ChemicalBook > CAS DataBase List > 3-(Aminomethyl)-1-methylpiperidine

3-(Aminomethyl)-1-methylpiperidine

Product Name
3-(Aminomethyl)-1-methylpiperidine
CAS No.
14613-37-7
Chemical Name
3-(Aminomethyl)-1-methylpiperidine
Synonyms
(1-METHYLPIPERIDIN-3-YL)METHANAMINE;CHEMBRDG-BB 4103006;1-Methyl-3-(aminomethyl)p...;3-AMINOMETHYL-1-METHYLPIPERIDINE;1-Methyl-3-piperidinemethanamine;(1-METHYLPIPERID-3-YL)METHYLAMINE;(1-methyl-3-piperidyl)methanamine;3-PIPERIDINEMETHANAMINE, 1-METHYL-;N-Methyl-3-(aMinoMethyl)piperidine;N-Methyl-3-(aMinoMethyl)-piperidin
CBNumber
CB3687503
Molecular Formula
C7H16N2
Formula Weight
128.22
MOL File
14613-37-7.mol
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3-(Aminomethyl)-1-methylpiperidine Property

Boiling point:
58°C/6mm
Density 
0.9096 g/cm3
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
10.12±0.29(Predicted)
form 
liquid
color 
Colourless to pale yellow
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
22
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H318Causes serious eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
A613905
Product name
3-(Aminomethyl)-1-methylpiperidine
Packaging
25mg
Price
$45
Updated
2021/12/16
TRC
Product number
A613905
Product name
3-(Aminomethyl)-1-methylpiperidine
Packaging
250mg
Price
$145
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-1-M3
Product name
3-(Aminomethyl)-1-methylpiperidine
Packaging
1g
Price
$225
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA51097
Product name
3-(Aminomethyl)-1-methyl-piperidine
Packaging
500mg
Price
$360
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA51097
Product name
3-(Aminomethyl)-1-methyl-piperidine
Packaging
1g
Price
$435
Updated
2021/12/16
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3-(Aminomethyl)-1-methylpiperidine Chemical Properties,Usage,Production

Synthesis

672324-98-0

14613-37-7

3-(Di-tert-butoxymethylamino)-1-methylpiperidine (500 mg, 1.52 mmol) was used as raw material and dissolved in a 1,4-dioxane solution (19.75 mL) of methanol (7.5 mL) and 10% (v/v) concentrated sulfuric acid. The reaction mixture was stirred at 25°C for 0.5 hours. Methanol (300 mL) was then added and BioRad AG1-X8 resin (OH type) was added until the pH reached 10. The resin was removed by filtration and the resin was washed with methanol (2 x 200 mL). The eluates were combined and evaporated to dryness, and the residue was purified by silica gel column chromatography (30 × 2.5 cm) to afford 3-(aminomethyl)-1-methylpiperidine (69.2 mg, 35%) using 10% concentrated ammonium hydroxide in methanol solution-dichloromethane as eluent. The product characterization data were as follows: FABMS: m/z 129.1 (MH+); HRFABMS: m/z 129.1392 (MH+), calculated value C7H17N2: m/z 129.1392; 1H NMR (CDCl3) δ 0.90 (2H, m, CH2), 1.65 (2H, m, CH2), 1.72 (1H, m. CH), 1.79 (1H, m, CH2), 1.91 (1H, m, CH2), 2.30 (3H, s, NCH3), 2.64 (2H, m, CH2), 2.82 (1H, m, CH2NH2), 2.92 (1H, m, CH2NH2); 13C NMR (CDCl3) δ CH3: 46.7; CH2: 25.2, 28.0, 46.0, 36.4, 60.3; CH: 39.9.

References

[1] Patent: WO2004/22561, 2004, A1. Location in patent: Page 109

3-(Aminomethyl)-1-methylpiperidine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(Aminomethyl)-1-methylpiperidine manufacturers

Career Henan Chemical Co
Product
3-(Aminomethyl)-1-methylpiperidine 14613-37-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2019-12-20

14613-37-7, 3-(Aminomethyl)-1-methylpiperidineRelated Search:

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