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(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID

Product Name
(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID
CAS No.
20876-29-3
Chemical Name
(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID
Synonyms
5-Methoxy-2-nitrobenzeneacetic acid;2-(5-methoxy-2-nitrophenyl)aceticaci;(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID;Benzeneacetic acid, 5-Methoxy-2-nitro-;(5-Methoxy-2-nitro-phenyl)-acetic acid ,97%
CBNumber
CB3416057
Molecular Formula
C9H9NO5
Formula Weight
211.17
MOL File
20876-29-3.mol
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(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID Property

Melting point:
176 °C
Boiling point:
404.7±30.0 °C(Predicted)
Density 
1.382±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
3.83±0.10(Predicted)
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M219743
Product name
2-(5-Methoxy-2-nitrophenyl)aceticAcid
Packaging
50mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0290210
Product name
(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID
Purity
98.00%
Packaging
5MG
Price
$502.57
Updated
2021/12/16
AK Scientific
Product number
0675AB
Product name
2-(5-Methoxy-2-nitrophenyl)aceticacid
Packaging
250mg
Price
$113
Updated
2021/12/16
AK Scientific
Product number
0675AB
Product name
2-(5-Methoxy-2-nitrophenyl)aceticacid
Packaging
25g
Price
$1108
Updated
2021/12/16
Matrix Scientific
Product number
132365
Product name
2-(5-Methoxy-2-nitrophenyl)aceticacid
Purity
97%
Packaging
10g
Price
$1684
Updated
2021/12/16
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(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID Chemical Properties,Usage,Production

Synthesis Reference(s)

Journal of the American Chemical Society, 77, p. 670, 1955 DOI: 10.1021/ja01608a039

Synthesis

89302-15-8

20876-29-3

General procedure for the synthesis of 2-nitro-5-methoxyphenylacetic acid from 5-methoxy-2-nitrophenylacetonitrile: 1 equivalent of 5-methoxy-2-nitrophenylacetonitrile was dissolved in a mixture of acetic acid (AcOH) and concentrated hydrochloric acid (HCl) (1:5, v/v), and the reaction mixture was heated for 4 hr under reflux conditions. Upon completion of the reaction, the target product 2-nitro-5-methoxyphenylacetic acid was extracted with ethyl acetate and the organic phase was dried with anhydrous sodium sulfate (Na2SO4), followed by removal of solvent by rotary evaporator to give the product.

References

[1] Tetrahedron Letters, 2014, vol. 56, # 1, p. 89 - 94
[2] Bioorganic and Medicinal Chemistry, 2010, vol. 18, # 4, p. 1482 - 1496

(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID Suppliers

Service Chemical Inc.
Tel
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Fax
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Email
sales@chemos-group.com
Country
Germany
ProdList
6350
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