ChemicalBook > CAS DataBase List > 3,5-DIBROMOBENZYL ALCOHOL

3,5-DIBROMOBENZYL ALCOHOL

Product Name
3,5-DIBROMOBENZYL ALCOHOL
CAS No.
145691-59-4
Chemical Name
3,5-DIBROMOBENZYL ALCOHOL
Synonyms
RARECHEM AL BD 0770;3,5-DIBROMOBENZYL ALCOHOL;3,5-Dibromobenzenemethanol;(3,5-DibroMophenyl)Methanol;Benzenemethanol, 3,5-dibromo-;1,3-Dibromo-5-hydroxymethylbenzene
CBNumber
CB3422562
Molecular Formula
C7H6Br2O
Formula Weight
265.93
MOL File
145691-59-4.mol
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3,5-DIBROMOBENZYL ALCOHOL Property

Melting point:
107-108°C
Boiling point:
328℃
Density 
1.960
Flash point:
152℃
storage temp. 
Sealed in dry,Room Temperature
pka
13.98±0.10(Predicted)
Appearance
Light brown to brown Solid
Water Solubility 
Slightly soluble in water.
InChI
InChI=1S/C7H6Br2O/c8-6-1-5(4-10)2-7(9)3-6/h1-3,10H,4H2
InChIKey
ZQNSHKZQTZSNTB-UHFFFAOYSA-N
SMILES
C1(CO)=CC(Br)=CC(Br)=C1
CAS DataBase Reference
145691-59-4(CAS DataBase Reference)
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Safety

Hazard Codes 
C
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
HS Code 
2906290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
D422855
Product name
3,5-DibromobenzylAlcohol
Packaging
50mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD64456
Product name
3,5-Dibromobenzyl alcohol
Packaging
1g
Price
$70
Updated
2021/12/16
AK Scientific
Product number
X8143
Product name
3,5-Dibromobenzylalcohol
Packaging
1g
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD64456
Product name
3,5-Dibromobenzyl alcohol
Packaging
2g
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD64456
Product name
3,5-Dibromobenzyl alcohol
Packaging
5G
Price
$200
Updated
2021/12/16
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3,5-DIBROMOBENZYL ALCOHOL Chemical Properties,Usage,Production

Uses

It is used in the synthesis of substituted benzylamines.

Synthesis

618-58-6

145691-59-4

Step 1: To a stirred solution of 3,5-dibromobenzoic acid (2 g, 7.168 mmol) in tetrahydrofuran (20 mL) was slowly added borane dimethyl sulfide (3.4 mL, 35.842 mmol, 5 eq.) at 0 °C. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was carefully quenched with methanol (appropriate amount). Subsequently, the reaction mixture was concentrated under reduced pressure to afford (3,5-dibromophenyl)methanol as an off-white solid (1.8 g, 94% yield). The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 4.47 (d, J = 6Hz, 2H), 5.39 (t, J = 6Hz, 1H), 7.49 (s, 2H), 7.65 (s, 1H).

References

[1] Patent: WO2017/46739, 2017, A1. Location in patent: Page/Page column 60
[2] Patent: JP2005/120047, 2005, A. Location in patent: Page/Page column 165
[3] Synlett, 2002, # 2, p. 251 - 254
[4] European Journal of Medicinal Chemistry, 2011, vol. 46, # 9, p. 4227 - 4237

3,5-DIBROMOBENZYL ALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3,5-DIBROMOBENZYL ALCOHOL Suppliers

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View Lastest Price from 3,5-DIBROMOBENZYL ALCOHOL manufacturers

Career Henan Chemical Co
Product
3,5-DIBROMOBENZYL ALCOHOL 145691-59-4
Price
US $1.00/KG
Min. Order
1g
Purity
95-99%
Supply Ability
1MT/month
Release date
2019-07-31

145691-59-4, 3,5-DIBROMOBENZYL ALCOHOLRelated Search:

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  • RARECHEM AL BD 0770
  • (3,5-DibroMophenyl)Methanol
  • 1,3-Dibromo-5-hydroxymethylbenzene
  • 3,5-DIBROMOBENZYL ALCOHOL
  • Benzenemethanol, 3,5-dibromo-
  • 3,5-Dibromobenzenemethanol
  • 145691-59-4
  • Benzhydrols, Benzyl & Special Alcohols
  • Alcohol
  • Alcohols
  • Bromine Compounds