3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE

Product Name: 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
CAS No.: 24422-15-9
Chemical Name: 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE
Synonyms: Rivaroxaban Impurity 166;trichlorothiophene-2-carbonyl chloride;3,4,5-trichloro-2-thiophenecarbonyl chloride;3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE;2-Thiophenecarbonyl chloride, 3,4,5-trichloro-;3,4,5-Trichlorothien-2-carboxylic acid chloride
CBNumber: CB3482535
Molecular Formula: C5Cl4OS
Formula Weight: 249.93
MOL File: 24422-15-9.mol

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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Property

Melting point:: 38-40°C
Boiling point:: 124-125°C 10mm
Flash point:: 124-125°C/10mm
Sensitive: Moisture Sensitive
BRN: 1427060

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Safety

Risk Statements: 34
Safety Statements: 26-36/37/39-45
RIDADR: 3261
HazardClass: 8
PackingGroup: II

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Alfa Aesar

Product number: L17704
Product name: 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
Packaging: 1g
Price: $38.9
Updated: 2021/12/16

Alfa Aesar

Product number: L17704
Product name: 3,4,5-Trichlorothiophene-2-carbonyl chloride, 97%
Packaging: 5g
Price: $118
Updated: 2021/12/16

AHH

Product number: MT-36791
Product name: 3,4,5-Trichlorothiophene-2-carbonylchloride
Purity: 97%
Packaging: 25g
Price: $300
Updated: 2021/12/16

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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Chemical Properties,Usage,Production

Preparation

3,4,5-Trichlorothiophene-2-carbonyl chloride synthesis: A mixture of 3,4,5-trichloro-2-thiophenecarboxylic acid (20.4 g, 0.088 mol), SOCl2 (7.3 mL, 0.1 mol), and DMF (0.2 mL) in 80 mL of 1,2-dichloroethane was heated at reflux temperature for 3 h. The reaction mixture became homogeneous after 1 h of heating. The solution was cooled to 25℃, concentrated and placed under high vacuum to remove residual solvent, giving 22.0 g (98% wt.) of 3,4,5-trichloro-2-thiophenecarbonyl chloride as an oil which solidified on standing to an off-white powder; m.p. 37-41℃, having a GC area % purity > 99%.

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Thionyl chloride n-Butyllithium TETRACHLOROTHIOPHENE

Preparation Products

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3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE Suppliers

China 11 Germany 2 India 2 United Kingdom 4 United States 4 Global 23

3B Scientific Corporation

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Email: sales@3bsc.com
Country: United States
ProdList: 6962
Advantage: 56

Riedel-de Haen AG

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Country: United States
ProdList: 6773
Advantage: 87

Alfa Aesar

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Country: United States
ProdList: 6814
Advantage: 81

3B Scientific Corporation

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Email: sales@3bsc.com
Country: United States
ProdList: 6718
Advantage: 47

24422-15-9, 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDERelated Search:

2,3-DICHLOROTHIOPHENE 5-CHLOROTHIOPHENE-2-CARBONYL CHLORIDE 4-CHLORO-2-THIOPHENECARBOXALDEHYDE 2-Chloro-5-chloromethylthiophene 3-Chlorothiophene-2-carbonyl chloride 3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE 2,3,4-TRICHLOROTHIOPHENE

3,4,5-Trichlorothien-2-carboxylic acid chloride

3,4,5-TRICHLOROTHIOPHENE-2-CARBONYL CHLORIDE

3,4,5-trichloro-2-thiophenecarbonyl chloride

2-Thiophenecarbonyl chloride, 3,4,5-trichloro-

Rivaroxaban Impurity 166

trichlorothiophene-2-carbonyl chloride

24422-15-9

C5Cl4OS