3,5-Dibenzyloxybenzaldehyde
Uses- Product Name
- 3,5-Dibenzyloxybenzaldehyde
- CAS No.
- 14615-72-6
- Chemical Name
- 3,5-Dibenzyloxybenzaldehyde
- Synonyms
- TIMTEC-BB SBB008628;3,5-BENZYLOXY BENZALDEHYDE;3,5-DIBENZYLOXYBENZALDEHYDE;3,5-DibroMobenzaldehyde, 95+%;3,5-BIS(BENZYLOXY)BENZALDEHYDE;3,5-Dibenzyloxybenzaldehyde>Benzaldehyde, 3,5-bis(phenylmethoxy)-
- CBNumber
- CB3476242
- Molecular Formula
- C21H18O3
- Formula Weight
- 318.37
- MOL File
- 14615-72-6.mol
3,5-Dibenzyloxybenzaldehyde Property
- Melting point:
- 78-80 °C (lit.)
- Boiling point:
- 502.4±40.0 °C(Predicted)
- Density
- 1.176±0.06 g/cm3(Predicted)
- storage temp.
- -20°C Freezer, Under inert atmosphere
- solubility
- Chloroform (Sparingly), Methanol (Slightly)
- form
- Solid
- color
- White to Brown
- InChI
- InChI=1S/C21H18O3/c22-14-19-11-20(23-15-17-7-3-1-4-8-17)13-21(12-19)24-16-18-9-5-2-6-10-18/h1-14H,15-16H2
- InChIKey
- CHUAMRVJSRBRHT-UHFFFAOYSA-N
- SMILES
- C(=O)C1=CC(OCC2=CC=CC=C2)=CC(OCC2=CC=CC=C2)=C1
- CAS DataBase Reference
- 14615-72-6(CAS DataBase Reference)
Safety
- Safety Statements
- 24/25
- WGK Germany
- 3
- HS Code
- 29125000
N-Bromosuccinimide Price
- Product number
- 368105
- Product name
- 3,5-Dibenzyloxybenzaldehyde
- Purity
- 98%
- Packaging
- 1g
- Price
- $49
- Updated
- 2023/01/07
- Product number
- D3184
- Product name
- 3,5-Dibenzyloxybenzaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $42
- Updated
- 2025/07/31
- Product number
- D3184
- Product name
- 3,5-Dibenzyloxybenzaldehyde
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $139
- Updated
- 2025/07/31
- Product number
- D448788
- Product name
- 3,5-Dibenzyloxybenzaldehyde
- Packaging
- 2.5g
- Price
- $70
- Updated
- 2021/12/16
- Product number
- FD61769
- Product name
- 3,5-Dibenzyloxybenzaldehyde
- Packaging
- 10g
- Price
- $75
- Updated
- 2021/12/16
3,5-Dibenzyloxybenzaldehyde Chemical Properties,Usage,Production
Uses
3,5-Dibenzyloxybenzaldehyde is a useful research chemical.
Uses
3,5-Dibenzyloxybenzaldehyde may be used in the synthesis of survivin dimerization modulators.
Synthesis
24131-31-5
14615-72-6
To a solution of (3,5-bis(benzyloxy)phenyl)methanol (9.9 g, 31.0 mmol) in dichloromethane (140 mL) was added dimethyl sulfoxide (22 mL, 0.31 mol) and diisopropylethylamine (26.92 mL, 0.154 mol). The reaction mixture was cooled to 0 °C, followed by the addition of sulfur trioxide-pyridine complex (14.76 g, 92.73 mmol). The reaction was stirred continuously at 0 °C for 1 h, after which the reaction was quenched with saturated aqueous sodium thiosulfate solution (310 mL). The reaction mixture was extracted with ethyl acetate (3 x 200 mL) and the organic layers were combined and dried over anhydrous magnesium sulfate. The solvent was removed by evaporation under reduced pressure to afford an oily crude product, which was purified by silica gel column chromatography using dichloromethane as eluent to give 3,5-dibenzyloxybenzaldehyde (9.2 g, 93% yield). The spectral data of the product were in agreement with those reported in the literature.
References
[1] Journal of Organic Chemistry, 1998, vol. 63, # 25, p. 9367 - 9374
[2] Journal of Medicinal Chemistry, 1993, vol. 36, # 20, p. 2950 - 2955
[3] Chemistry - A European Journal, 2009, vol. 15, # 10, p. 2278 - 2288
[4] ChemCatChem, 2017, vol. 9, # 20, p. 3880 - 3887
[5] ACS Catalysis, 2018, vol. 8, # 4, p. 3030 - 3034
3,5-Dibenzyloxybenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-Dibenzyloxybenzaldehyde manufacturers
- Product
- 3,5-Dibenzyloxybenzaldehyde 14615-72-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-12
- Product
- 3,5-Dibenzyloxybenzaldehyde 14615-72-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-15
- Product
- 3,5-Dibenzyloxybenzaldehyde 14615-72-6
- Price
- US $30.00-10.00/kg
- Min. Order
- 10kg
- Purity
- 99%
- Supply Ability
- 100000kg
- Release date
- 2024-08-20