METHYL 3-FLUOROPHENYLACETATE
- Product Name
- METHYL 3-FLUOROPHENYLACETATE
- CAS No.
- 64123-77-9
- Chemical Name
- METHYL 3-FLUOROPHENYLACETATE
- Synonyms
- Methyl 2-(3-fluorophenyl);METHYL 3-FLUOROPHENYLACETATE;Methyl 2-(3-fluorophenyl)acetate;Methyl 3-fluorophenylacetate,98%;Methyl 3-Fluorophenylacetate >Methyl 3-fluorophenylacetate, 97.5%;3-Fluorobenzeneacetic acid methyl ester;(3-Fluorophenyl)acetic acid methyl ester;2-(3-Fluorophenyl)acetic acid methyl ester;Benzeneacetic acid, 3-fluoro-, methyl ester
- CBNumber
- CB3418778
- Molecular Formula
- C9H9FO2
- Formula Weight
- 168.16
- MOL File
- 64123-77-9.mol
METHYL 3-FLUOROPHENYLACETATE Property
- Boiling point:
- 204.0±15.0℃ (760 Torr)
- Density
- 1.148±0.06 g/cm3 (20 ºC 760 Torr)
- refractive index
- 1.487-1.489
- Flash point:
- 75.3±15.3℃
- storage temp.
- Sealed in dry,Room Temperature
- form
- Liquid
- color
- Clear colorless to slightly yellow
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H227Combustible liquid
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M2536
- Product name
- Methyl 3-Fluorophenylacetate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $60
- Updated
- 2025/07/31
- Product number
- M2536
- Product name
- Methyl 3-Fluorophenylacetate
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $208
- Updated
- 2025/07/31
- Product number
- M321358
- Product name
- Methyl2-(3-Fluorophenyl)acetate
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 7277AE
- Product name
- Methyl2-(3-fluorophenyl)acetate
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
- Product number
- 058253
- Product name
- Methyl 2-(3-fluorophenyl)acetate
- Purity
- 95+%
- Packaging
- 5g
- Price
- $29
- Updated
- 2021/12/16
METHYL 3-FLUOROPHENYLACETATE Chemical Properties,Usage,Production
Chemical Properties
clear colorless to slightly yellow liquid
Synthesis
67-56-1
331-25-9
64123-77-9
General steps: 1. Thionyl chloride (4.00 mL, 52.2 mmol) was slowly added to a solution of 3-fluorophenylacetic acid (24.85 g, 158 mmol) in methanol (200 mL) at 0 °C. 2. The reaction mixture was stirred at room temperature for 3 hours and then concentrated under reduced pressure to remove the solvent. 3. The concentrated residue was extracted by partitioning between 1N sodium hydroxide solution (250mL) and ethyl acetate (250mL). 4. The organic layer was separated and washed with brine (100 mL) and subsequently dried over anhydrous magnesium sulfate. 5. The desiccant was removed by filtration and the filtrate was concentrated under reduced pressure to afford the colorless oily product methyl (3-fluorophenyl)acetate (25.81 g, 97% yield). Product characterization data: 1H NMR (CDCl3) δ 3.62 (2H, s), 3.71 (3H, s), 6.92-7.09 (3H, m), 7.29 (1H, ddd, J = 7.9, 7.7, 6.0 Hz);. IR (KBr) cm-1: 3065, 3024, 3001, 1955, 2845, 1740, 1616, 1593, 1489, 1450, 1437, 1342, 1258, 1200, 1165, 1144, 1076, 1015, 955, 930.
References
[1] Bioorganic and Medicinal Chemistry, 2003, vol. 11, # 13, p. 2843 - 2866
[2] Advanced Synthesis and Catalysis, 2012, vol. 354, # 4, p. 751 - 756
[3] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 14, p. 3719 - 3735
[4] Bioorganic and Medicinal Chemistry, 2005, vol. 13, # 15, p. 4694 - 4703
[5] Tetrahedron, 2002, vol. 58, # 51, p. 10113 - 10126
METHYL 3-FLUOROPHENYLACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
METHYL 3-FLUOROPHENYLACETATE Suppliers
- Tel
- --
- Fax
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- sales-in@tcichemicals.com
- Country
- India
- ProdList
- 6768
- Advantage
- 58
- Tel
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- sales@ajchem.in
- Country
- India
- ProdList
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- Advantage
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View Lastest Price from METHYL 3-FLUOROPHENYLACETATE manufacturers
- Product
- Methyl 3-fluorophenylacetate 64123-77-9
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 95%-99%
- Supply Ability
- 1000kg
- Release date
- 2018-12-25