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METHYL 3-FLUOROPHENYLACETATE

Product Name
METHYL 3-FLUOROPHENYLACETATE
CAS No.
64123-77-9
Chemical Name
METHYL 3-FLUOROPHENYLACETATE
Synonyms
Methyl 2-(3-fluorophenyl);METHYL 3-FLUOROPHENYLACETATE;Methyl 2-(3-fluorophenyl)acetate;Methyl 3-fluorophenylacetate,98%;Methyl 3-Fluorophenylacetate >Methyl 3-fluorophenylacetate, 97.5%;3-Fluorobenzeneacetic acid methyl ester;(3-Fluorophenyl)acetic acid methyl ester;2-(3-Fluorophenyl)acetic acid methyl ester;Benzeneacetic acid, 3-fluoro-, methyl ester
CBNumber
CB3418778
Molecular Formula
C9H9FO2
Formula Weight
168.16
MOL File
64123-77-9.mol
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METHYL 3-FLUOROPHENYLACETATE Property

Boiling point:
204.0±15.0℃ (760 Torr)
Density 
1.148±0.06 g/cm3 (20 ºC 760 Torr)
refractive index 
1.487-1.489
Flash point:
75.3±15.3℃
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid
color 
Clear colorless to slightly yellow
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Safety

Hazard Codes 
Xn
Risk Statements 
22
Safety Statements 
24/25
HazardClass 
IRRITANT
HS Code 
29163990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
M2536
Product name
Methyl 3-Fluorophenylacetate
Purity
>98.0%(GC)
Packaging
5g
Price
$60
Updated
2025/07/31
TCI Chemical
Product number
M2536
Product name
Methyl 3-Fluorophenylacetate
Purity
>98.0%(GC)
Packaging
25g
Price
$208
Updated
2025/07/31
TRC
Product number
M321358
Product name
Methyl2-(3-Fluorophenyl)acetate
Packaging
500mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
058253
Product name
Methyl 2-(3-fluorophenyl)acetate
Purity
95+%
Packaging
25g
Price
$98
Updated
2021/12/16
AK Scientific
Product number
7277AE
Product name
Methyl2-(3-fluorophenyl)acetate
Packaging
1g
Price
$10
Updated
2021/12/16
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METHYL 3-FLUOROPHENYLACETATE Chemical Properties,Usage,Production

Chemical Properties

clear colorless to slightly yellow liquid

Synthesis

67-56-1

331-25-9

64123-77-9

General steps: 1. Thionyl chloride (4.00 mL, 52.2 mmol) was slowly added to a solution of 3-fluorophenylacetic acid (24.85 g, 158 mmol) in methanol (200 mL) at 0 °C. 2. The reaction mixture was stirred at room temperature for 3 hours and then concentrated under reduced pressure to remove the solvent. 3. The concentrated residue was extracted by partitioning between 1N sodium hydroxide solution (250mL) and ethyl acetate (250mL). 4. The organic layer was separated and washed with brine (100 mL) and subsequently dried over anhydrous magnesium sulfate. 5. The desiccant was removed by filtration and the filtrate was concentrated under reduced pressure to afford the colorless oily product methyl (3-fluorophenyl)acetate (25.81 g, 97% yield). Product characterization data: 1H NMR (CDCl3) δ 3.62 (2H, s), 3.71 (3H, s), 6.92-7.09 (3H, m), 7.29 (1H, ddd, J = 7.9, 7.7, 6.0 Hz);. IR (KBr) cm-1: 3065, 3024, 3001, 1955, 2845, 1740, 1616, 1593, 1489, 1450, 1437, 1342, 1258, 1200, 1165, 1144, 1076, 1015, 955, 930.

References

[1] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 13, p. 2843 - 2866
[2] Advanced Synthesis and Catalysis, 2012, vol. 354, # 4, p. 751 - 756
[3] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 14, p. 3719 - 3735
[4] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 15, p. 4694 - 4703
[5] Tetrahedron, 2002, vol. 58, # 51, p. 10113 - 10126

METHYL 3-FLUOROPHENYLACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 3-FLUOROPHENYLACETATE Suppliers

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View Lastest Price from METHYL 3-FLUOROPHENYLACETATE manufacturers

Career Henan Chemical Co
Product
Methyl 3-fluorophenylacetate 64123-77-9
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
1000kg
Release date
2018-12-25

64123-77-9, METHYL 3-FLUOROPHENYLACETATERelated Search:

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  • METHYL 3-FLUOROPHENYLACETATE
  • (3-Fluorophenyl)acetic acid methyl ester
  • 2-(3-Fluorophenyl)acetic acid methyl ester
  • 3-Fluorobenzeneacetic acid methyl ester
  • Methyl 3-fluorophenylacetate,98%
  • Methyl 2-(3-fluorophenyl)acetate
  • Methyl 2-(3-fluorophenyl)
  • Methyl 3-fluorophenylacetate, 97.5%
  • Methyl 3-Fluorophenylacetate &gt
  • Benzeneacetic acid, 3-fluoro-, methyl ester
  • METHYL 3-FLUOROPHENYLACETATE ISO 9001：2015 REACH
  • 64123-77-9