiperidin-4-one,N-BOCprotected
Purity: 97%
Packaging: 5g
Price: $95
Updated: 2021/12/16

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1-BOC-2-METHYL-PIPERIDIN-4-ONE Chemical Properties,Usage,Production

Uses

1-Boc-2-methyl-piperidin-4-one s a crucial compound that could be used as a pharmaceutical intermediate in pharmaceutical synthesis and scientific research.

Synthesis

126503-08-0

190906-92-4

1-tert-butoxycarbonyl-2-methyl-4-piperidone vinyl acetal (6.00 g) was used as starting material and dissolved in acetone (150 mL). To this solution, p-toluenesulfonic acid monohydrate (4.40 g) was slowly added under ice bath cooling and stirring conditions. After addition, the reaction mixture was gradually warmed to room temperature with continuous stirring overnight. Upon completion of the reaction, the reaction mixture was diluted with ethyl acetate and the organic layer was subsequently washed with saturated sodium bicarbonate solution and saturated aqueous sodium chloride solution sequentially. The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to remove the solvent to afford 1-tert-butoxycarbonyl-2-methyl-piperidone (2.40 g, 48% yield) as a yellow oil. Its 1H NMR (500 MHz, CDCl3) data were as follows: δ 1.18 (3H, d, J=7.0 Hz), 1.49 (9H, s), 2.20-2.30 (1H, m), 2.30-2.40 (1H, m), 2.45-2.55 (1H, m), 2.65-2.70 (1H, m), 3.25-3.35 ( 1H, m), 3.90-4.05 (1H, m), 4.20-4.30 (1H, m).

References

[1] Patent: EP1375482, 2004, A1. Location in patent: Page 153

1-BOC-2-METHYL-PIPERIDIN-4-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-BOC-2-METHYL-PIPERIDIN-4-ONE Suppliers

China 124 Germany 2 India 1 United Kingdom 4 United States 20 Global 151

Aikon International Limited

Tel: 025-58859352 18921922613
Email: hywu@aikonchem.com
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J & K SCIENTIFIC LTD.

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Fax: 86-10-82849933
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Energy Chemical

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Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
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Capot Chemical Co., Ltd

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Tetranov Biopharm

Tel: 13526569071
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Shanghai Hanhong Scientific Co.,Ltd.

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China DongFan Chemical Co.,LTD

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Shanghai AmasPharm Co., Ltd.

Tel: 021-54540637 18621091017
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Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
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View Lastest Price from 1-BOC-2-METHYL-PIPERIDIN-4-ONE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1-BOC-2-METHYL-PIPERIDIN-4-ONE 190906-92-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

Career Henan Chemical Co

Product: 1-BOC-2-METHYL-PIPERIDIN-4-ONE 190906-92-4
Price: US $8.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 100kg
Release date: 2019-08-05

190906-92-4, 1-BOC-2-METHYL-PIPERIDIN-4-ONERelated Search:

1-BOC-2-PHENYL-PIPERIDIN-4-ONE N-Boc-Nortropinone 1-BOC-2-BENZYL-PIPERIDIN-4-ONE 1-BOC-2-METHYL-PIPERIDIN-4-ONE 2-Methyl-4-piperidone 1-BOC-2-ETHYL-PIPERIDIN-4-ONE TERT-BUTYL 5-OXO-2-AZABICYCLO[2.2.1]HEPTANE-2-CARBOXYLATE 1-Piperidinecarboxylicacid,2-methyl-4-oxo-,1,1-dimethylethylester,(2R)-(9CI) 1-Piperidinecarboxylicacid,2-methyl-4-oxo-,1,1-dimethylethylester,(2S)-(9CI) TERT-BUTYL 4-OXO-1-AZASPIRO[5.5]UNDECANE-1-CARBOXYLATE 1-BOC-2-ISOPROPYL-PIPERIDIN-4-ONE TERT-BUTYL (2S)-2-BENZYL-4-OXOPIPERIDINE-1-CARBOXYLATE 1-BOC-2-TERT-BUTYL-PIPERIDIN-4-ONE tert-butyl 8-oxo-5-azaspiro[3.5]nonane-5-carboxylate TERT-BUTYL (2R)-2-BENZYL-4-OXOPIPERIDINE-1-CARBOXYLATE 1-BOC-2-PROPYL-PIPERIDIN-4-ONE 1-BOC-3-METHYL-PIPERIDIN-4-ONE (2S)-N-BOC-4-OXOPIPECOLIC ACID

1-BOC-2-METHYL-PIPERIDIN-4-ONE

2-METHYL-4-OXOPIPERIDINE, N-BOC PROTECTED

1-N-BOC-2-METHYL-PIPERIDIN-4-ONE

1-TERT-BUTOXYCARBONYL-2-METHYL-4-PIPERIDONE

TERT-BUTYL 2-METHYL-4-OXOPIPERIDINE-1-CARBOXYLATE

1-Boc-2-methyl-4-piperidinone

1-Boc-2-Methyl-Piperidinone

2-Methyl-4-oxopiperidine, N-BOC protected 97%

N-Boc-2-methyl-piperidone

1-(tert-Butoxycarbonyl)-2-methylpiperidin-4-one

2-Methyl-4-oxo-piperidine-1-carboxylic acid tert-butyl ester

1-Boc-2-methyl-4-piperidi...

2-Methyl-4-oxo-piperidine-1-Boc

2-Methyl-4-oxopiperidine, N-BOC protected, tert-Butyl 2-methyl-4-oxopiperidine-1-carboxylate, 1-(tert-Butoxycarbonyl)-2-methylpiperidin-4-one

2-Methylpiperidin-4-one, N-BOC protected 97%

1-Piperidinecarboxylicacid,2-Methyl-4-oxo-,1,1-diMethylethylester

tert-butyl 2-Methyl-3-oxopiperidine-1-carboxylate

2-Methyl-4-oxo-piperidine-1-Boc 97%

utyl 2-Methyl-4-oxopiperidine-1-carboxylate

1-Boc-2-Methyl-4-piperidinone/tert-butyl 2-Methyl-4-oxopiperidine-1-carboxylate

2-Methylpiperidin-4-one, N-BOC protected

N-Boc-(+/-)-2-methyl-4-piperidone

190906-92-4

Pyrans, Piperidines & Piperazines

pharmacetical

Pyrans, Piperidines &Piperazines

Piperidine

Piperidines