ChemicalBook > CAS DataBase List > TERT-BUTYL-3-BROMOBENZOATE

TERT-BUTYL-3-BROMOBENZOATE

Product Name
TERT-BUTYL-3-BROMOBENZOATE
CAS No.
69038-74-0
Chemical Name
TERT-BUTYL-3-BROMOBENZOATE
Synonyms
t-Butyl-3-bromobenzoate;TERT-BUTYL-3-BROMOBENZOATE;3-bromo-2-tert-butylbenzoate;tert-Butyl 3-bromobenzoate 95+%;Tert-Butyl 3-Bromobenzoate,Canonical;3-Bromobenzoic Acid-tert-Butyl Ester;Benzoic acid, 3-broMo-, 1,1-diMethylethyl ester
CBNumber
CB3486003
Molecular Formula
C11H13BrO2
Formula Weight
257.12
MOL File
69038-74-0.mol
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TERT-BUTYL-3-BROMOBENZOATE Property

storage temp. 
Sealed in dry,Room Temperature
form 
liquid
color 
Colourless
InChI
InChI=1S/C11H13BrO2/c1-11(2,3)14-10(13)8-5-4-6-9(12)7-8/h4-7H,1-3H3
InChIKey
NPVLZVSAZXTBSR-UHFFFAOYSA-N
SMILES
C(OC(C)(C)C)(=O)C1=CC=CC(Br)=C1
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B690513
Product name
t-Butyl3-bromobenzoate
Packaging
500mg
Price
$65
Updated
2021/12/16
AK Scientific
Product number
X2854
Product name
tert-Butyl3-bromobenzoate
Packaging
1g
Price
$75
Updated
2021/12/16
ChemScene
Product number
CS-M2538
Product name
Benzoicacid,3-bromo-,1,1-dimethylethylester
Purity
99.57%
Packaging
10g
Price
$99
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB142657
Product name
tert-Butyl 3-bromobenzoate
Packaging
5G
Price
$101
Updated
2021/12/16
SynQuest Laboratories
Product number
2623-9-03
Product name
tert-Butyl 3-bromobenzoate
Purity
98%
Packaging
250mg
Price
$15
Updated
2021/12/16
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TERT-BUTYL-3-BROMOBENZOATE Chemical Properties,Usage,Production

Synthesis

585-76-2

83766-88-5

69038-74-0

Boron trifluoride diethyl ether compound (0.31 g, 2.21 mmol) was added as m-bromobenzoic acid (0.2 g, 1.64 mmol) and 2-(tert-butoxy)pyridine (0.33 g, 2.21 mmol) after dissolution in anhydrous toluene (2 mL). The reaction mixture was stirred at room temperature for 30 min, followed by quenching the reaction with anhydrous sodium bicarbonate. The reaction mixture was diluted with ethyl acetate (30 mL) and washed sequentially with water (20 mL) and brine (20 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure. The resulting residue was purified by fast column chromatography on silica gel with dichloromethane/hexane (0:4 to 1:4) as eluent to afford the target product tert-butyl m-bromobenzoate (5a) as a colorless oil.

References

[1] Tetrahedron, 2018, vol. 74, # 27, p. 3748 - 3754

TERT-BUTYL-3-BROMOBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from TERT-BUTYL-3-BROMOBENZOATE manufacturers

Career Henan Chemical Co
Product
TERT-BUTYL-3-BROMOBENZOATE 69038-74-0
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
100kg
Release date
2018-12-20

69038-74-0, TERT-BUTYL-3-BROMOBENZOATERelated Search:

Tert-butyl 3-chloro-2-methoxyisonicotinate tert-butyl 3-fluoro-5-(methylthio)benzoate Tert-butyl 3-bromo-4-methoxybenzoate tert-butyl 3-Bromo-4-iodo-5-methylbenzoate tert-Butyl 3-fluoro-4-methylbenzoate 3-Bromo-5-trifluoromethyl-benzoic acid tert-butyl ester 2,2-Dimethoxy-2-phenylacetophenone TERT-BUTYL-4-BROMOBENZOATE TERT-BUTYL-2-BROMOBENZOATE Tert-Butyl-4'-bromobenzoate-2'-boronicacid tert-Butyl 5-bromo-2-chlorobenzoate TERT-BUTYL 3-BROMO-4-NITROBENZOATE TERT-BUTYL-3-BROMOBENZOATE T-BUTYL 3-BROMO-4-FLUOROBENZOATE

  • 3-bromo-2-tert-butylbenzoate
  • tert-Butyl 3-bromobenzoate 95+%
  • t-Butyl-3-bromobenzoate
  • Benzoic acid, 3-broMo-, 1,1-diMethylethyl ester
  • TERT-BUTYL-3-BROMOBENZOATE
  • 3-Bromobenzoic Acid-tert-Butyl Ester
  • Tert-Butyl 3-Bromobenzoate,Canonical
  • 69038-74-0
  • Esters
  • Phenyls & Phenyl-Het
  • Aryl
  • Ester
  • Organohalides
  • Phenyls & Phenyl-Het